Flash Lamps as Ignition and Initiation Sources of the VS-2 Pyrotechnic Composition

In the present work it is found that the pyrotechnic composition VS-2 can be initiated with flash lamps IFC-500 and EVIS. VS-2 pyrotechnic composition contains 90% of mercury（Ⅱ） 5-hydrazinotetrazolate perchlorate and 10% of optically transparent copolymer of 2-methyl-5-vinyltetrazole and methacrylic acid （PVMT）. We have found that the flash lamps make it possible to initiate combustion of VS-2 composition with its transition to detonation both in cylindrical charges placed in brass caps of 5 mm diameter and 2 mm high， and film charges with 10 mm×80 mm in size and surface weights of 60 mg·cm^-2 and 90 mg·cm^-2， showing ignition delay times 10 μs and 3 μs， respectively. We also measured detonation velocities for VS-2 composition film charges， which were 4375-4505 m·s^-1 （of the charge being surface mass 60 mg·cm^-2） and 4221-4281 m·s^-1 （of the charge being surface mass 90 mg·cm^-2） and their blasting action on the aluminum plate. The depths of the normal shock wave imprints at the charge-barrier interface were 0.6-0.7 mm （for surface mass of the film charges 60 mg·cm^-2） and 1.2-1.3 mm （for surface mass of the film charges 90 mg·cm^-2）.     

Advantages and disadvantages of nuclear reactions used in reactors or cyclotrons,in addition to a theoretical study based on photodisintegration on natural indium for 111Ag production

Production routes were recorded on available reactions for ¹¹¹Ag production from nuclear reactors or cyclotrons using a natural palladium target based on ¹¹⁰Pd（n, γ） and ¹¹⁰pd（d, n） reactions, respectively.^natCd（γ,x） based on ¹¹⁰Cd（γ, p） has also been studied as a prospective reaction for the production of ¹¹¹Ag. Unfortunately, these nuclear reactions are difficult to utilize because, in some cases, they reduce the specific activi...     

Fe3O4-carbon spheres core–shell supported palladium nanoparticles: A robust and recyclable catalyst for suzuki coupling reaction

Suzuki-Miyaura (S-M) is regarded the most powerful way for synthesis biaryls, triaryls, or incorporating of substituted aryl moieties in organic preparation by the cross-coupling of aryl boronic acid with aryl halides using the Pd catalyst. This work reports the combining of the hydrothermal and microwave-assisted protocol to convert the glucose to magnetic carbon spheres (Fe₃O₄-CSPs) decorated with Pd nanoparticles (NPs) as the catalyst for Suzuki-Miyaura cross-coupling reactions. The physicochemical properties in the produced composite were examined using FESEM, HRTEM, nitrogen isotherms, Raman spectroscopy, FTIR, XPS, and XRD. The as-fabricated composite Pd/Fe₃O₄-CSPs is mostly spherical with a core–shell structure and possesses a great surface area of 253.2 m²·g^-1. Its catalytic performance demonstrates that the composite has excellent stability and high tolerance Suzuki-Miyaura cross-coupling reactions in 30 min at 80 ℃. Both activated and deactivated aryl halides provided excellent yield. The as-fabricated catalyst was recycled for up to four catalytic cycles without a substantial decline in performance. Moreover, this research offers a facile roadmap for synthesizing Pd/Fe₃O₄-CSPs composites and promoting the practical implementation of Pd/Fe₃O₄-CSPs catalysts for organic transformation processes.     

Metal-organic Frameworks Derived Cobalt Encapsulated in Nitrogen-doped Porous Carbon Nanosheets for Oxygen Reduction Reaction and Rechargeable Zinc-air Batteries

Nitrogen(N)-doped carbon nanosheets(TCM-900) were prepared by pyrolyzing the cobalt metal organic framework(MOF) and acid treatment.The TCM-900 showed outstanding ORR performance with half-potential of 0.805 V.The density function theory(DFT) reveals the nitrogen activates the carbon atoms in the framework.The homemade ZAB with TCM-900 as ORR electrocatalyst exhibits high-power density of 45 mW·cm^-2 and excellent long recharge cycling stability compared to Pt/C at 10 mA·cm^-2     

基于CAN总线的矿用电喷柴油机单轨吊电控系统开发

目前井下的矿用柴油机基本上都是基于机械泵的柴油机,存在尾气排放不达标,污染严重,油耗高,可靠性、智能化水平不高,严重影响推广应用。基于此我们开发了矿用电喷柴油机单轨吊。该柴油机单轨吊排放达到国三标准,具有低污染、低油耗、高可靠性,智能化水平高等优点。     

2016—2017年北天山地区两次6级地震前地电场异常

地下介质在应力积累过程中，会导致岩体裂隙结构变化，从而使得大地电场E_T的优势方位角发生变化.文中收集了2016年到2017年的数据，利用大地电场优势方位角方法，提取与分析了北天山地区2016年12月8日呼图壁6.2级和2017年8月9日精河6.6级地震前地电场异常，探讨这两次6级地震前的地电场异常表现特征.结果表明:这两次地震前，震中周围的乌鲁木齐、克拉玛依台均显示出显著的地电场异常，即岩体裂隙优势方位角异常；异常特征以突跳和偏转为主；岩体裂隙结构发生异常时间上存在准同步性，表现出短临异常信息.因此，地电场岩体裂隙优势方位角方法短期内具有一定的预报效能，可为今后利用地电场方法预测地震积累经验和震例.