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排序方式: 共有142条查询结果,搜索用时 265 毫秒
1.
Caio Felippe Curitiba Marcellos Camila M. Senna Figueiredo Frederico W. Tavares Maurício Bezerra de Souza Jr. Paulo Laranjeira da Cunha Lage João Francisco Cajaiba da Silva Argimiro R. Secchi Amaro G. Barreto Jr. 《加拿大化工杂志》2020,98(11):2435-2450
An experimental methodology for inferring brine dissolution rate in monoethylene glycol (MEG) solutions at different temperatures using a webcam combined with a mathematical model is presented. The measurement system is designed to track the RGB (red, green, and blue) colour variations during the dissolution process. A dynamic model augmented with the population balance equation is applied to describe the dissolution process. Moreover, the dissolution rate is consistently related to the temperature and MEG concentration through the driving force based on the Gibbs energy and chemical affinity. The applied low-cost measurement apparatus proved to be a useful resource for tracking the dissolution dynamics in a wide range of undersaturation. 相似文献
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Valéria T. Crexi Micheli L. Monte Maurício L. Monte Luiz A. A. Pinto 《Journal of the American Oil Chemists' Society》2012,89(2):329-334
The aims of this study were to compare three treatments in the chemical hydrolysis reaction of bleached oil from carp (Cyprinus carpio) heads and to obtain polyunsaturated fatty acid concentrates by urea complexation. The three treatments were carried out
with different oil:ethanol molar ratios. In the treatment with a 1:39 molar ratio, a higher yield of free fatty acids was
found. These fatty acids were submitted to urea complexation (−10 °C for 20 h, and urea–fatty acid ratio of 4.5–1). There
was a 31.4% increase in monounsaturated and polyunsaturated fatty acids (MUFA and PUFA) content and a 75% decrease in saturated
fatty acids (SAF) content. An increase of 85.4% in the EPA + DHA content was found. The non-urea complexing fraction can be
considered a rich source of MUFA and PUFA with a total amount of 88.9%. 相似文献
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Daniel Discini Silveira José de Souza Lima Maurício Silveira 《International Journal of Communication Systems》2014,27(12):4346-4354
For the fast prototyping, production, and delivery of commercial radio frequency products/systems, accurate and reliable test systems are necessary. These systems are usually product customized and thus expensive solutions, capable of performing all necessary measurements for a specific product. The purpose of this paper is to present a flexible cost‐effective test solution, capable of realizing all necessary measurement on a high output power amplifier system greater than 500 W, and to generate essential reports. These reports allow the system operator to (i) perform an analysis and a statistical comparison among various products, assuring that the quality is the same for all products; and (ii) retain products that present a performance poorer than other similar products, without a rigorous technical analysis, thus increasing efficiency in factory assembly line. Copyright © 2013 John Wiley & Sons, Ltd. 相似文献
7.
Comparison of vacuum impregnation and soaking techniques for addition of the probiotic Lactobacillus acidophilus to minimally processed melon 下载免费PDF全文
Patrícia Martins de Oliveira Afonso Mota Ramos Eliane Maurício Furtado Martins Érica Nascif Rufino Vieira Ariana de Souza Soares Marcel Cardoso de Noronha 《International Journal of Food Science & Technology》2017,52(12):2547-2554
This study aimed to evaluate the vacuum impregnation (VI) and soaking methods in the addition of Lactobacillus acidophilusLA‐3 to minimally processed melon (MPM). The melons were washed, sanitised in chlorine solution (200 mg L?1), peeled and cutted into cubes. Lactobacillus acidophilusLA‐3 (1.4 × 1010 CFU g?1) were added to the MPM through both techniques. The L. acidophilusLA‐3 count in MPM was similar to those commonly found in dairy products having probiotic claim, but VI was more efficient than soaking in maintaining the viability (8.61 and 7.98 Log CFU g?1, respectively). The pH, acidity and soluble solids were not affected by probiotic culture and the incorporation technique; however, the VI affected the firmness of fruit. The MPM was within Brazilian standards for their microbiological characteristics. MPM may be used as a carrier of probiotic bacteria, being one more alternative for individuals who consume probiotic products. 相似文献
8.
Determination of alcohols and volatile organic acids in anaerobic bioreactors for H2 production by near infrared spectroscopy 总被引:1,自引:0,他引:1
Maurílio Gustavo Nespeca Caroline Varella Rodrigues Kamili Oliveira Santana Sandra Imaculada Maintinguer José Eduardo de Oliveira 《International Journal of Hydrogen Energy》2017,42(32):20480-20493
In recent years, near infrared (NIR) spectroscopy has been investigated as a tool for monitoring anaerobic digesters, but several adversities in its application have been reported. This study proposes the application of NIR for the determination of alcohols and volatile organic acids from H2 production bioreactors and evaluates different approaches to optimize the prediction models. Partial least squad (PLS) models were developed using samples from anaerobic batch reactors fed with crude glycerol for wastewater treatment. The analytes predicted were: methanol, ethanol, 1-butanol, acetic, propanoic, butyric, isocaproic and total volatile organic acids (VFA). The optimization of the predictive capacity of the models was achieved through the orthogonal signal correction (OSC) preprocessing and the selection of variables performed by the genetic algorithm (GA). The application of the proposed models were based on the following figures of merit: accuracy, precision, linearity, limits of detection and quantitation, measurement interval, sensitivity, selectivity, signal-to-noise ratio and bias. Despite the low selectivity (maximum of 0.12%), the models presented high sensitivity [γ?1 = 0.19 (mg L?1)?1], low LOQ (1 mg L?1) and correlation between reference and predicted values (r) at least 0.93, except for propanoic acid (rpred = 0.85). The F-test revealed that the selection of variables by GA significantly improved the accuracy and linearity of the prediction models for methanol, acetic acid, isocaproic acid and VFA. NIR spectroscopy has proved to be a powerful tool for monitoring H2 production bioreactors since provides fast, low cost and multicomponent information. 相似文献
9.
L. M. Atayde P. P. Cortez T. Pereira P. A. S. Armada-da-Silva A. Afonso M. A. Lopes J. D. Santos A. C. Maurício 《Journal of materials science. Materials in medicine》2014,25(8):1885-1901
Presently, several bone graft substitutes are being developed or already available for clinical use. However, the limited number of clinical and in vivo trials for direct comparison between these products may complicate this choice. One of the main reasons for this scarcity it is the use of models that do not readily allow the direct comparison of multiple bone graft substitutes, due especially to the small number of implantation sites. Although sheep cancellous bone models are now well established for these purposes, the limited availability of cancellous bone makes it difficult to find multiple comparable sites within a same animal. These limitations can be overcome by the monocortical model here proposed as it consists in 5–6 holes (5 mm Ø), in the femoral diaphysis, with similar bone structure, overlying soft tissue and loading pattern for all defects. Associated to this model, it is also described a fast histomorphometric analysis method using a computer image segmentation test (Threshold method) to assess bone regeneration parameters. The information compiled through the experimental use of 45 sheep in several studies allowed determining that this ovine model has the potential to demonstrate differences in bone-forming performance between various scaffolds. Additionally, the described histomorphometric method is fast, accurate and reproducible. 相似文献
10.
Maurício L. Sforça Inez V. P. Yoshida Cristiano P. Borges Suzana P. Nunes 《应用聚合物科学杂志》2001,82(1):178-185
Hybrid materials were prepared incorporating silica networks by the sol–gel process into the poly(amide-b-polyether) block copolymer PEBAX®. PEBAX®/silica hybrids were characterized by transmission electron microscopy, atomic force microscopy, differential scanning calorimetry, and X-ray diffraction. The pervaporation of phenol from dilute aqueous solutions through hybrid membranes was investigated. Films prepared with lower silica contents showed better dispersed inorganic networks and were more selective in the pervaporation of phenol/water solutions. Films prepared with higher silica contents had a clear phase-separated morphology with lower performance in pervaporation. © 2001 John Wiley & Sons, Inc. J Appl Polym Sci 82: 178–185, 2001 相似文献