Mechanical properties and wear behavior of Tin+1(Al,A)Cn (A = Ga,In, Sn,n = 1, 2) via quasi-high-entropy of single atomic thick A layer

The strengthening method of multi-element M-site solid solution is a common approach to improve mechanical properties of MAX phase ceramic. However, the research on capability of multi-element A-site solid solution to improve mechanical properties has rarely been reported. Thereupon, quasi-high-entropy MAX phase ceramic bulks of Ti₂(Al_1?xA_x)C and Ti₃(Al_1?xA_x)C₂ (A = Ga, In, Sn, x = 0.2, 0.3, 0.4) were successfully synthesized by in situ vacuum hot pressing via multi-elements solid solution. The multi-elements solid solution in single-atom thick A layer was confirmed by X-ray diffraction and X-ray photoelectron spectroscopy as well as by energy dispersive X-ray spectroscopy mappings. Effects of doped multi-elements contents on the phase, microstructure, mechanical properties, and high temperature tribological behaviors were studied. Results demonstrated that the Vickers hardness, anisotropic flexural strength, fracture toughness, and tribological properties of Ti–Al–C based MAX ceramics could be remarkably improved by constitution of quasi-high-entropy MAX phase in A layers. Moreover, the strengthening and wear mechanisms were also discussed in detail. This method of multi-element solid solution at A-site provides new way to enhance mechanical properties of other MAX phase ceramics.     

Fabrication of crescent-shaped ceramic microparticles based on single emulsion microfluidics

Ceramic microparticles have great potentials in various fields such as materials engineering, biotechnology, microelectromechanical systems, etc. Morphology of the microparticle performs an important role on their application. To date, it remains difficult to find an effective and controllable way for fabricating nonspherical ceramic microparticles with 3D features. This work demonstrates a method that combines UV light lithography and single emulsion opaque-droplet-templated microfluidic molding to prepare the crescent-shaped ceramic microparticles. By tailoring the intensity of UV light and flow rate of fluid, the shapes of microparticles are accordingly tuned. Therefore, varieties of crescent-shaped microparticles and their variations have been fabricated. After sintering, the crescent-shaped alumina ceramic microparticles were obtained. Benefitting from the light absorption and scattering behavior of most ceramic nanoparticles, this system can serve as a general platform to produce crescent-shaped microparticles made from different materials, and hold great potentials for applications in microrobotics, structural materials in MEMS, and biotechnology.     

Fluoride-mediately solvothermal synthesis and tunable photocatalytic selectivity of urchin-like ZrO2 hollow microspheres

Photocatalysts often show excellent performances on the basis of their surface state of exposed faces with high reactivity, but unfortunately surfaces of this type are usually concealed into the interior of crystals for their high surface energy. We report here a possibility that for fluorine-terminated surfaces of monoclinic ZrO₂, these higher-energy surfaces could be retained and exposed. Urchin-like ZrO₂ hollow microspheres (UZHS) composed of nanoribbons with exposed (010) facets are obtained through a fluoride mediately solvothermal method. We prove the stabilization effect of fluorine adsorption on (010) facets by density functional theory calculations. More interestingly, UZHS exhibit tunable photocatalytic selectivity in dye degradation. The fluorinated UZHS exhibit good performances both on decomposing Congo red (CR) and methylene blue, while the surface-modified UZHS by calcination only favor decomposition of CR.     

紫色马铃薯酒发酵工艺优化及主发酵期花青素与色泽的动态变化

以紫色马铃薯为原料，在单因素的基础上，通过响应面法对紫色马铃薯酒的发酵工艺参数进行优化。最佳发酵工艺参数为:马铃薯与面粉比1:0.6、料水比1:1 (g/mL)、α-淀粉酶添加量8.5 U/g、酒曲添加量0.45%。此工艺在28 ℃下发酵14 d，得到的紫色马铃薯酒酒精度13.5%vol，花青素含量166.34 mg/mL，酒体澄清透明呈紫红色，酸甜适中，有独特酒香，综合感官评定得分90分。测定主发酵期花青素和色泽的动态变化，分析表明，紫色马铃薯酒在发酵过程中花青素呈现先上升后下降的趋势，色度呈现先下降后趋于平缓的趋势，色调则与之相反。聚合色度和褐变指数总体均呈现逐渐上升的趋势。试验结果为工业化生产紫色马铃薯酒提供理论依据。     

认同度修正下的近相邻改进推荐算法研究

如何融合多方因素准确地为用户提供个性化产品一直是关注的热点问题，由此，一个新的近相邻改进算法融入了大众化认同度和个性化认同度，利于更加高效地挖掘隐藏信息。实验结果表明，相对于传统近相邻算法，认同度修正算法虽然查全率小幅度上下波动，但其他多个评价指标都得到极大提升，假正率和深度有所减少，查准率、[F1]值和提升度得以增加，并且，受试者特征曲线和提升曲线也都说明此修正算法具有更为显著的推荐效果。     

Bio-inspired power control and channel allocation for cellular networks with D2D communications

With the tremendous increment of traffic in the next generation mobile networks, device to device (D2D) communication is proposed to relieve the traffic burden of the base station and improve the overall network capacity. It supports direct communications between devices and could reuse the resources of cellular users (CUs). Despite the advantages, D2D communications bring great challenges in interference management. In this paper, we study the power control and channel allocation problems in three scenarios: (1) one CU and one D2D pair; (2) one CU and multiple D2D pairs; (3) multiple CUs and multiple D2D pairs. The goal is to coordinate the mutual interferences and maximize the overall network capacity. We derive sufficient conditions to guarantee the efficiency of D2D communications in scenarios with one CU and one D2D pair. We propose the bio-inspired PSO-P power control algorithm for the scenarios with one CU and multiple D2D pairs, and the PSO-CP algorithm for the scenarios with multiple CUs and multiple D2D pairs to jointly assign channels and powers. Simulation results show that the proposed algorithms are efficient in improving the overall network capacity.

     

基于同轴图像传感的激光焊接过程质量监测技术

针对激光焊接过程中由于参数不匹配、装配误差等原因造成的焊接过程不稳定等焊接缺陷，基于同轴图像传感技术，建立起一套激光焊接过程中的质量在线监测系统，对焊接过程中的熔池图像进行了采集分析及其熔池特征信息的提取. 结果表明，在激光功率为1 500 W的不等厚不锈钢薄板激光焊接试验条件下，焊接过程中的不稳定、下塌缺陷以及焊偏现象与熔池形状各特征信息变化具有一定的相关性. 结合BP神经网络算法对所提特征信息进行分类、识别，基于LabVIEW软件平台，可实现相应缺陷的自动化识别及报警功能.     

核电厂聚乙烯管道设计方法及标准简介

随着聚乙烯管道在三门核电厂、大亚湾核电厂中的试应用成功，大量的新建核电厂及核电厂改造项目均将聚乙烯管道作为海水冷却水管道系统的首选管材，自主研制核电厂聚乙烯管技术标准迫在眉睫。本文介绍了核电聚乙烯管道的发展历史和应用现状，对比了核安全3级聚乙烯管道和非核安全相关聚乙烯管道、城市燃气与给水聚乙烯管道技术标准的设计方法及适用范围，探讨了中国目前聚乙烯管技术标准与核3级聚乙烯管道技术标准的差异与差距，为核电厂聚乙烯管道的设计制造与标准研制提供参考。     

支撑柱缺位对弧面钢化真空玻璃支撑应力的影响

根据弹性力学、柱壳理论及数学微分法建立了弧面钢化真空玻璃力学模型,基于ANSYS有限元数值分析模拟,分析了3 mm厚弧面钢化玻璃基板不同部位支撑柱缺位对弧面钢化真空玻璃的支撑应力和弯曲变形的影响.研究结果表明,支撑柱缺位对其周围支撑应力影响较大.在中间和角落部位,当支撑柱连续缺位数量超过2个,最大应力为117.77 MPa,最大变形量为0.566 mm;在边缘部位,当支撑柱连续缺位数量超过3个,最大应力为96.183 MPa,最大变形量为0.217 mm,均超过安全允许范围.该研究对弧面钢化真空玻璃的质量检测具有指导意义.     

面向过程装备工程师培养的O2O课程体系构建

过程装备与控制工程专业的人才培养方案及课程体系可以划分为线上和线下两块。线上课程侧重于新知识传授,有助于学生开阔眼界,活跃思维,启迪智慧;线下课程侧重于基本知识传授,有助于学生夯实专业基础,培养专业素养,锻炼工程技能。研究线上和线下课程的主辅关系及交互模式,形成具有鲜明流程工业装备特征的“线上+线下”一体化课程群,建立培养效果(达成度)的评价方法与持续改进机制,有利于培养掌握综合知识、善于设计计算、了解制造检验的优秀过程装备工程师。