Recent advances in isotropic conductive adhesives for electronics packaging applications

Isotropic conductive adhesives (ICAs) have recently received a lot of focus and attention from the researchers in electronics industry as a potential substitute to lead-bearing solders. Numerous studies have shown that ICAs possess many advantages over conventional soldering such as environmental friendliness, finer pitch printing, lower temperature processing and more flexible and simpler processing. However, complete replacement of soldering by ICAs is yet not possible owing to several limitations of ICAs which are mainly related to reliability aspects like limited impact resistance, unstable contact resistance, low adhesion and conductivity etc. Continued efforts for last 15 years have resulted in development of ICAs with improved properties. This review article is aimed at providing a better understanding of ICAs, their principles, performance and significant research and development work addressing the technological utility of ICAs.     

酚醛树脂-CarboresP结合镁碳材料的性能与应用

研究了环境友好型含碳材料CarboresP在镁碳砖中的应用。采用MT14A镁碳砖生产工艺,改变CarboresP的加入量,对试样180℃处理后的体积密度、高温抗折强度(1400℃),以及1000℃埋炭处理后的显气孔率、耐压强度等指标进行了研究和对比,确定镁碳砖中合适的CarboresP添加量为1%,并且可适量降低金属防氧化剂的加入量;分析了酚醛树脂-CarboresP结合炭的显微结构,表明其为均质炭和非均质石墨化炭的混合结构,这将有助于改善炭化结构的抗氧化性能;采用尖劈试验绘制镁碳砖试样的应力-应变曲线,表明添加CarboresP的镁碳砖的特征长度LCH值得到明显提高,说明它具有很好的韧性和吸收应力的能力;与传统工艺生产的MT14A镁碳砖相比较,采用酚醛树脂-CarboresP“软性结合”工艺生产的MT14A镁碳砖,成型性能及热处理后各项性能指标均得到改善,在国内某40tLF-VD精炼钢包渣线上进行现场使用证明,平均使用寿命比现用渣线镁碳砖提高18.4%。     

Combined damaged elasticity and creep modeling of ceramics with wedge splitting tests

During the crack propagation in common refractory ceramics at high temperatures, creep may occur in the wake of a process zone and in front of a crack tip. To account for this phenomenon, an integrated material constitutive model was developed by combining the mechanical behavior following isotropic damaged elasticity concept and Norton-Bailey creep. The post peak fracture behavior followed the bilinear softening law and a simple criterion was defined to consider the creep asymmetricity in uniaxial tension and compression. The material constitutive model was applied to inversely identify mode I fracture parameters with wedge splitting tests of an alumina spinel material at 1200 °C. It showed that the mean ratio of the nominal notch tensile strength to the actual tensile strength was 1.93 and the mean pure fracture energy was 297.6 N/m. In addition, the creep contributed 12.9% on average into the total fracture energy.     

On the calibration of cohesive parameters for refractories from notch opening displacements in wedge splitting tests

Cohesive elements are commonly used to describe crack propagation in heterogeneous materials with toughening mechanisms. This work aims to provide a guideline on how these fracture parameters can be calibrated using notch opening displacements (NODs) measured via digital image correlation and force data from wedge splitting tests (WSTs). Weighted finite element model updating was applied to calibrate material and boundary condition parameters in the same framework. The influence of each parameter on force and NOD data are given together with uncertainties for the calibrated parameters. Numerical results were in very good agreement in terms of splitting force, NOD, displacement and gray level residual fields. It is shown that images obtained during WSTs focusing on the crack path (i.e., hiding the loading region) can be used to drive numerical simulations and obtain cohesive parameters.     

Cu丝超声球焊及楔焊焊点可靠性及失效机理研究

Cu丝由于具有优良的导热性能、机械性能以及低成本等优点使得用铜丝替代传统的Au丝和Al丝已经成为半导体工艺发展的必然方向.综述了Cu丝超声球焊以及楔焊焊点可靠性问题,对焊点的各种失效模式与机理进行探讨.     

铁道车辆用车轴成形方法现状与研究

铁道车辆用车轴是火车传动部分的重要部件,探寻车轴高效、精密成形方法具有重要的应用价值。对目前国内外火车车轴成形技术的现状进行较详细论述,分析各种火车轴成形方法的优劣,指出多楔楔横轧精密成形技术生产火车轴将是今后火车轴成形的主流。     

Effect of particle grading on fracture behavior and thermal shock resistance of MgO-C refractories

Two types of MgO-C refractories with tight particle grading and non-tight particle grading were prepared according to Andreasen's continuous packing theory. Fracture behaviors were investigated using wedge splitting tests combined with digital image correlation method and acoustic emission techniques. The results indicated that MgO-C refractory with non-tight particle grading treated at 1400 ℃ had more in situ phases (e.g., AlN and MgAl₂O₄) and exhibited less brittleness than specimens with tight particle grading even though they had similar nominal tensile strengths. In contrast, specimens with non-tight particle grading had greater horizontal strain under various loading stages, reflecting their better ability to resist rupture deformation. In addition, more microcracks were initiated earlier in the pre-peak region, and more energy was consumed. The decrease in coarse particles and corresponding increase in fine powder content increased the interface between particles, benefiting for reducing the local stress concentration and improving the thermal shock resistance of refractories.     

An experimental research on the rock cutting process of the gage cutters for rock tunnel boring machine (TBM)

This paper proposed an experimental method to investigate the rock cutting process of TBM gage cutters based on the full-scale rotary cutting machine (RCM). The key point of this method is to reconstruct the RCM by inserting three wedges with angles of 10°, 20° and 30° respectively into the space between the cutter base and cutter box. As a result, the rock cutting process of gage cutters with tilt angles of 10°, 20° and 30° can be proceed. Using this method, rock cutting experiments were conducted with penetrations of 2 mm, 4 mm, 6 mm and 8 mm respectively. The testing results were analysed on the rock cutting force, rock debris dimension, specific energy and cutting surface profile, and it was found that: (1) the cutting forces and specific energy of the gage cutter were lower than those of the normal cutter respectively; and (2) the depth of the rock broken zone was smaller than the cutting depth. The testing results can also be used to validate corresponding numerical models and design the layout of gage cutters.     

Critical and Subcritical Adhesion Measurements of a Model Epoxy Coating Exposed to Moisture Using the Shaft-Loaded Blister Test

The shaft-loaded blister test (SLBT) was used to investigate the adhesion between a model epoxy coating and a silicon oxide surface as a function of relative humidity. Critical and subcritical strain energy release rates were measured using specimens that incorporate reinforcing layers of Kapton® film. A simplified procedure that eliminates the need for video imaging to measure the blister radius and fracture energy was developed. A critical relative humidity level for adhesion loss was observed, in agreement with measurements that have been made previously in a number of polymeric systems. The SLBT was confirmed to be particularly attractive for fracture energy measurements on thin, strongly adhered coatings and films which otherwise tend to be problematic.     

A cellular finite element model for the cutting of softwood across the grain

In this paper, the mechanics of cutting wood across the grain are reexamined. A hybrid cellular/macroscopic finite element model of wood was developed to simulate the effects of cell collapse during the cutting process. Initially, the model was used to simulate the compression test across the grain. The linear elastic and cell collapse behaviours of the compression tests were sucessfully simulated. The model was then used to simulate two orthogonal cutting processes, wedge cutting and chip-forming cutting. The cellular/macroscopic model revealed that during the cutting process, the load compresses the wood until cell wall buckling occurs ahead of the tool. The collapse of the supporting cell wall results in a localized tensile stress in the longitudinal direction of the cell at the tip of the tool. It is postulated that this longitudinal tensile stress would lead to microfibrils being pulled out of the matrix and hence to failure of the cell wall. Therefore, the cellular/macroscopic model has been used to explain the mechanics of severing wood fibres during the process of cutting wood across the grain.