Prediction of Flooding in Packed Liquid-Liquid and High-Pressure Extraction Columns Using a Gaussian Process

Reliable prediction of flooding conditions is needed for sizing and operating packed extraction columns. Due to the complex interplay of physicochemical properties, operational parameters and the packing-specific properties, it is challenging to develop accurate semi-empirical or rigorous models with a high validity range. State of the art models may therefore fail to predict flooding accurately. To overcome this problem, a data-driven model based on Gaussian processes is developed to predict flooding for packed liquid-liquid and high-pressure extraction columns. The optimized Gaussian process for the liquid-liquid extraction column results in an average absolute relative error (AARE) of 15.23 %, whereas the algorithm for the high-pressure extraction column results in an AARE of 13.68 %. Both algorithms can predict flooding curves for different packing geometries and chemical systems precisely.     

Headspace fingerprinting approach to identify the major pathway influencing volatile patterns of vinasse-cured duck processed by high pressure,as well as its impact on physicochemical and sensory attributes

As a decisive attribute, flavour could be influenced by HP treatments through multiple physical and chemical pathways within the high pressure (HP)-assisted meat curing process. This investigation aimed to identify the major pathway influencing volatile flavour patterns of two representative vinasse-cured duck (VCD) products with HP treatments (150–300 MPa/15 min), including wet and dry types, by employing headspace fingerprinting as an untargeted approach. Results suggested that HP treatments greatly lowered moisture contents and increased Warner-Bratzler shear force and thiobarbituric acid reactive substances of the cured samples. According to multivariate models, the volatile flavour patterns of the HP-processed VCD could be clearly separated from the unprocessed samples, but the VCD pressurised at different intensities represented similar volatile fingerprinting, which was validated by e-nose analysis. The discriminant analysis (OPLS-DA) model outlined vinasse-derived ethanol, acetic acid, 3-methyl-1-butanol, 2-methyl-1-butanol, phenethyl alcohol and 2-methyl-3-octanone as the major discriminant aromas across the unpressurised and pressurised samples.     

动态高压微射流处理对方竹笋膳食纤维理化及结构特性的影响

以方竹笋中提取的膳食纤维为研究对象，采用动态高压微射流（dynamic high-pressure micro-fluidization, DHPM）在不同压力条件（0，50，100，150，200 MPa）下进行处理，探究其对竹笋膳食纤维（bamboo shoots dietary fiber, BSDF）理化和结构特性的影响。结果表明，随着处理压力的增大，BSDF粒径先增大后减小，当处理压力为150 MPa时，粒径最小，为（370±11） nm，此条件下BSDF的持水力、持油力和膨胀力达到最大，较对照组分别提高了47.74%，50.54%，61.27%，且差异显著（P<0.05）。红外光谱分析表明DHPM处理不会改变BSDF的官能团，但会使BSDF内部的部分氢键断裂和半纤维素、木质素等发生降解；X射线衍射和热重分析表明DHPM处理不会引起BSDF的晶体结构改变，但晶体有序度会下降，进而导致其热稳定性降低；微观结构分析显示DHPM处理会使BSDF颗粒尺寸减小、表面粗糙、组织松散，且当处理压力为200 MPa时，颗粒发生团聚。综上，DHPM可以有效改善BSDF的理化性质，在膳食纤维改性方面具有一定的应用价值。     

Incoloy825材料在加氢裂化装置高压空冷器上的应用

对Incoloy825材料的焊接和抗腐蚀性能,以及在加氢裂化装置高压空冷器上的应用中应注意的问题进行了探讨.对此种空冷器在制造中如何解决异种钢焊接的难题,在清洗和水压试验中如何避免腐蚀等提出了建议.     

东营凹陷王庄-宁海地区流体包裹体分析与流体充注研究

利用流体包裹体分析技术，系统地分析了东营凹陷王庄-宁海地区覆盖所有含油层位的流体包裹体样品。包裹体荧光观察和均一温度特征分析揭示了包裹体发育期次为5期，说明该区油藏存在5次流体充注过程；据此确定了备期烃类的成藏期次。东营组沉积时期和明化镇组沉积末期的油气运聚均在成藏后遭受大气淡水淋滤和降解作用。沙三段原油可能经历至少2期稠油化作用。荧光观察进一步证实该区主要发生2期充注、2期成藏。     

高压加热器技术简介

介绍了东芝高压加热器技术以及技术转让的一些内容 ,以及为能制造出符合东芝技术要求的高压加热器而采取的保证措施     

高压水射流技术粉碎原盐的研究

以原盐为被粉碎研究对象,通过对高压水射流粉碎原盐形貌的观察和成分分析、高压水射流原盐粉碎性能分析,以及高压水射流粉碎原盐各影响因素的正交分析,研究表明高压水射流粉碎技术对原盐具有良好的解理性且粉碎效率高、耗能低。各因素对原盐粉碎效果的影响顺序为:射流压力卤水喷嘴直径、料液混合喷嘴直径、靶面形状。     

如何延长高压液相色谱柱的使用寿命

分析了液相色谱柱失效的诸多现象和原因，并论述了极性溶剂冲洗法等一些使色谱柱恢复活性的方法。     

On the mechanical behavior of aluminum alloys reinforced by long or short alumina fibers or SiC whiskers

This study was initiated to examine the dispersion of longitudinal and transverse waves in metal matrix composites in order to obtain the dynamic elastic modulus and to evaluate various models for predicting the composite's macroscopic elastic constants from the properties of its constituents. The materials chosen for this investigation were alumina continuous fibers on the one hand and alumina and SiC short fibers on the other hand, all embedded in an aluminum alloy matrix. In addition, some indications have been obtained experimentally for the acoustoelastic effect in the composite.