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Marcus Heinze Sandra Starke Marcel Händler Hartmut Komber Marco Drache Norbert Moszner Brigitte Voit Doris Pospiech 《应用聚合物科学杂志》2019,136(48):48256
We demonstrate in this study that the combination of modern inline monitoring methods [here: inline nuclear magnetic resonance (NMR)] with simulations gains more exact and profound kinetic results than previously used methods like linearization without that combination. The 1H-NMR spectroscopic data (more than 100 data points) are used to construct the copolymerization diagram. The reactivity ratios are obtained applying the van Herks nonlinear least square method. The examination of the radical copolymerization of 2-hydroxyethyl methacrylate (HEMA) with (2-{[2-(ethoxycarbonyl)prop-2-en-1-yl]oxy}ethyl) phosphonic acid (ECPPA) as important adhesive monomer used in dentistry yields reactivity ratios of rHEMA = 1.83; rECPPA = 0.42. The copolymerization diagram reflects nonideal, non-azeotropic copolymerization. The sequence distribution of the obtained by Monte Carlo simulation indicates the generation of statistical copolymers. As an important finding, it is demonstrated that the repeating units responsible for etching and adhesion are arranged over the whole polymer chain, which is necessary to achieve proper functionality. © 2019 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2019 , 136, 48256. 相似文献
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Multiphase flow in mini/micro channels has been widely studied for its potential in many industrial applications. The normal experimental method cannot capture two separate regions of interest (ROI) with a long distance synchronously for the limited field of views. In order to solve this problem, an improved experimental method is proposed and validated with experimental results. Prism groups are applied to reflect the two regions of interest to a very small shooting zone. Though the actual distance between the two regions is far, the reflected regions adjoin with each other on the top surface of the prisms. Thus, the two regions can be captured synchronously with one image using a small field of view. Two types of configurations with 4 prisms and 6 prisms are compared using gas-liquid and liquid-liquid experimental results. The resolution of the two configurations is similar, while the maximum amplification ratio is smaller for the latter configuration with 6 prisms. The first type is more suitable for experimental studies focusing on the formation and breakup of dispersed phases near two branches. The second configuration is recommended for cases focusing on the formation and fully developed hydraulic characteristics of the dispersed phase. The proposed method is very efficient for studies of hydraulic, heat and mass transfer characteristics of multiphase flows in mini/micro channels. 相似文献
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Jinho Choi Sanghun Jung Deok Gun Park Jaegul Choo Niklas Elmqvist 《Computer Graphics Forum》2019,38(3):249-260
The majority of visualizations on the web are still stored as raster images, making them inaccessible to visually impaired users. We propose a deep‐neural‐network‐based approach that automatically recognizes key elements in a visualization, including a visualization type, graphical elements, labels, legends, and most importantly, the original data conveyed in the visualization. We leverage such extracted information to provide visually impaired people with the reading of the extracted information. Based on interviews with visually impaired users, we built a Google Chrome extension designed to work with screen reader software to automatically decode charts on a webpage using our pipeline. We compared the performance of the back‐end algorithm with existing methods and evaluated the utility using qualitative feedback from visually impaired users. 相似文献
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No authorship indicated 《Canadian Metallurgical Quarterly》2004,59(8):673
Provides the biography of Sheldon Cohen and announces that he has received the APA Award for Distinguished Scientific Contributions (2004) for his elegant research in psychoneuroimmunology. The award citation and a selected bibliography are also provided. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
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报导了新型鞣剂 7-羟基全氢化唑并嗪 (以下简称 OX- Z)的合成方法。试验确定合成的最佳条件为 :在氮气保护下 ,将等摩尔量的二乙醇胺在 10℃水浴中缓慢滴入乙二醛中 ,滴加时间 0 .5 h,在 2 0℃水浴中继续反应 1.5 h,产率为 6 2 .9%。 OX- Z对浸酸绵羊皮单独鞣制 ,可使收缩温度升高到 87℃。最佳鞣制条件为 :p H10 .0 ,OX- Z用量 5 % ,鞣制时间 8h。在对 OX- Z与皮胶原的结合类型的研究中证明它们之间是以化学键结合的。 相似文献
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简单介绍了碳氧比测井的原理及通常的数据处理方法。分析了由常规数据处理所得曲线仍然存在的问题及可能的成因 ,并给出了可行的修正办法。讨论了另一种可行的曲线异常数据的检测、剔除方法。实践表明 :文章讨论的两点建议都是可行的 ,并且在提高测量曲线质量的同时也提高了地层含油饱和度的解释精度。 相似文献
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Poly[2‐methoxy‐5‐(2′‐ethyl‐hexyloxy)‐para‐phenylene vinylene] (MEH‐PPV)/silica nanoparticle hybrid films were prepared and characterised. Three kinds of materials were compared: parent MEH‐PPV, MEH‐PPV/silica (hybrid A films), and MEH‐PPV/coupling agent MSMA/silica (hybrid B films), in which MSMA is 3‐(trimethoxysilyl) propyl methacrylate. It was found that the hybrid B films could significantly prevent macrophase separation, as evidenced by scanning electron and fluorescence microscopy. Furthermore, the thermal characteristics of the hybrid films were largely improved in comparison with the parent MEH‐PPV. The UV‐visible absorption spectra suggested that the incorporation of MSMA‐modified silica into MEH‐PPV could confine the polymer chain between nanoparticles and thus increase the conjugation length. The photoluminescence (PL) studies also indicated enhancement of the PL intensity and quantum efficiency by incorporating just 2 wt% of MSMA‐modified silica into MEH‐PPV. However, hybrid A films did not show such enhancement of optoelectronic properties as the hybrid B films. The present study suggests the importance of the interface between the luminescent organic polymers and the inorganic silica on morphology and optoelectronic properties. Copyright © 2004 Society of Chemical Industry 相似文献