Superconductivity in nearly single-phase Bi-Pb-Sr-Ca-Cu-O samples with different nominal compositions

The preparation conditions, phase composition, and superconducting properties of Bi-Pb-Sr-Ca-Cu oxide materials from different nominal compositions have been investigated. Nearly single-phase samples from Bi₂Pb_0.4Sr₂Ca₃Cu₄O _y , as well as from the proposed compositions Bi_1.8Pb_0.4Sr₂Ca₃Cu₄O _y and Bi_1.8Pb_0.4Sr₂Ca_2.5Cu_3.5O _y were obtained by a solid-state reaction in air. Samples with the third nominal composition showed the best superconducting properties (T _on=111 K and zero resistance atT ₀=103 K). A possible mechanism for the 2223 phase formation in the three investigated compositions has been discussed.     

Al-Cu-Fe QUASICRYSTALLINE PHASE FORMATION BY MECHANICAL ALLOYING

Al-Cu-Fe alloys were prepared from elemental powders in a high-energy planetary ball mill. A sequence of solid state reactions resulting in quasicrystal (QC) phase formation takes place during heating of the as-milled powder. These reactions were studied by both differential scanning calorimetry and x-ray diffraction methods. Mechanically alloyed powders were consolidated by cold and hot pressing, as well as by explosive compaction. After annealing at sufficiently high temperatures, the consolidated samples are single-phase QC, except the ones consolidated by explosion. The high reactivity of the as-milled alloys causes the appearance of high porosity of the consolidated samples after the annealing.     

硫脲型整合树脂在分析上的应用 Ⅰ.岩样中微量银的中子活化分析

前言银和其他贵金属元素一样,在地壳中比较稀少,按其自然丰度为第67号元素,平均含量仅0.07 ppm。由于地质样品成分非常复杂,为测定其微量银,必须进行严格的化学分离。但是迄今文献中报道的许多分离分法,步骤都相当冗长,一般采用氯化银反     

Are Samples in Randomized Controlled Trials of Psychotherapy Representative of Community Outpatients? A New Methodology and Initial Findings.

To determine the extent to which published randomized controlled trials (RCTs) of psychotherapy can be generalized to a sample of community outpatients, the authors used a method of matching information obtained from outpatient charts to inclusion and exclusion criteria from published RCT studies. They found that 80% of the patients in their sample who had diagnoses represented in the RCT literature were judged eligible for at least 1 published RCT; however, 58% of the patients had primary diagnoses such as adjustment disorder or dysthymia, which were not represented in the existing psychotherapy outcome literature. The most common reasons that patients in their sample did not match with published RCTs for psychotherapy are listed, and the implications of these findings for research and practice are discussed. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

EASY2000色谱处理系统在酒样色谱分析中的运用

介绍了EASY2000色谱处理系统在酒类产品分析实际应用过程中的方法，步骤，特点及注意事项等。     

Microplastic and other anthropogenic microparticles in water and sediments of Lake Simcoe

Microplastics (plastic particles <5 mm in size) have been reported in ecosystems worldwide and have been shown to cause adverse negative impacts on organisms. This study provides the first report of microplastics and other anthropogenic microparticles in the surface waters and sediments of Lake Simcoe in Ontario, Canada, a popular recreational and fishing lake. Surface waters (low volume grabs and manta trawls) and sediments were sampled from eight sites to determine microparticle abundances and character (size, morphology, material identity). Concentrations ranged from 0 to 0.7 particles/L in surface water grab samples, 0.4–1.3 particles/m³ in manta trawl samples, and 8.3–1070 particles/kg in sediment samples. Spectroscopic analysis confirmed that 72% of particles were anthropogenic, with 64% unambiguously identified as microplastics. However, confirmed microplastic concentrations were approximately 6–7 times lower than unadjusted counts in sediments, demonstrating the importance of verifying and adjusting reported values. Fibers were only quantified and characterized in surface water grab samples and sediments, and were the most common morphology, accounting for 82% and 89% of anthropogenic particles, respectively. Fragments were most common in manta trawl samples (75%, excluding fibers) and consisted predominantly of polyethylene (41%) and polypropylene (22%). The influence of proximity to urban centers and prevailing winds on the distribution of microplastics was apparent in surface water manta trawls. Microplastics and other anthropogenic microparticles are present in Lake Simcoe but at lower abundances than at locations impacted by larger population centers in other large freshwater lakes such as Lakes Ontario and Erie of the Great Lakes.     

多系列铸铁光电发射光谱标准样品的研制

采用中频炉熔炼，用自行设计的多孔隔离式金属型和独特的补缩和浇注系统及临界激冷工艺进行浇铸，成功地研制出了带有高低标的铸铁系列多元素光电光谱分析标样。对标样的白口化程度、均匀性、呈线性分布及分析精度等进行了检测并得出可行性结论。     

不平衡样本下基于变分自编码器预处理深度学习和DGA的变压器故障诊断方法

为提高变压器故障诊断效果,并改善训练样本数量不平衡对故障诊断的不利影响,提出了一种基于变分自编码预处理深度学习和油中溶解气体分析(dissolved gas-in-oil analysis,DGA)的变压器故障诊断方法。该方法以各样本DGA特征量为诊断模型输入,以各故障状态概率分布为诊断模型输出。首先通过变分自编码器对少数类训练样本进行预处理,在学习确定少数类训练样本分布特征的基础上实现训练样本自动生成,进而提高训练样本的均衡性。基于3隐层结构堆栈稀疏自编码器深度学习网络构建变压器故障诊断模型,并以经变分自编码器预处理后的均衡训练样本对诊断模型参数进行更新优化。基于实例验证了所提方法的有效性。实验结果表明,所提方法可改善训练样本不平衡的不利影响,各训练集下,采用所提方法的变压器故障诊断结果准确率均保持在91%以上,且漏报率较低。     

基于相似样本和多模型动态最优组合的光伏功率预测

针对传统单一预测方法存在的局限性,引入了考虑特征加权的模糊聚类方法,进行关于天气类型的划分以得到相似样本;提出多模型动态最优组合预测方法,根据各窗口期预测误差的波动情况,设置合适的临近历史样本窗口宽度,利用窗口期中的数据和构建的最优赋权模型进行组合权重的求解,在避免单一预测方法片面性的同时,提高了对各种天气的适应性。通过算例验证分析表明,所提出的组合预测方法在各种天气类型下的预测效果都优于理论预测、BP预测和LSSVM预测等单一预测方法,能够有效提高预测的有效性和准确性,具有较高的工程实用价值。