| 高氯酸铵中草酸铵含量的分析 |
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| 引用本文： | 李军峰,曾建红,姚齐春.高氯酸铵中草酸铵含量的分析[J].化学推进剂与高分子材料,2010,8(5):61-64. |
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| 作者姓名： | 李军峰 曾建红 姚齐春 |
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| 作者单位： | 黎明化工研究院,河南洛阳,471000 |
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| 摘 要： | 为了回收利用含草酸铵的高氯酸铵产品,建立了用高锰酸钾测定高氯酸铵溶液中草酸铵含量的分析方法。研究结果和生产应用表明:此分析方法简便、有效、实用,其相对标准偏差为0.49%;在测定过程中和测定温度范围内,溶液中高氯酸铵与草酸铵不发生反应,对分析操作和测定结果没有影响。
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| 关 键 词： | 草酸铵 高氯酸铵 高锰酸钾 测定 含量 |
Analysis of Ammonium Oxalate Content in Ammonium Perchlorate |
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| LI Junfeng,ZENG Jianhong,YAO Qichun.Analysis of Ammonium Oxalate Content in Ammonium Perchlorate[J].Chemical Propellants & Polymeric Materials,2010,8(5):61-64. |
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| Authors: | LI Junfeng ZENG Jianhong YAO Qichun |
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| Affiliation: | (Liming Research Institute of Chemical Industry,Luoyang 471000,China) |
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| Abstract: | To reclaim ammonium perchlorate product containing ammonium oxalate,an analytic method of ammonium oxalate content in ammonium perchlorate solution using potassium permanganate was built.The research results and applications in production show that the method is simple,effective,practical,and its relative standard deviation is 0.49%.During the determining course and in the range of determination temperature,ammonium perchlorate does not react with ammonium oxalate in the solution,has not influence on analysis operation and determining result. |
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| Keywords: | ammonium oxalate ammonium perchlorate potassium permanganate determination content |
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