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Polymer nanoparticles: Preparation techniques and size-control parameters

Authors:	J Prasad RaoKurt E Geckeler

Affiliation:	^a Department of Materials Science and Engineering, Gwangju Institute of Science and Technology (GIST), 1 Oryong-dong, Buk-gu, Gwangju 500-712, South Korea ^b Department of Nanobio Materials and Electronics, World-Class University (WCU), 1 Oryong-dong, Buk-gu, Gwangju 500-712, South Korea

Abstract:

Keywords:	AA acrylic acid AAm acrylamide ACPA 4 4&prime -azobis(4-cyanopentanoic acid) AIBN 2 2&prime -azobisisobutyronitrile AOT sodium bis(2-ethylhexyl) sulfosuccinate AMA-80 sodium dihexyl sulfosuccinate Amphi-Dex amphiphilic derivative of dextran AN acrylonitrile Ani aniline APS ammonium persulfate ASPS alkali soluble polymeric surfactant ATRP atom transfer radical polymerization BA butyl acrylate BCA n-butyl cyanoacrylate BMA butyl methacrylate BPO benzoyl peroxide BPMODA bis(2-pyridylmethyl)-octadecylamine Brij 30 polyoxyethylene-4-lauryl ether [C₄mim]PF₆ 1-butyl-3-methylimidazolium hexafluorophosphate CA897 poly(oxyethylene) octyl phenyl ether CaCl₂ calcium chloride CAN cerium ammonium nitrate CH cyclohexane CH₂Cl₂ methylene chloride C₄H₆O₂ methacrylic acid C/LRP controlled/living radical polymerization CMC-A9 polymeric surfactant based on carboxymethyl cellulose and alkyl poly(etheroxy)acrylate CMPEG carboxymethylated poly(ethylene glycol) CMS chloromethyl styrene CO₂ carbon dioxide CPDB 2-cyanoprop-2-yl dithiobenzoate CTAB cetyltrimethylammonium bromide CTMA-Cl cetyltrimethylammonium chloride CuSO₄ 5H₂O cupric sulfate DDAB didodecyldimethylammonium bromide DDA-HEEE dodecanoic acid 2-(2-hydroxyethoxy)ethyl ester (neutral surfactant) DeTAB decyltrimethylammonioumbromide DDM dodecyl mercaptane DexEst dextran ester DIAMA-Na SG1-based difunctional alkoxyamine DMAc dimethyl acetamide DMA dodecyl methacrylate DMAEMA (dimethylamino)ethyl methacrylate DMF dimethylformamide DMMA-PS 3-(N N-dimethylmyristylammonio) Propanosulfonate (zwitterionic salt) DMSO dimethyl sulfoxide C₁₂H₂₆S dodecyl mercaptane Dowfax 8390 a mixture of mono- and dihexadecyl disulfonated diphenyloxide disodium salts DTAB dodecyltrimethylammonioumbromide C₄H₈O₂ ethyl acetate EBiB ethyl 2-bromoisobutyrate ECNA ethyl cyanoacrylate EG ethylene glycol EUDRAGIT L100-55 methacrylic acid copolymer Type C USP/NF FeCl₃ 6H₂O ferric chloride GMA glycidyl methacrylate HO-EBiB 2-hydroxyethyl 2-bromoisobutyrate H₂O₂ hydrogen peroxide HCl hydrochloric acid HD hexadecane HEMA hydroxylethyl methacrylate HMA hexyl methacrylate IP interfacial polymerization IPDI isophorone diisocyanate K₂CO₃ potassium carbonate KLE3729 poly(ethylene-co-butylene)-b-poly(ethylene oxide) KPS potassium persulfate LMA lauryl methacrylate MAMA SG1-based water-soluble alkoxyamine derived from methacrylic acid (also called BlocBuilder) Mg(CH₃COO)₂· 4H₂O magnesium acetate tetrahydrate MgCl₂ magnesium chloride MgCl₂· 6 H₂O magnesium chloride hexahydrate Miglyol 812 mixture of triglycerides MIM macroinimer MONAMS SG1-based alkoxyamine derived from methyl acrylate mPEG monomethoxy-poly(ethylene glycol) mPEO-PLA monomethoxy-poly(ethylene oxide)-poly(lactic acid) MMA methyl methacrylate MMCO molar mass cut-off NaCl sodium chloride NaHCO₃ sodium bicarbonate Na₂S₂O₃ Sodium Thiosulphate NaSS 4-styrenesulfonic acid sodium salt hydrate (NH₄)₂S₂O₈ ammonium persulfate NMA N-methylolacrylamide NMPy N-methyl-2-pyrrolidone NMP nitroxide-mediated polymerization NPA N-propargylamide NVP N-vinyl pyrrolidone OEOMA oligo(ethylene oxide) monomethyl ether methacrylate OTAB octyl trimethyl ammonium bromide (o/w) oil-in-water PA pullulan acetate PAK-02 photocurable monomer PANI-PSS polyaniline-poly(styrenesulfonic acid) P(B/E-b-EO) poly(butylenes-co-ethylene)-b-poly(ethylene oxide) PBG-PEO l-glutamate)-b-poly(ethylene oxide)" target="_blank">poly(γ-benzyl-l-glutamate)-b-poly(ethylene oxide) PCL poly(?-caprolactum) PDMAAm-TTC poly(N N-dimethylacrylamide)s (PDMAAm) with a reactive trithiocarbonate PE/F68 poly(oxyethylene)-poly(oxypropylene) copolymer PEO poly(ethylene oxide) PEG poly(ethyleneglycol) PHB poly(hydroxyl butyrate) PHDFDA poly(heptadecafluorodecylacrylate) PHEMA poly(hydroxyethyl methacrylate) PLAF poly(lactide-fumarate) PLGA d" target="_blank">poly(d l-lactic acid-co-glycolic acid)" target="_blank">l-lactic acid-co-glycolic acid) PLGF poly(lactide-co-glycolide fumarate) PLLA l-lactic acid)" target="_blank">poly(l-lactic acid) Pluronic F-108 non-ionic surfactant PMA poly(α l-malic acid)" target="_blank">β-l-malic acid) PMMA poly(methyl methacrylate) P(MAA-co-S)-SG1 Macroinitiator SG1 nitroxide-capped poly(methacrylic acid-co-styrene) macroalkoxyamines P(NIPAM-MAA) poly(N-isopropylacrylamide-co-methacrylic acid) Poloxamine 908 poly(ethylene oxide)-poly(propylene oxide) ethylene diamine co-polymer PNP polymer nanoparticles POP Poly(organophosphazene) PSFTE poly[2-(3-thienyl) acetyl-3 3 4 4 5 5 6 6 7 7 8 8 8-tridecafluorooctanoate] PSS poly(styrenesulfonic acid) PTMC poly(trimethylene carbonate) PVA poly(vinyl alcohol) Py pyrrole RAFT reversible addition and fragmentation transfer RESOLV rapid expansion of supercritical solution into liquid solvent RESS rapid expansion of supercritical solution Rh-Catyl rhodium based catalyst SABS sodium 4-(v-acryloyloxyalkyl) oxy benzene sulfonate SDS sodium dodecyl sulfate SEM scanning electron microscopy SG1 (trade name of the Arkema group) N-tert-butyl-N-(1-diethyl-phosphono-2 2-dimethylpropyl) nitroxide SHOA sodium 12-hexinoyloxy-9-octadecenate SLS sodium lauryl sulfate SOBS sodiumoctylbenzene sulfonate SMA stearyl methacrylate SMTAPE 5-sulfoisophthalic acid dimethyl ester sodium salt modified tetracarboxylic acid-terminated polyester Span 40 sorbitan monopalmitate Span 80 sorbitan monooleate Span 85 sorbitane trioleate SPS sodium persulfate St styrene SWNT single-walled carbon nanotube TEM transmission electron microscopy Th thiophene THF tetrahydrofuran TMEDA tetramethylethylenediamine TosDex tosyl dextran TPGS d-α-tocopheryl poly(ethylene glycol)" target="_blank">d-α-tocopheryl poly(ethylene glycol) TPMA tris[(2-pyridyl)methyl]amine Tween 80 non-ionic surfactant VA vinyl acetate VA-044 2 2&prime -azobis[2-(2-imidazolin-2-yl)propane]dihydrochloride V-50 2 2&prime -azobis(2-amidinopropane) dichloride (w/o)/w (water-in-oil)-in-water
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