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基于食用油为连续相的茶多酚反相微乳液的制备
引用本文:陈梦洁,王道源,李志勇,杨迎,吴金鸿,钟耀广,王正武.基于食用油为连续相的茶多酚反相微乳液的制备[J].食品科学,2018,39(6):39-44.
作者姓名:陈梦洁  王道源  李志勇  杨迎  吴金鸿  钟耀广  王正武
作者单位:(1.上海海洋大学食品学院,上海 201306;2.上海交通大学农业与生物学院,上海 200240)
基金项目:“十三五”国家重点研发计划重点专项(2016YFD0400200);国家自然科学基金面上项目(31571763;31671923;31471623)
摘    要:制备油烯基聚氧乙烯(10)醚(polyoxyethylene(10)oleyl ether,Brij97)-单油酸甘油酯(glyceryl monooleate,GMO)-乙醇-食用油-水反相微乳液,成功将抗氧化剂茶多酚添加至食用油中。通过拟三元相图法、动态光散射法和差示扫描量热法研究微乳液的相行为、粒径和抗氧化能力。结果显示,微乳液的最佳配方条件为复合表面活性剂Brij97与GMO质量比2∶8、水相中水与乙醇质量比4∶1。微乳液中茶多酚质量浓度越高,微乳液粒径越小,但多分散指数越大。当水相中茶多酚质量浓度达到0.10 g/m L时,30 d内5种微乳液粒径都稳定在8.00~12.00 nm范围内。差示扫描量热法显示空白大豆油微乳液的起始氧化温度为163.40℃,添加0.01 g/m L茶多酚后为175.77℃,添加0.10 g/m L茶多酚后为210.88℃。

关 键 词:反相微乳液  抗氧化剂  茶多酚  食用油  差示扫描量热法  

Preparation of Tea Polyphenols-Loaded Inverse Microemulsion Using Edible Oil as Continuous Phase
CHEN Mengjie,WANG Daoyuan,LI Zhiyong,YANG Ying,WU Jinhong,ZHONG Yaoguang,WANG Zhengwu.Preparation of Tea Polyphenols-Loaded Inverse Microemulsion Using Edible Oil as Continuous Phase[J].Food Science,2018,39(6):39-44.
Authors:CHEN Mengjie  WANG Daoyuan  LI Zhiyong  YANG Ying  WU Jinhong  ZHONG Yaoguang  WANG Zhengwu
Affiliation:(1. College of Food Science and Technology, Shanghai Ocean University, Shanghai 201306, China; 2. School of Agriculture and Biology, Shanghai Jiaotong University, Shanghai 200240, China)
Abstract:Tea polyphenols-loaded water-in-oil microemulsion (ME) of polyoxyethylene (10) oleyl ether (Brij97)-glyceryl monooleate (GMO)-ethanol-edible oil-water to envelop was prepared successfully in this paper. The phase behavior, particle size, and oxidative stability were investigated by pseudo-ternary phase diagram method, dynamic light scattering (DLS) and differential scanning calorimetry (DSC). The results showed that the optimal mass ratio of Brij97 to GMO was 2:8; the optimal mass ratio of water to ethanol was 4:1. Higher tea polyphenol (TP) concentration resulted in smaller mean particle size and higher polydispersity index of ME system. Moreover, the mean particle size of 5 kinds of ME systems with 0.10 g/mL TP in the aqueous phase remained between 8.00 and 12.00 nm for 30 days. The results of DSC showed that the incipient oxidation temperature of blank soybean oil ME was 163.40 ℃, while those of ME with 0.01 and 0.10 g/mL TP added were 175.77 and 210.88 ℃, respectively.
Keywords:inverse microemulsion  antioxidant  tea polyphenols  edible oil  differential scanning calorimetry  
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