A force modulation study on crystallization process in ferroelectric vinylidene fluoride and trifluoroethylene copolymer films

This paper introduces the Force Modulation technique to the study of crystallization process in ferroelectric vinylidene fluoride and trifluoroethylene copolymer films. Using this technique we have successfully visualized ferroelectric crystalline domains and observed that these ferroelectric domains grow out from amorphous phase, unite into strip-like structures, and finally congregate into a union. Force Modulation can weaken the influence of topography on imaging of ferroelectric domains, and reveal more details, which are difficult to be observed in topographical image.     

陇上天路

如果说青藏铁路是一条“雪域天路”，那么宝鸡至天水高速公路就是一条“陇上天路”。宝鸡至天水是从关中平原到西北黄土高原的跨越地段，垂直跨度大，山连山，岭连岭，几乎看不到任何平原地段。作为2005年西部新开工的十大工程和交通部十二项示范工程之一，这条全长91公里的高速公路还要穿过甘肃屈指可数的林带，跨越黄河、长江两大流域，穿越甘肃最大的天然林保护基地--小陇山林业自然保护区、麦草沟自然保护区和麦积山国家森林公园。     

内嵌闪存MCU的高性能多通道24位采集系统ADuC845

ADuC845是ADI公司新推出的嵌有单指令周期8052闪存MCU、带两路24位∑ -△A/D、双12位D/A以及两个灵活脉宽调制输出的高性能24位数据采集与处理系统芯片。该芯片的数据处理速度达12MIPS,且设计简单 ,噪声低 ,非常适用于精密仪器仪表。文中详细介绍了该芯片的功能特点和工作原理 ,给出了该芯片的应用方法。     

Co^3＋—modified Surface of LiMn2O4 Spinel for its Improvementof Electrochemical Properties

Cobalt was used to modify the surface of spinel LiMn2O4 by a solution technique to produce Co^3 -modified surface material (COMSM). Cobalt was only doped into the surface of LiMn2O4 spinel. XPS(X-ray photoelectron spectroscopy) analysis confirms the valence state of Co^3 . COMSM has stable spinel structure and can prevent active materials from the corrosion of electrolyte. The ICP(inductively coupled plasma) determination of the spinel dissolution in electrolyte showed the content of Mn dissolved from COMSM was smaller than that from the pure spinel. AC impedance patterns show that the charge-transfer resistance (Rct) for COMSM is smaller than that for pure spinel. The particles of COMSM are bigger in size than those of pure spinel according to the micrographs of SEM(scanning electron microscopy). The determinations of the electrochemical characterization show that COMSM has both good cycling performance and high initial capacity of 124.1 mA/h at an average capacity loss of 0.19 mAh/g per cycle.     

当心新的"信息化陷阱"——合理规划、慎重选择"信息化"切入点

信息化巳成为当今的一大热点，文章以客观的角度分析了企业信息化应用的现状，阐述了如何合理规划、选择“信息化”切入点，对待实施信息化的企业具有重要的意义。     

A Study of AlN Films Prepared by Arc Ion Plating

Hexagonal AlN films have been obtained by arc ion plating at different negative biases ,X-ray diffraction and scanning electron microscopy results show that AlN films with smooth surfaces and (002) preferred orientation are obtained at low biases ,whereas those with coarse surfaces and (100) preferred orientation are obtained at high biases,The formation mechanism of AlN is analyzed and the experiment results are discussed,The effect of bias on adhesion strength has also been examined.     

撬装式油井热洗装置研制及应用效果评价

油井热洗是油田最常用的一种清蜡方法。靖安长6油藏是采油三厂的主力油藏,截至2004年底建成油井1064口,由于长6层原油含蜡量高,油井结蜡严重,通常采用常规热洗方法进行油井清蜡。存在以下两方面问题：一是常规油井热洗方法操作比较复杂,运行动力设施多,热洗费用较高；二是常规洗井油源均来自联合站或接转站,为不同层所采的混合原油,进入地层后,会对地层造成一定程度的伤害。为此,我们认真分析了现有油井热洗工艺的不足,查找了油井热洗费用高的影响因素,结合靖安油田长6油藏丰富的伴生气资源,自主研发了撬装式油井热洗装置,经过现场应用取得了较好的效果。     

A-6A甲胺合成催化剂使用总结

安阳九天化工集团甲胺/DMF(二甲基甲酰胺)工程是河南省重点建设项目.装置采用先进的甲醇和液氨气相催化胺化法生产混甲胺.一期工程30 kt/a 甲胺/DMF装置于2003年10月建成投产,其合成催化剂选用的是上海石化研究院生产的A-6A甲胺合成催化剂,从投产到现在,合成催化剂共更换了4次,催化剂平均使用寿命为13个月,共生产混甲胺112 kt,达到国内领先水平.     

土钉加锚杆联合支护基坑的失稳分析及处理

根据具体工程实例,介绍了在基坑开挖时采用土钉加锚杆的联合支护方式后在施工过程中出现坍塌裂缝的现象,针对这一现象,分析了施工条件与环境,得出了事故发生的原因,并结合实际情况提出了处理措施.