Rückgewinnung von Vinylchloridmonomer

The production of the polymer polyvinylchloride (PVC) emits a high amount of waste gas. The recovery of the evaporated base product vinylchoridemonomer (VC) is an important aspect for the economics of the whole process. Membrane and vacuum technology improve the efficiency and the economics of the recovery process considerably.     

Multistage amplifier topologies with nested Gm-Ccompensation

This paper presents a multistage amplifier for low-voltage applications (<2 V). The amplifier consists of simple (noncascode) low gain stages and is stabilized using a nested transconductance-capacitance compensation (NGCC) scheme. The resulting topology is similar to the well known nested Miller compensation (NMC) multistage amplifier, except that the proposed topology contains extra G _m feedforward stages which are used to enhance the amplifier performance. The NGCC simplifies the transfer function of the proposed multistage amplifier which, in turn, simplifies its stability conditions. A comparison between the NGCC and NMC shows that the NGCC has wider bandwidth and is easier to stabilize. A four-stage NGCC amplifier has been fabricated using a 2-μm CMOS process and is tested using a ±1.0 V power supply. A dc gain of 100 dB has been measured. A gain bandwidth product of 1 MHz with 58° of phase margin and power of 1.4 mW can be achieved. The op amp occupies an active area of 0.22 mm². Step response shows that the op amp is stable     

激光光束质量因子的研究进展

本文详细分析了各种光场下光束质量M2因子。在不同的场中,A.E.Siegman当初所定义的M2因子,已经有了很大的变化,因而M2因子的特性也与当初不同,不仅M2因子可以大于等于1,而且可以小于1,甚至小于0。其反映的物理意义,也从经典场中的衍射极限倍数,变化为非经典场中的准直性量度以及对空间相干性的某些反映。此外还列举并分析了几种特殊的光束质量因子,最后讨论了M2因子应用的问题并指出了其局限性。     

Statistical analysis of decision threshold for parallel acquisitionwith reference filtering in Rician fading channel

Statistical analysis of the decision threshold for parallel PN code acquisition in a Rician fading channel is presented. It is shown that in the performance analysis of the acquisition system with reference filtering, the statistical evaluation of the decision threshold seems more appropriate than the approximation of the decision threshold     

稻壳基碳量子点对废水中Pb(Ⅱ)的检测

为了进一步实现生物质废弃资源的综合利用,以及对废水中污染物的检测,以稻壳粉为原料,在600℃和N2氛围下煅烧完成后使用一步水热法制备了钝化剂修饰的碳量子点,得到荧光为蓝绿光的二酸铵(ACA-CQDs)改性稻壳基碳量子点.采用SEM/EDS、HRTEM、FTIR等现代分析技术对碳量子点进行了理化特性表征,发现二酸铵(ACA-CQDs)量子点可以成功检测水中的Pb(Ⅱ).建立了一种有效的检测水体中Pb(Ⅱ)简便快速高效的方法.     

Kinetics of the methanation of carbon dioxide over a supported Ni-La2O3 catalyst

The kinetics of the methanation of carbon dioxide was investigated using an alumina supported Ni-La₂O₂ catalyst in a differential and integral reactor. In the differential reactor the molar ratio of H₂ to CO₂ was varied from 0.6 to 30. In the integral reactor the rates were measured with up to 90% conversion. Both reactor tests were carried out at temperatures between 513 and 593 K. The experimental results were described by a Langmuir-Hinshelwood type equation. The kinetics can be explained by assuming equilibrium of dissociative carbon dioxide and hydrogen adsorption, and assuming hydrogenation of surface carbon as the rate determining step.     

我国明矾石的物化性质及其在水泥中的水化硬化

本文系统地介绍了我国明矾石的地质成因、化学成份和矿物组成及其在水泥中的水化硬化,提出了明矾石在碱-硫酸盐激发下形成钙矾石的水化机理,综述了我国利用明矾石作为特种水泥、外加剂的原料及作为普通水泥的混合材所取得的应用成果。     

抗氧剂3114合成反应热力学和动力学的研究

研究了常温溶剂法合成抗氧剂3114反应热力学和动力学过程。控制温度在117±2℃,研究结果表明,反应是零级反应,反应速率常数k=1.91×10-3/min,反应的平衡常数K=138.4(mol/L)-6,反应活化能Ea=1366.2J/mol。