新取代苯基荧光酮试剂的合成及其性质的研究Ⅱ．新型取代苯基荧光酮与金属离子显色反应的研究

研究了３，５－二溴－４－氨基苯基荧光酮、３，５－二溴－４－偶氮变色酸等８种苯基荧光酮在酸性介质中与高价金属离子Ｚｒ（Ⅳ）、Ｍｏ（Ⅵ）、Ｗ（Ⅵ）、Ａｌ（Ⅲ）、Ｇａ（Ⅲ）等的显色反应。３，５－位二溴取代的试剂的灵敏度高于未取代的灵敏度，摩尔吸光系数绝大多数在１０５Ｌ·ｍｏｌ－１·ｃｍ－１以上。     

Flashover voltage characteristics of contaminated station insulators under temporary ac overvoltages in the ac system connected with a frequency converter station

According to the recent analysis results of temporary ac overvoltage in the ac system connected with a frequency converter station, large-magnitude over-voltages were confirmed to occur under some special system conditions. Most of the station insulators currently used cannot withstand such overvoltages according to an evaluation based on the data obtained earlier. The necessity of tests to be done to evaluate such performance more accurately was recognized. Both power frequency and switching impulse overvoltage flashover tests were made on contaminated insulators by the method well simulating the natural wetting condition. Switching impulse flashover voltage with the waveshape having a long wavefront time of 2 ms can be well correlated with the flashover voltage characteristics of temporary ac overvoltage. Higher flashover voltage characteristics were obtained by a clean fog test method compared with those obtained by equivalent fog test method.     

Li2O在保护渣中的作用

采用在不同玻璃性的两种基渣中加入Ｌｉ２Ｏ为研究Ｌｉ２Ｏ对保护渣粘度，熔化温度及玻璃性能的影响，并对Ｌｉ２Ｏ改善保护渣玻璃性的机理进行了探讨，提出了寻找高速连铸保护渣中Ｌｉ２Ｏ的代用物的一种方法。     

Ti,N,Mg对M2高速钢凝固组织和硬度的影响

为了改善Ｍ２高速钢共晶碳化物的分布，本文利用小凝固试样变质的方法研究了Ｔｉ，Ｎ和Ｍｇ对Ｍ２高速钢凝固组织和硬度的影响。试验结果表明，加入Ｔｉ或Ｔｉ－Ｎ后，共晶碳化物形态和分布有很大改善，而加入Ｔｉ－Ｎ后对凝固组织有轻微的细化作用，但只添加Ｔｉ不补碳时，钢的淬火硬度和回火硬度均下降；加入适量的Ｍｇ可以使片状的Ｍ２Ｃ型共晶碳化物转为鱼骨状的Ｍ６Ｃ型共晶碳化物，使其分布有所改善，Ｔｉ和Ｍｇ复合加入可以明     

Improvement of levitation characteristics in a magnetic bearing system using HTSC‐permanent magnet hybrid structure

Magnetic bearing using pinning force of a permanent magnet and a high‐temperature superconductor has been developed. Additional permanent magnet is introduced to increase the levitation force of the magnetic bearing. In this hybrid magnetic bearing system, levitation force is mainly given by the repulsive force of the permanent magnets, and stability for the lateral direction is given by pinning force of the superconductor. The experimental device is developed. A ring‐type superconductor and a bulk one are examined. Levitation characteristics of the hybrid magnetic bearing are measured. The bulk superconductor shows better characteristics of both levitation and lateral stability than the ring one. Levitation force of the hybrid system becomes about twice as large as that of the nonhybrid one. Although, the repulsive force of the permanent magnet decreases the lateral stability of the system, its influence becomes small by choosing an adequate position of the permanent magnets and the superconductor. © 2004 Wiley Periodicals, Inc. Electr Eng Jpn, 150(1): 71–77, 2005; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/eej.10350     

Scanning electron microscope electron detector with a radial type discrete dynode electron multiplier

A discrete dynode electron multiplier with radial flux of electrons was built and tested in the range of low‐voltage scanning electron microscopy as a backscattered electron detector of topographic contrast. The multiplier collects backscattered electron emitted in a specific range of take‐off angles and over the whole azimuth angular range enabling large solid collection angle. Multipliers with different dynode shapes were studied theoretically with the use of the software for particle optics and three assemblies were built and tested experimentally. The gain estimation, assessment of the type of detected electrons (secondary electron or backscattered electron), imaging the spatial collection efficiency and signal‐to‐noise measurements were performed.     

建(构)筑物机械拆除方法综述

介绍了几种常用的建(构)筑物机械拆除方法,对其工作原理、特点、应用条件及局限性加以分析和说明。     

高强度烧结钢

为开拓粉末冶金材料新的应用领域，近年来对高强度烧结钢进行了大量的研究与开发。本文简要介绍Ｈｏｇａｎａｓ公司开发的一些高强粉末冶金材料及对一些高强度烧结材料尺寸变化的控制。     

Study on Factors Affecting the Structure of High SpeedSteel Ingot Produced by ESR

ＳｔｕｄｙｏｎＦａｃｔｏｒｓＡｆｆｅｃｔｉｎｇｔｈｅＳｔｒｕｃｔｕｒｅｏｆＨｉｇｈＳｐｅｅｄＳｔｅｅｌＩｎｇｏｔＰｒｏｄｕｃｅｄｂｙＥＳＲＬｉＺｈｅｎｇｂａｎｇ；ＣｈｅＸｉａｎｇｑｉａｎＡｂｓｔｒａｃｔ：Ｔｈｅｉｎｆｌｕｅｎｃｅｏｆｔｈｅｍｅｔａｌｐ...     

交流探尺的控制及其在武钢新3^#高炉上的应用

本文论述了交流探尺的控制原理及到料面信号的检测方法。以其在武钢新３＃高炉上的应用为例，给出系统组态、控制框图及它在无料钟系统中所起的补偿倾动角度的作用。最后对交流、直流探尺系统进行了比较。