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Z. Gruba? 《Materials Letters》2007,61(3):794-798
The initial stage of copper electrodeposition on the electrochemically activated assembly of carbon microelectrodes from an acid solution of copper sulfate was investigated using cyclic voltammetry, potentiostatic pulse technique and electrochemical impedance spectroscopy. Analysis of the experimental current transients has been carried out using a non-linear fitting procedure according to the model that takes into account spherical diffusion towards a disc-shaped microelectrode. The higher values of diffusion coefficient in comparison with those observed on planar electrodes were explained with an increased diffusion caused by the electrode geometry. Impedance spectra showed two time constants, the high-frequency related to the charge transfer process and the low-frequency corresponded to the deposit morphology. 相似文献
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从印刷技术的发展看印刷业的重新定位 总被引:1,自引:1,他引:0
近20年以来的技术革命使印刷业发生了脱胎换骨的变化,曾经被认为是技术含量低、员工文化素质低、劳动密集型的印刷业已今非昔比。世界上最先进的电子技术、激光技术、计算机技术及网络技术在印刷领域广泛地应用与发展,改变了人们对印刷的传统思维和行为。在信息时代的今天。印刷业已经成为信息社会的先行行业。在新的形势下,印刷业的经营既离不开生产又离不开增值服务,全面解决方案的推行使印刷业的外延扩大到了第三产业。 相似文献
14.
轻便型γ能谱测井仪几个关键技术问题的探讨 总被引:1,自引:0,他引:1
为研制性能好,功能强,微机化学程度高的轻便型γ能谱测井仪,针对非油气测井工作的井口径小(〈φ60mm)井身浅(〈1000m)等特点,探讨了γ能谱测井仪的轻便化,测量精度,信号传输技术,稳谱技术及微机化等关键技术问题。 相似文献
15.
国际乳业的热点论题:蛋白质标准化 总被引:1,自引:0,他引:1
介绍了蛋白质的标准化这一国际乳品界正热的研究和讨论题目,综述了蛋白质标准化的必要性和世界上目前采用的方法,展望了膜技术在蛋白质标准化上的应用前景。 相似文献
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为提高环网的容错性能,文献(1)提出了一种基于事件驱动的故障重构算法,其缺点是该算法只能容忍连线故障。本文给出一种新的采用时钟起时驱动的重构算法,该算法既能容忍连线故障也能容忍站(或节点)故障,且令牌控制较文献(1)的简单。 相似文献
18.
Nuclear magnetic resonance (n.m.r.) studies of 19F nuclei in a random copolymer of vinylidene fluoride and trifluoroethylene were performed at 9.14 MHz and 20.0 MHz. The free induction decays (FIDs) were analysed in terms of two T2 components attributed to the amorphous and crystalline portions of the polymer. The changes in crystallinity as well as the effects of the ferroelectric transition were observed during cycles of heating and cooling between 20°C and 140°C. The crystalline component of the FID lengthens by a factor of 2 at 100°C on heating and decreases by this factor at 60°C on cooling, thus exhibiting the thermal hysteresis of this ferroelectric transition. The spin-lattice relaxation was also investigated. From measurements at 9.14 MHz the observed longitudinal relaxation time T1 appears to be dominated by the dynamics of the amorphous phase and exhibits no anomaly through the phase transition. However, from measurements at 20 MHz, well defined minima of T1 were observed, which are associated with the ferroelectric transition (especially after repeated annealing of the samples). Results are discussed in terms of the crystalline phase structure, which appears dynamically disordered above the ferroelectric phase transition. An analogy is considered with the plastic phase transitions encountered in molecular crystals. 相似文献
19.
F. D. McDaniel B. L. Doyle C. H. Seager D. S. Walsh G. Vizkelethy D. K. Brice C. Yang P. Rossi M. Nigam M. El Bouanani G. V. Ravi Prasad J. C. Schwartz L. T. Mitchell J. L. Duggan 《Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms》2002,190(1-4):1-10
A new ion beam analysis-based, single ion technique called the time to first photon has been developed to measure the decay of the luminescence signal of phosphors. Such measurements are currently needed to study luminescence decay mechanisms following high-density excitations and to identify strongly luminescent phosphor coatings with short lifetimes for ion photon emission microscopy (IPEM). The samples for this technique consist of thin phosphor layers placed or coated on the surface of PIN diodes. Single ions from an accelerator strike this sample and simultaneously create ion beam induced luminescence (IBIL) from the phosphor that is measured by a single-photon-detector, and an ion beam induced charge collection (IBICC) signal in the PIN diode. In this case, the IBICC signal provides the start pulse and the IBIL signal the stop pulse to a time to amplitude converter. It is straightforward to show that this approach also measures a signal proportional to activity versus time with an accuracy of 5% as long as the number of detected photons per ion is less than 0.1, which usually requires the use of absorbers for the IBIL detector or electronic discrimination for the IBIL signals. Details of the new analysis are given together with examples of luminescence decay measurements of several ceramic phosphors being considered to coat IPEM samples. IPEM is currently being developed at Sandia National Laboratory (SNL), the University of North Texas in Denton, and the Universities and INFN of Padova and Torino. 相似文献
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