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131.
To confirm the reliability of the theory of phase equibria of multicomponent polymer 1/multicomponent polymer 2 systems (i.e. quasi-binary systems) and the method of computer experiment based on this theory (Brit. Polym. J., 23 (1990)285; 23 (1990)299; Polym. Int., 29 (1992)219), could point curves (CPC), two-phase volume ratios ( R ) and critical solution points (CSP) have been determined experimentally for the quasi-binary mixtures of poly(ethylene oxide) (M¯w = 647, M¯w/M¯n = 1.15; M¯w and M¯n, the weight-average and numberaverage molecular weights, respectively) and poly(propylene oxide) (M¯w = 2028, M¯w/M¯n = 1.08; and Mw = 2987, Mw/Mn = 1.13). The hydroxyl end groups of both polymers were methoxylated in advance by the Cooper & Booth method (Polymer, 18 (1977)164). The thermodynamic interaction parameter between both polymers, χ12, and the concentration dependence parameters for the above quasi-binary systems were determined by the method proposed in a previous paper (Brit. Polym. J., 23 (1990)299). CPC, R and CSP values calculated on the basis of the theory are in good agreement with the values determined experimentally. 相似文献
132.
133.
The relatively fast diffusion of Au atoms in eutectic PbSn matrix is considered one of the contributing factors to the Au
embrittlement problem. In this study, we further investigated the Au embrittlement problem in high-Sn solders. Experimentally,
Sn3.5Ag (wt.%) spheres with 500-μm diameter were soldered over the Au/Ni soldering pads. It was found that some of the AuSn4 needles that formed after reflow inside the solder migrated back to the solder/pad interface during thermal aging. However,
the migration kinetics in high-Sn solders was slower compared to that in eutectic PbSn. The difference in migration kinetics
of AuSn4 in eutectic PbSn and SnAg was ascribed to the difference in the magnitudes of the Au flux and the Ni flux. In eutectic PbSn,
the Au flux was much greater than that of the Ni flux, and the Au and Ni flux were in the same order of magnitude in eutectic
SnAg. The relative magnitude of the Au and Ni flux changed in eutectic PbSn and SnAg because the homologous temperatures of
PbSn and SnAg were different. 相似文献
134.
135.
136.
Takaaki Wajima Tomoe Shimizu Yasuyuki Ikegami 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(6):921-927
BACKGROUND: This study aimed to investigate the synthesis of zeolites from paper sludge ash (PSA) with added diatomite to remove both NH4+ and PO43? for water purification. The PSA had low Si and significant Ca contents. Four types of diatomite: white (T‐W) and brown (T‐B) from deposits of marine origin in Takanosu, and white (S‐W) and gray (S‐G) from lacustrine deposits in Shonai, were added to NaOH solution to increase the Si content and thereby synthesize zeolites with high cation exchange capacity (CEC). RESULTS: The order of the amounts of Si extracted from the diatomite to the alkali solution was S‐W > T‐W = T‐B > S‐G, which correlates with the amorphous SiO2 content of diatomite. The original ash without addition of diatomite yielded hydroxysodalite with CEC of about 1.0 mmol g?1. For all samples, the addition of diatomite to the solution yielded zeolite‐P with a higher CEC, but the addition of excess Si inhibited the synthesis of zeolite‐P, and the CEC of the product was low. A product with high CEC including zeolite‐P was obtained in a solution with around 500 mmol L?1 of Si concentration, and had the ability to remove both NH4+ and PO43?. CONCLUSION: Diatomite has the potential for used as an additive for the synthesis of high CEC zeolite from PSA. The product with zeolite‐P exhibited relatively high CEC, capacity for NH4+ uptake, and the ability to remove PO43? by precipitation, which is preferable for water purification applications. Copyright © 2008 Society of Chemical Industry 相似文献
137.
The forming behaviour at high temperature of a modified 9%Cr‐1%Mo (P91) ferritic steel containing B and Ti for elevated temperature service was investigated. The microstructure of the as‐received material is mainly martensite at room temperature, but special etching revealed prior austenite grains of about 25 μm in size. Torsion tests were conducted at temperatures in the range 850 to 1250 °C to simulate the hot rolling process under comparable conditions of temperature, strain rate and strain. The deformation data obtained from these tests were correlated with the Garofalo equation with a stress exponent of 4.6 and an activation energy of 315 kJ/mol. This equation was used to predict the formability behaviour for the rolling process and also to determine the maximum forming efficiency and stability of the steel. A temperature of 1200 °C is recommended to conduct the forming process. 相似文献
138.
Nadia Ben Atti Gema M. Diaz–Toca Henri Lombardi 《Applicable Algebra in Engineering, Communication and Computing》2006,17(1):75-82
We propose a slight modification of the Berlekamp-Massey Algorithm for obtaining the minimal polynomial of a given linearly
recurrent sequence. Such a modification enables to explain it in a simpler way and to adapt it to lazy evaluation.
partially supported by the Galois Theory and Explicit Methods in Arithmetic Project HPRN-CT-2000-00114
partially supported by the European Union funded project RAAG CT-2001-00271 相似文献
139.
针对W9Cr3M04V轧制成品材低倍碳化物剥落的形成原因分析,得出一次碳化物颗粒粗大、在1/4D至中心区域聚集是导致低倍热酸浸试验碳化物剥落的主因;由此进行冶炼过程中注速(锭形)、浇注温度选择对比工艺试验,得出在原有冶炼+轧制的工艺基础上选用2.2t锭、降低浇注温度(1489℃)能有效改善一次碳化物颗粒大小和聚集程度,进而有效降低低倍碳化物剥落倾向。 相似文献
140.
In this research, Ni/SiO2 catalyst was modified with different amount of Gd2O3 and characterized with temperature-programmed desorption of CO2 (CO2-TPD) and NH3 (NH3-TPD), temperature-programmed reduction with H2 (H2-TPR) and X-ray diffraction (XRD). It was found that Gd2O3-modified Ni/SiO2 catalysts possessed higher CO2 adsorption and activation ability due to the formation of surface carbonate species. H2-TPR and XRD characterizations found that the strong interaction among nickel, Gd2O3 and SiO2 took place, which improved the dispersion of Ni. Gd2O3-modified Ni/SiO2 catalysts exhibited higher activity and stability for the combined oxy-CO2 reforming of methane in fluidized-bed reactor. The H2/CO ratio in produced syngas could be controlled via controlling reaction temperature and CO2/O2 ratio in feed. 相似文献