Growth and optical property of zinc oxide thornballs

A new microstructure, thornball, of zinc oxide (ZnO) was synthesized by a very simple solid vapor deposition process under lead oxide (PbO) atmosphere. The microthornballs consist of numerous needles, which extend outwards in all directions symmetrically. They have dimensions of 120 μm in diameter, while the average diameter of the needles is about 100-200 nm. The needles on the balls grow along the 〈0 0 0 1〉 orientation and have gradient compositions along radial. Control experiments proved that PbO played an important role in the growth. Additionally, photoluminescence property was observed and provided the evidence that PbO did not deteriorate the optical properties of ZnO thornballs. This kind of microstructures has potential applications in the field of photochemical catalysis.     

织物树脂层压复合材料抗弹性能研究

针对防弹织物树脂层压复合材料的研制，考察了层压复合材料面密度，纤维类型，树脂体系，铺层混杂方式及纤维混杂分数，织物铺层，预置分层等因素对层压复合材料靶板弹道冲击性能的影响。     

热物理性质测试技术研究现状和发展趋势

本文在对热物理性质研究在热能工程、材料科学、信息科学、航天工程、环境工程、生物科学、微电子技术和计量学等众多科技领域中的重要性进行探讨的基础上，评述了热物理性质测试技术的研究现状和发展趋势。鉴于薄膜材料在微电子器件、集成电路和微电子机械系统等领域中日益广泛的应用，本文还综述了亚微米－纳米尺度薄膜材料热导率和热扩散率的测试新技术。     

Influence of residual milk-clotting enzyme and proteolysis on melting properties of soft cheese

In this work, we assessed the influence of coagulant residual activity and primary proteolysis on Cremoso Argentino cheese melting properties. For that purpose, we made Cremoso soft cheeses using different amounts of coagulant, and also obtained samples in which milk-clotting enzyme was inactivated. Primary proteolysis correlated with residual activity of coagulant in early stages of cheese ripening; however, it was similar in all cheeses after 30 days. The hydrolysis of caseins did not significantly affect the melting ability of the cheeses, expressed as the area increase after heating samples under standardized conditions. Samples with similar proximate composition showed some changes in meltability; those seemed related to pH evolution during ripening.     

碘量法测铜中物质性质和分析操作

本文讨论了碘量法测定铜量中一些有关物质的特性,以及这些性质对分析条件和操作的要求。     

Water-soluble copolymers: 22. Copolymers of acrylamide with 2-acrylamido-2-methylpropanedimethylammonium chloride: Aqueous solution properties of a polycation

The viscometric, turbidimetric and potentiometric properties of copolymers of acrylamide (AM) with 2-acrylamido-2-methylpropanedimethylammonium chloride (AMPDAC) were studied in aqueous solutions. The AMPDAC polymers exhibit poor salt tolerance and large, negative viscosity/temperature coefficients. Furthermore, the polymers were found to be sensitive to changes in pH. The AMPDAC polymers undergo phase separation in the presence of dianions as a function of temperature and AMPDAC composition.     

La doping effects on intergrowth Bi2WO6–Bi3TiNbO9 ferroelectrics

La doping effects on intergrowth Bi₂WO₆–Bi₃TiNbO₉ ferroelectric ceramics were studied by X-ray diffraction, electron probe microanalysis and dielectric spectroscopy. It was found that the La³⁺ distribution, ferroelectric phase transition and dielectric relaxation behavior are apparently affected by La doping. With increasing La³⁺ content, the site of dopant ion varies, the grain growth of Bi₅TiNbWO₁₅ is restrained, the Curie temperature is reduced and broadened. Furthermore, two dielectric relaxation loss peaks were observed both in temperature and frequency spectra. The calculated relaxation parameters revealed the oxygen vacancy related to the relaxation process.     

The principles of information processing based on the numerical solution of the nonlinear heat-conduction problem. Pt. 1. The three-dimensional discrete mathematical model

A three-dimensional solution of the direct problem of heat conduction when a linear pulsed heat source acts in the plane of contact of two semibounded bodies is presented. The solution is obtained by the method of finite differences. An example of the modeling is considered. __________ Translated from Izmeritel’naya Tekhnika, No. 10, pp. 42–45, October, 2007.     

Nucleation of copper on an assembly of carbon microelectrodes

The initial stage of copper electrodeposition on the electrochemically activated assembly of carbon microelectrodes from an acid solution of copper sulfate was investigated using cyclic voltammetry, potentiostatic pulse technique and electrochemical impedance spectroscopy. Analysis of the experimental current transients has been carried out using a non-linear fitting procedure according to the model that takes into account spherical diffusion towards a disc-shaped microelectrode. The higher values of diffusion coefficient in comparison with those observed on planar electrodes were explained with an increased diffusion caused by the electrode geometry. Impedance spectra showed two time constants, the high-frequency related to the charge transfer process and the low-frequency corresponded to the deposit morphology.     

VN合金在大规格角钢生产中的应用研究

大规格角钢主要用于铁塔制造和建筑结构中。唐钢过去用16Mn钢生产Q345级别角钢，因供轧化学成分范围较窄，供轧率偏低。通过加入V-Fe合金及VN合金进行微合金化，设计了16Mnv(N)钢种生产角钢，使角钢综合性能有显著提高。分析比较了16Mn、16MnV及16MnV(N)角钢的性能，认为在大规格高强度角钢生产中，用VN合金进行微合金化，其效果是最佳的。