碘量法测铜中物质性质和分析操作

本文讨论了碘量法测定铜量中一些有关物质的特性,以及这些性质对分析条件和操作的要求。     

Water-soluble copolymers: 22. Copolymers of acrylamide with 2-acrylamido-2-methylpropanedimethylammonium chloride: Aqueous solution properties of a polycation

The viscometric, turbidimetric and potentiometric properties of copolymers of acrylamide (AM) with 2-acrylamido-2-methylpropanedimethylammonium chloride (AMPDAC) were studied in aqueous solutions. The AMPDAC polymers exhibit poor salt tolerance and large, negative viscosity/temperature coefficients. Furthermore, the polymers were found to be sensitive to changes in pH. The AMPDAC polymers undergo phase separation in the presence of dianions as a function of temperature and AMPDAC composition.     

La doping effects on intergrowth Bi2WO6–Bi3TiNbO9 ferroelectrics

La doping effects on intergrowth Bi₂WO₆–Bi₃TiNbO₉ ferroelectric ceramics were studied by X-ray diffraction, electron probe microanalysis and dielectric spectroscopy. It was found that the La³⁺ distribution, ferroelectric phase transition and dielectric relaxation behavior are apparently affected by La doping. With increasing La³⁺ content, the site of dopant ion varies, the grain growth of Bi₅TiNbWO₁₅ is restrained, the Curie temperature is reduced and broadened. Furthermore, two dielectric relaxation loss peaks were observed both in temperature and frequency spectra. The calculated relaxation parameters revealed the oxygen vacancy related to the relaxation process.     

The principles of information processing based on the numerical solution of the nonlinear heat-conduction problem. Pt. 1. The three-dimensional discrete mathematical model

A three-dimensional solution of the direct problem of heat conduction when a linear pulsed heat source acts in the plane of contact of two semibounded bodies is presented. The solution is obtained by the method of finite differences. An example of the modeling is considered. __________ Translated from Izmeritel’naya Tekhnika, No. 10, pp. 42–45, October, 2007.     

Nucleation of copper on an assembly of carbon microelectrodes

The initial stage of copper electrodeposition on the electrochemically activated assembly of carbon microelectrodes from an acid solution of copper sulfate was investigated using cyclic voltammetry, potentiostatic pulse technique and electrochemical impedance spectroscopy. Analysis of the experimental current transients has been carried out using a non-linear fitting procedure according to the model that takes into account spherical diffusion towards a disc-shaped microelectrode. The higher values of diffusion coefficient in comparison with those observed on planar electrodes were explained with an increased diffusion caused by the electrode geometry. Impedance spectra showed two time constants, the high-frequency related to the charge transfer process and the low-frequency corresponded to the deposit morphology.     

大型水轮发电机组励磁变压器参数及绝缘方式的选择--由三峡机组励磁系统投运引起的思考

结合三峡机组励磁系统的调试及投运经验,对大型水电机组静止自励系统选型中存在的一些关键性技术课题进行分析与论证,期望得出的结论有助于在大型水轮发电机组励磁系统参数选择和在提高机组运行安全、可靠性方面提供有益的借鉴。文中提出的励磁系统设计新理念仅代表个人的观点。     

论普通型胶辊表面不处理的合理工艺参数

论述了普通胶辊表面不处理的性能特点和存在问题，技术措施和合理工艺参数，提高了成纱条干水平，减少缠绕和磨损。     

VN合金在大规格角钢生产中的应用研究

大规格角钢主要用于铁塔制造和建筑结构中。唐钢过去用16Mn钢生产Q345级别角钢，因供轧化学成分范围较窄，供轧率偏低。通过加入V-Fe合金及VN合金进行微合金化，设计了16Mnv(N)钢种生产角钢，使角钢综合性能有显著提高。分析比较了16Mn、16MnV及16MnV(N)角钢的性能，认为在大规格高强度角钢生产中，用VN合金进行微合金化，其效果是最佳的。     

Investigation of structural properties of ITO thin films deposited on different substrates

The influence of the substrate nature on the structure and morphology of ITO thin films grown by thermal evaporation in vacuum is investigated. The as-prepared metal films with Sn/In molar ratio of 0.1 were subsequently annealed for 2 h at 723 K in air (to obtain tin doped indium oxide), then annealed in vacuum at 523 K, followed by UV irradiation (to reduce the electrical resistivity). Irrespective of substrate nature, XRD data evidence a (222) preferential orientation in films. Substrate nature, annealing in vacuum and UV irradiation influence the structure, morphology, optical, electrical and surface wetting properties of the films' surface.     

Industrialization of High Performance Sintered NdFeB Magnets

Sintered Nd-Fe-B magnet was manufactured by advanced equipment via a SC (Strip casting) technology.It has integrative performance.