Cu含量对Mullite／Al—Cu复合材料时效硬化行为的影响

用挤压铸造方法制备了Mullite/Al-Cu复合材料,用硬度测试仪、差示扫描量热仪（DSC）和透射电镜（TEM）等设备研究了铝基复合材料及其基体合金中Cu含量变化对时效硬化行为的影响,同时还研究了增强纤维对时效相的板出序列、析出相和位错结构的影响。结果表明,无论是在复合材料中还是在基体合金中,随着Al-Cui合金中Cu含量的增加,时效硬化过程均有不同程度的加速;Mullite纤维的引入提高了Al-Cu合金的时效硬度,明显加速了Al-Cu合金的时效硬化过程,对GP区的形成有抑制作用,但不影响基体沉淀相的析出顺序。     

温度及溶质浓度对Mullite短纤维增强的Al—Cu复合材料及其基体合金时效行为的影响

用挤压铸造方法制备Mullite／Al—Cu复合材料及其基体合金。用硬度测试(HB)、差示扫描量热仪(DSC)和透射电镜(TEM)等手段，研究了温度和溶质原子浓度对复合材料及其基体合金时效行为的影响。结果表明：复合材料和基体合金具有相似的时效硬化曲线及相同的时效析出序列，随时效温度的升高，峰值硬度降低、析出过程加快；溶质浓度升高，峰值硬度升高、析出过程同样得到加快；纤维除了能明显提高Al—Cu合金的时效硬度外，还能加速其时效析出过程，但对GP区的形成具有明显的抑制作用，而对θ相的析出影响不大。     

莫来石短纤维增强Al—0.95Mg—0.85Si复合材料的时效行为研究

用挤压铸造方法制备Mullite/Al-0.95Mg-0.85Si复合材料。用硬度测试、差示扫描量热仪（DSC）和透射电镜（TEM）等手段,研究了莫来石短纤维增强Al-0.95Mg-0.85Si复合材料及其基体合金的时效行为。结果表明：无论是复合材料还是基体合金,它们都具有相似的时效硬化曲线及相同的析出序列;Mullite纤维的引入明显提高了基体合金的时效硬度,并一定程度地加速了Al-0.95Mg-0.85Si合金的时效硬化过程,但对低温下由空位扩散控制的SSS→GP反应无明显抑制;温度对复合材料及其基体合金时效硬化行为的影响基本一致。     

Mullite/Al-Mg-Si复合材料时效行为研究

选用挤压铸造法制备Mullitel/Al-Mg-Si复合材料，采用扫描电镜、透射电镜等手段．研究了莫来石短纤维增强不同镁硅比Al-Mg-Si复合材料及其基体合金的时效行为。结果表明：复合材料具有和基体合金相似的时效硬化曲线，相同的析出序列；Mullite纤维的引入提高了基体合金的时效硬度，并一定程度地加速了基体合金的时效硬化过程．但对CP区的抑制不明显；Si或Mg元素的富余都加速了复合材料及其基体合金的时效硬化过程，且两类材料的时效峰明显提前。Mullite短纤维与富余的Si或Mg元素对复合材料的时效硬化过程具有交互促进作用。     

Mullite/ZL101复合材料的组织及时效特性

用挤压铸造制备Mullite/ZL101复合材料。用光学显微镜及透射电镜（TEM）观察复合材料及其基体合金的微观组织，用硬度测试及差示扫描量热仪研究Mullite/ZL101复合材料及其基体合金的时效特性。结果表明：采用挤压铸造法可获得复合良好的Mullite/ZL101复合材料，Mullite纤维对ZL101合金有明显的强化作用；在整个时效过程中，复合材料的时效硬度明显高于基体合金，纤维的引入没有改变基体合金时效析出序列，对低温下由空位扩散控制的SSS－GP反应无明显的抑制作用；复合材料中β″析出反应的峰值温度及活化能较基体合金的低，时效硬化过程得到一定程度的加速。     

温度对Mullite/Al-3.5Cu复合材料时效的影响

用挤压铸造方法制造Mullite/Al-3.5Cu复合材料及其基体合金，用硬度测试（HB），差示扫描量热仪（DSC）和透射电镜（TEM）等手段，研究了温度对复合材料及其基体合金时效和为的影响。结果表明：复合材料和基体合金具有相似的时效硬化曲线及相同的时效析出序列，随时效温度的升高，峰值硬度降低，时效析出过程加快；莫来石纤维除了能明显提高Al-3.5Cu合金的时效硬度外，还能加速其时效析出进程，但对GP区的形具有明显的抑制作用，而对θ相的析出影响不大。     

镍和锰对Al-Si-Cu-Mg合金凝固组织及时效硬化的影响

采用DSC差热分析及急冷试验方法并辅以微区成分分析 ,探讨了Ni和Mn对Al Si Cu Mg四元合金凝固组织、凝固过程及时效硬化特性的影响。Ni的加入量达 4%以上时 ,在组织中将形成初晶型Al Ni Cu三元化合物和共晶型Al Ni Cu三元化合物 ,若同时添加Mn ,则还会结晶出共晶型的Al Si Cu Ni Mn五元化合物 ;Ni和Mn的加入可以加快Al Si Cu Mg合金的时效硬化速度 ,同时又可推迟过时效现象的出现 ,有利于合金耐热性的提高。     

Cu含量对Al-2.5Mg-xCu-0.2Si合金微观组织和性能的影响

研究了Cu含量对Al-2.5Mg-x Cu-0.2Si合金微观组织和性能的影响。结果表明:由于形成Cu、Mg原子团簇,加入Cu的合金的显微硬度在时效初期有明显的快速硬化。随着时效时间的延长,由于S′相和GPB的形成使得合金的硬度再次提高,并达到硬度峰值。快速硬化的硬度值和峰值硬度值均随铜含量的增加而增加。铜含量增高,合金的抗拉强度和屈服强度增加明显,延伸率降低。含铜量增高,合金的抗晶间腐蚀能力变差。当Cu含量低于1.14%(质量分数,下同)时,合金具有良好的抗晶间腐蚀性能;但含铜2.10%的合金抗晶间腐蚀性能显著降低。实验结果表明:含铜量为1.14%的合金具有较好的机械性能和抗腐蚀能力。     

Cu含量对Al-2.5Mg-xCu-0.2Si合金微观组织和性能的影响（英文）

研究了Cu含量对Al-2.5Mg-x Cu-0.2Si合金微观组织和性能的影响。结果表明:由于形成Cu、Mg原子团簇,加入Cu的合金的显微硬度在时效初期有明显的快速硬化。随着时效时间的延长,由于S′相和GPB的形成使得合金的硬度再次提高,并达到硬度峰值。快速硬化的硬度值和峰值硬度值均随铜含量的增加而增加。铜含量增高,合金的抗拉强度和屈服强度增加明显,延伸率降低。含铜量增高,合金的抗晶间腐蚀能力变差。当Cu含量低于1.14%(质量分数,下同)时,合金具有良好的抗晶间腐蚀性能;但含铜2.10%的合金抗晶间腐蚀性能显著降低。实验结果表明:含铜量为1.14%的合金具有较好的机械性能和抗腐蚀能力。     

铸造Al8Si0.4Mg合金时效行为研究

利用硬度测定、差热扫描量热分析 (DSC)、电子探针微区成分分析和透射电子显微分析 (TEM)技术研究了铸造Al8Si0 .4Mg合金的铸态时效及固溶淬火时效 (T6)行为。硬度测定结果表明 :Al8Si0 .4Mg合金具有明显的铸态时效硬化效果 ,其铸态时效峰值硬度仅比T6状态硬度值低 6HV。冷却速度对合金时效没有明显的影响。DSC和TEM分析结果表明 :两种时效状态下合金的时效硬化均是过渡相 β″和 β′相析出对基体的强化。对合金在两种时效状态下析出相的分布及硬度均匀化系数进行了分析讨论     

Mullite/Al-4.5Cu复合材料的时效特性

选用挤压铸造法制备mullite/Al-4.5Cu复合材料，采用硬度测试（HB）、差示扫描量热（DSC）、透射电镜（TEM）等手段研究了mullite/Al-4.5Cu复合材料的时效特性。结果表明：莫来石纤维的引入明显提高了基体合金的时效硬度，加速了基体合金的时效硬化速度，对SSS→GPI反应有抑制作用，但没有改变基体合金的时效析出序列。复合材料具有和基体合金相似的时效硬化曲线。温度对两类材料时效硬化行为的影响基本一致。     

纤维及界面反应对mullite／Al—4.0Cu—1.85Mg铝基复合材料时效行为的影响

采用挤压铸造方法制备mullite/Al-4.0Cu-1.85Mg铝基复合材料。用硬度测试（HB）,差示扫描量热仪（DSC）和分析透射电镜（ATEM）等手段,研究了复合材料及其基体合金的时效硬化特性,时效相的析出序列,析出相和位错的微观形貌特征以及界面结构,结果表明：mullite纤维的引入抑制了GPB区的形成,提高了基体合金的时效硬度,但纤维加速复合材料时效硬化的作用不明显,这是由于Mg元素在纤维／基体界面处发生了界面反应,生成镁铝尖晶石（MgCl2O4),使复合材料中非纤维区内实际Mg含量降低所致。     

Aging characteristics of short mullite fiber reinforced Al-4.0Cu-1.85Mg metal matrix composite

Mullite short fiber reinforced Al-4.0Cu-1.85Mg composite and its base alloy were fabricated by squeeze casting. The age-hardening behavior, precipitation procedure, microstructure of dislocation and precipitates, and the interfacial structure have been studied by means of hardness measurement (HB), differential scanning calorimetry (DSC), and analytical transmission electron microscope (ATEM), respectively. The short mullite fiber in the composite induces high dislocation density in the near vicinity of the interface after it is solutionized and quenched in ice water, and suppresses or delays the formation of GPB zones. The aged hardness of the composite is always higher than that of its base alloy, but there appears little difference between the time needed in the composite and in the base alloy to reach the peak hardness, which means that the acceleration effect of mullite fiber in the precipitation of Al-Cu-Mg alloy is not great enough. Mg also reacts with Al and SiO₂, resulting in the formation of spinel (MgAl₂O₄), which depletes Mg in the matrix and finally hinders the aging acceleration in the testing composite.     

Effect of fabrication method on the aging behavior of 6061 Al matrix composites reinforced with SiC whiskers

Age hardening behaviors of SiC whisker reinforced composites with 6061 Al matrix fabricated by P.M. (powder metallurgy) and squeeze casting were investigated to examine the effect of the fabrication method on the aging kinetics. In the squeeze cast composite, numorous triangular particles which is believed to be MgAlp₂O₄ were observed at Al/SiC interfaces whereas no visible interface particles were observed in the P. M. composite. P.M. composite showed faster age hardening and reached the maximum hardness earler than the squeeze cast composites. The decrease of the aging kinetics in squeeze cast 6061 Al matrix composites compared to that in P.M. composites is thought to result from more severe depletion of Mg atoms due to interfacial reactions in squeeze cast composites. The uniformity of whisker distribution is suggested to influence the general aging behavior through its effect on the local dislocation density. Data on the aging kinetics and the interfacial reactions in other Al alloys were also examined to study various factors which can influence the aging kinetics.     

Comparative evaluation of X‐ray test results with bend test results for aluminium alloy welded joints

The SiC particle reinforced aluminum alloy has been developed for various machine parts. Aluminum welded machine parts often require welded joints composed of dissimilar alloys. In the present study, electron beam weldability of dissimilar joints was investigated on different combinations of aluminum alloys of 10 mm thickness. The main alloy is 10% SiC particle reinforced Al–Si aluminum alloy. Combination wrought alloys are Al–Si, Al–Mg, Al–Mg–Si and Al–Zn–Mg–Cu alloys. The electron beam machine is a 6 kW high voltage type. The joint groove is of square butt without filler metal.

In the case of SiC reinforced alloy/Al–Si and Al–Mg, joints, weldability was poor because some weld imperfections were recognized such as arcing and other defects. In the case of SiC reinforced alloy/Al–Mg–Si, Al–Zn–Mg–Cu, the cracking sensitivity is low while some small porosity was recognized. Tensile strength became about 150 MPa such as SiC reinforced alloy. Impact values of the SiC reinforced alloy/Al–Mg–Si joint were recovered through 2160 h room temperature ageing. Micro segregation of the Si element was recognized for the SiC reinforced alloy/Al–Mg–Si joint by electron probe microanalyser analysis.     

Casting fabrication of in situ Al3Ti-Al composites and their wear behaviors

The Al3li intermetallic reinforced pure Al, Al-13Si and Al-17Cu matrix composites were prepared by casting method. Their microstructures and dry sliding wear behaviors at room temperature and 100℃ were particularly investigated. The results indicated that the Al3Ti phases in these composites were all in flaky form. But the aspect ratio of the Al3Ti platelets decreased with the increase of Ti content in the pure AI, Al-Cu and Al-Si matrix composites, in order of effectiveness. The effect of Si on the Al3Ti morphology seemed to be greater than that of Cu. The distributions of the Al3Ti platelets were different in the different matrix composites, leading to different grain refining effects. Except for the sub-wear regime of adhesive wear, the plastic deformation induced wear was a dominant wear mechanism for all of the composites at room temperature and 100℃. Increasing the testing temperature, decreasing the Al3Ti content or the hardness of materials could enhance these two wear mechanisms, and thus increase the wear rate. The Al-Cu matrix composite had the best wear resistance, while the pure Al matrix composite showed the worst for the same Ti content. These differences or changes were attributed to the differences in materials' hardness or the strengthening effects of the Al3Ti platelets.     

莫来石纤维对氧化铝陶瓷性能的影响

选用莫来石纤维为增强体,通过添加适量的烧结助剂,制备莫来石纤维增强氧化铝陶瓷基复合材料,探讨了不同烧结温度和不同纤维含量对复合材料性能的影响规律.结果表明:莫来石纤维增强氧化铝陶瓷基复合材料的相对密度、弯曲强度和断裂韧性随烧结温度和纤维含量的增加先增大后减小,当烧结温度为1450 ℃、纤维含量为15%时,复合材料的弯曲强度、断裂韧性最高,复合材料弯曲强度和断裂韧性分别达到502.36 MPa和3.48 MPa·m~(1/2),比基体材料分别提高63.8%和54.7%;相对密度达到98.41%.纤维的拔出和脱粘消耗了大量的能量,是莫来石纤维增强氧化铝陶瓷复合材料力学性能提高的主要原因.