固液混合铸造Al-40Si合金的显微组织和力学性能

采用固液混合铸造的Al-40Si合金组织细小，合金力学性能明显优于传统铸造和半固态加工合金，并且解决了传统铸造Al-40Si合金铸件难以热加工的问题。在本工艺条件下，当添加平均粒度为120μm的粉末且粉末添加量与合金熔体质量比为1时，Al-40Si合金中的初晶硅平均粒度可控制在30μm以下；材料的室温力学性能为：σb=119.6MPa，σ0．2=105MPa，δ=1．43％。     

固液铸造技术在高铬铝合金中的应用研究

采用一种全新的材料制备工艺——固液混合铸造技术制备了Al-Cr合金坯料。采用该技术获得的Al-Cr合金坯料的金相显微组织均匀,晶粒细小,呈等轴状或近等轴状,热挤后合金的力学性能为：σb=119．4MPa,σ0.2=89．3MPa,δ=1％,优于传统铸造和半固态铸造合金,使难以应用的高铬铝合金有了应用可能。     

固液混合铸造制备Al-10Cr合金的研究

采用固液混合铸造新技术，制备了Al-10Cr合金，研究了合金熔体过热度，加粉量和粉末粒度对材料组织和性能的影响。试验结果表明：合金熔体的过热度为35℃时最佳，当加粉量为60％、粉末粒度为147-246μm时可获得均匀的细晶组织，最佳室温力学性能为σb=119MPa，σ0.2=89．5MPa，δ=1．0％。     

固液铸造技术在高锰铝合金中的应用研究

通过加入同种成分粉末,研究了Al-Mn合金的固液混合铸造工艺,初步探索固液混合铸造后的金相组织及力学性能变化.采用该技术获得的Al-Mn合金坯料的金相显微组织均匀,晶粒细小,呈等轴状或近等轴状.采用固液混合铸造的室温力学性能σb=130MPa, σ0.2=80MPa, δ=1.2%;优于传统铸造和半固态铸造合金,使难以应用的高锰铝合金有了应用可能.     

挤压铸造2A50铝合金的热处理工艺

采用挤压铸造工艺生产了2A50大型铝合金轮毂,借助金相组织分析、微观形貌观察和力学性能测试等手段,对2A50变形铝合金在挤压铸造状态下的热处理工艺进行了试验研究。结果表明,合金的过烧温度为530℃;经过505℃×8h+515℃×2h固溶处理和160℃×12h时效处理,合金力学性能σb≥400MPa、δ≥6.5%;合金组织致密,晶粒细化,无各向异性。     

等径角挤压对AZ91D镁合金力学性能的影响

通过等径角挤压试验,并借助Instron拉伸材料试验机、金相显微镜等手段,对等径角挤压工艺对AZ91D镁合金力学性能的影响进行了研究。结果表明：用等径角挤压工艺可大大细化其微观组织,提高其力学性能;组织从原始铸坯的晶粒平均尺寸300μm左右细化到50pm以下,最细的可达到4～10μm;强度σb从100MPa提高到240MPa以上,伸长率δ从1％提高到4％以上。挤压温度对力学性能也有一定影响,当挤压温度为300C时,经过固熔处理的AZ91D镁合金试件的力学性能最好,σb=292．4MPa,δ=12．8％。加工路线也影响挤压后材料的力学性能,其中,路线B使材料的力学性能最好,路线C次之,路线A最低。     

多层喷射共沉积法制备6066铝合金／SiC颗粒复合材料

采用多层喷射共沉积工艺制备６０６６铝合金／１５％ＳｉＣ颗粒复合材料，得到了增强颗粒分布均匀、增强颗粒与基体界面洁净、基体冷凝速度高的沉积坯，沉积坯经挤压后进行Ｔ６状态处理，其力学性能为σｂ＝６４０ＭＰａ，σ０．２＝５１０ＭＰａ，Ｅ＝１３３ＧＰａ，δ＝９．４％。     

喷射沉积耐热铝合金8009板坯轧制工艺及其对板材组织性能的影响

研究了喷射沉积Al-8．5Fe-1．3V-1．7Si(8009)耐热铝合金板坯的轧制工艺，观察了轧制态板材的微观组织。实验结果表明：当变形程度达到60％左右，合金致密化阶段已基本完成；变形程度达到86.4％时，材料的相对密度为99％；合金金相组织微细均匀，未观察到明显的孔洞；成品板材在室温下σb=430MPa，δ=10％，350℃保温420s后测得σb=202MPa，δ=25．5％。     

AZ91D-RE-xCa镁合金挤压管件组织及性能

研究了镁合金AZ91D加入混合RE及Ca进行合金化后的AZ91D-RE-xCa（x=0．5、1．0、1．5）镁合金挤压管件的显微组织、室温及高温（150℃和200℃）力学性能。结果表明，合金化之后的镁合金挤压管件高温性能得到了显著的提高。在200℃时，钙含量（质量分数）为0．5％时，δb为225．2MPa，δ0.2为179．3MPa，δ为5．3％，好于同等试验条件下的镁合金AZ91D管件。     

喷射成形7055铝合金的显微组织和力学性能

采用全自动控制往复喷射成形工艺制备了7055铝合金的大规格喷射成形锭坯.通过显微组织分析和力学性能测试,研究工业规格喷射成形7055铝合金的初始组织、挤压工艺及热处理制度对显微组织和力学性能的影响.结果表明,喷射成形7055铝合金锭坯规格可达d 260 mm×1600 mm,晶粒为等轴状,粒度宏观均匀,主要在20～30 μm,组织无明显宏观偏析,锭坯致密度达到98.2 %.喷射成形态材料的T6态σb为500～543 MPa,显示控制往复喷射成形铝合金锭坯冶金质量优越.喷射成形锭坯经过小挤压比变形后达到全致密,大规格产品的T6态纵向σb提高到745 MPa,δ为12.8 %.     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

THERMODYNAMICS STUDY ON THE DECOMPOSITION OF CHROMITE WITH KOH

Institute of Process Engineering, Chinese Academy of Sciences, China, has proposed a method for oxidative leaching of chromite with potassium hydroxide. Understanding the mechanism of chromite decomposition, especially in the potassium hydroxide fusion, is important for the optimization of the operating parameters of the oxidative leaching process. A traditional thermodynamic method is proposed and the thermal decomposition and the reaction decomposition during the oxidative leaching of chromite with KOH and oxygen is discussed, which suggests that chromite is mainly destroyed by reactions with KOH and oxygen. Meanwhile, equilibrium of the main reactions of the above process was calculated at different temperatures and oxygen partial pressures. The stable zones of productions, namely, K2CrO4 and Fe2O3, increase with the decrease of temperature, which indicates that higher temperature is not beneficial to thermodynamic reactions. In addition, a comparison of the general alkali methods is carried out, and it is concluded that the KOH leaching process is thermodynamically superior to the conventional chromate production process.     

INFLUENCE OF HEAT TREATMENT ON DAMPING BEHAVIOUR OF THE MAGNESIUM WROUGHT ALLOY AZ61

The effect of isochronal heat treatments for 1h on variation of damping, hardness and microstructural change of the magnesium wrought alloy AZ61 was investigated. Damping and hardness behaviour could be attributed to the evolution of precipitation process. The influence of precipitation on damping behaviour was explained in the framework of the dislocation string model of Granato and Lücke.     

Theoretical Analysis for the Motion and Temperature of Melt Droplets in Spray Degassing Process

The motion of melt droplets in spray degassing process was analyzed theoretically. The height of the treatment tank in spray degassing process could be determined by the results of theoretical calculation of motion of melt droplets. To know whether the melt droplets would solidify during spraying process, the balance temperature of melt droplets was also theoretically analyzed. Then proof experiments for theoretical results about temperature of melt droplets were carried. In comparison, the experimental results were nearly similar to the calculation results.     

Growth Kinetics of Single Inclusion Particle in Molten Melts

On the basis of the single-particle framework, a new theory on inclusion growth in metallurgical melts is developed to study the kinetics of inclusion growth on account of reaction and collision. The studies show that the early growth of inclusion depends on reaction growth and Brawnian motion collision, and where the former is decisive, the late growth depends on turbulence collision and Stokes＇ collision, and where the former is dominant; collision growth is very quick during the smelting process, lessened in the refining process, but nearly negligible in the continuous casting process.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

An Easy Way to Quantify the Adhesion Energy of Nanostructured Cu/X(X=Cr,Ta,Mo,Nb,Zr) Multilayer Films Adherent to Polyimide Substrates

An approach based on film buckling under simple uniaxial tensile testing was utilized in this paper to quantitatively estimate the interfacial energy of the nanostructured multilayer films(NMFs) adherent to flexible substrates. The interfacial energies of polyimide-supported NMFs are determined to be *5.0 J/m2 for Cu/Cr, *4.1 J/m2 for Cu/Ta,*2.8 J/m2 for Cu/Mo, *1.1 J/m2 for Cu/Nb, and *1.2 J/m2 for Cu/Zr NMFs. Furthermore, a linear relationship between the adhesion energy and the interfacial shear strength is clearly demonstrated for the Cu-based NMFs, which is highly indicative of the applicability and reliability of the modified models.     

High-Speed Friction Stir Welding of SiC_p/Al–Mg–Si–Cu Composite

A 17 vol% SiCp/Al–Mg–Si–Cu composite plate with a thickness of 3 mm was successfully friction stir welded(FSWed) at a very high welding speed of 2000 mm/min for the first time. Microstructural observation indicated that the coarsening of the precipitates was greatly inhibited in the heat-affected zone of the FSW joint at high welding speed, due to the significantly reduced peak temperature and duration at high temperature. Therefore, prominent enhancement of the hardness was achieved at the lowest hardness zone of the FSW joint at this high welding speed, which was similar to that of the nugget zone. Furthermore, the ultimate tensile strength of the joint was as high as 369 MPa, which was much higher than that obtained at low welding speed of 100 mm/min(298 MPa). This study provides an effective method to weld aluminum matrix composite with superior quality and high welding efficiency.     

A STUDY OF TEMPERATURE-DEPENDENT VALENCE BOND STRUCTURE OF TITANIUM

On the basis of energy and shape method for the determination of the valence bond (VB) structures of crystal, the valence bond structure of titanium is redetermined at room temperature and calculated in the whole temperature range of 0-1943K. The outer shell electronic distribution of Ti is e_c~(2.9907) · (s_c~(0.4980) d_c~(2.4927)) ef1.0093 in crystal. The temperature dependences of the VB structures of hcp and bcc phases are the same. The VB structures of hcp and bcc phases monotonically increase or decrease with the increase in temperature, but show discontinuous changes at the phase-transformation temperature 1155K.