终轧温度对超高强热轧双相钢组织性能的影响

摘要：基于汽车轻量化原则,利用热轧大压下+超快冷+弛豫制备得到1200MPa级热轧双相钢（DP）,借助OM、SEM、TEM和室温拉伸等试验手段,研究了终轧温度对试验钢组织性能的影响。研究表明：随着终轧温度增加,铁素体体积分数和晶粒尺寸逐渐减小,马氏体的体积分数逐渐增加;抗拉强度增加,伸长率减小,强塑积减小,屈强比最低为0.56,n值最高为0.13。终轧温度对各相的体积分数、形貌、分布和析出行为有影响,组织中细小的铁素体晶粒、细化的马氏体板条束和弥散的析出相提高了材料的均匀变形能力,综合考虑轧机负荷、生产效率和力学性能,试验钢在该工艺条件下合适的终轧温度可取810～840℃。     

终轧温度对超高强热轧双相钢组织性能的影响

基于汽车轻量化原则,利用热轧大压下+超快冷+弛豫制备得到1 200 MPa级热轧双相钢(DP),借助OM、SEM、TEM和室温拉伸等试验手段,研究了终轧温度对试验钢组织性能的影响。研究表明:随着终轧温度增加,铁素体体积分数和晶粒尺寸逐渐减小,马氏体的体积分数逐渐增加;抗拉强度增加,伸长率减小,强塑积减小,屈强比最低为0.56,n值最高为0.13。终轧温度对各相的体积分数、形貌、分布和析出行为有影响,组织中细小的铁素体晶粒、细化的马氏体板条束和弥散的析出相提高了材料的均匀变形能力,综合考虑轧机负荷、生产效率和力学性能,试验钢在该工艺条件下合适的终轧温度可取810～840℃。     

硫含量对极低屈服点钢组织与性能的影响

摘要：采用Gleeble 3800热模拟试验机、OM、TEM与Vickers 硬度计，研究了不同变形温度下S含量对极低屈服点钢析出相、晶粒尺寸与硬度的影响；结合拉伸和冲击试验考察了S含量对实验室试轧钢板力学性能的影响。结果表明，不同变形温度下，当S质量分数由0.0018%提高至0.0077%，钢中晶粒尺寸发生粗化，硬度降低，析出相的主要类型由TiC变为Ti4C2S2和TiS，析出粒子的尺寸随之增大，分布数量减小。S质量分数为0.0077%的试轧钢板较S质量分数为0.0018%的试轧钢板具有更低的屈服强度且塑韧性并未降低，其综合力学性能更优且完全满足极低屈服点钢的要求。     

CSP热轧工艺对Ti微合金化钢组织和性能的影响

采用金相显微镜、电子显微镜、化学相分析等手段研究了CSP热轧工艺对Ti微合金化高强钢组织和性能的影响。结果表明:880℃终轧、620℃卷取试验钢的屈服和抗拉强度分别为825、895 MPa,钢中存在大量的纳米尺寸TiC粒子,其沉淀强化效果超过150 MPa;卷取温度降低到580℃,TiC的析出受到抑制,沉淀强化效果明显减弱。卷取温度显著影响钢中第二相粒子的析出过程,终轧温度和卷取温度改变对晶粒尺寸也有影响,两者综合作用的结果使Ti微合金化钢的强度和韧性发生变化。     

高氮钒微合金钢中终轧温度和锰的综合作用

通过对高锰高终轧温度钢和低锰低终轧温度钢的力学性能测试、并观察其组织及其碳氮化物的析出,研究了Mn和终轧温度在高氮钒微合金钢中的综合作用.结果表明： 高锰含量可以弥补高的终轧温度对组织的不利影响,而高的终轧温度可以弥补高的锰含量对析出的不利作用;提高锰含量同时提高终轧温度比降低锰含量同时降低终轧温度有利于组织细化和析出.     

600MPa级Nb-Ti微合金化高成形性元宝梁用钢的开发

设计了一种低C低Mn、Nb-Ti复合微合金化成分体系的600MPa级元宝梁用钢,并采用OM和TEM等仪器对组织与第二相析出物进行了分析。结果表明,在不同终轧温度下力学性能均能满足技术条件的要求,整卷力学性能波动较小,表现出了较好的力学性能稳定性;随终轧温度的降低,铁素体晶粒明显细化,同时尺寸分布在3~60nm之间的第二相粒子数量变多,细晶强化与析出强化效果均增大;当终轧温度与卷取温度分别为830与600℃时,试验钢表现出了最优的力学性能,屈服强度、抗拉强度与伸长率分别达到了536MPa、612MPa与30.5%,同时室温到-60℃温度范围内冲击功均保持在125J以上。     

500 MPa级Nb Ti微合金化方矩形管用钢的强化机制

采用光学显微镜和透射电子显微镜等对500 MPa级Nb Ti微合金化方矩形管用钢的组织与性能进行了分析，研究了其强化机制。结果表明，终轧温度和卷取温度对试验钢的组织和力学性能有显著影响，在研究的温度范围内，终轧温度和卷取温度的降低均有利于获得更加细小的铁素体晶粒与细小弥散的第二相析出物；当卷取温度不变时，随着终轧温度的下降，屈服强度、抗拉强度和断后伸长率均升高；当终轧温度不变时，随着卷取温度的逐渐下降，屈服强度和抗拉强度呈现出先上升后下降的规律，而断后伸长率呈现出单调上升的规律；试验钢在终轧温度为840 ℃和卷取温度为570 ℃时可获得最优的综合力学性能，其屈服强度和抗拉强度分别为537和578 MPa，断后伸长率为33.5%；细晶强化是试验钢最主要的强化机制，由晶粒细化引起的强度增量占总强度的49%～51%，由固溶强化引起的强度增量次之，占总强度的23%～27%，由析出强化引起的强度增量较小，仅占总强度的3.8%～8.2%。     

终轧温度对热轧高强集装箱用钢组织及性能的影响

利用金相显微镜、扫描电镜以及透射电镜等检测设备,研究了不同终轧温度对高强集装箱用钢的组织、性能及第二相粒子析出行为的影响。研究结果表明;不同终轧温度下高强集装箱用钢的组织均由铁素体和少量珠光体组成,铁素体晶粒度均为13.0级;850℃终轧与890℃终轧相比,屈服强度与抗拉强度分别提高32 MPa与26 MPa。理论计算与透射电镜观察结果表明:高强集装箱用钢强度的提高主要是因为850℃终轧时第二相粒子的形核率更高、析出数量更多、粒子间距更小,析出强化效果更加显著。     

碳强化型超低碳钢组织性能及强化机理

为了探索碳含量对超低碳钢力学性能的影响,在实验室冶炼了3种碳质量分数分别为0.002%、0.005%、0.008%的超低碳钢,将其轧制成热轧板,并分析碳含量和热轧卷取温度对钢板的力学性能、显微组织和第二相析出的影响。结果表明,随着碳质量分数由0.002%增加至0.008%,钢的屈服强度、抗拉强度明显增加,断后伸长率降低;随着碳含量的升高,580℃卷取时的强度变化比730℃卷取时的更显著。试验钢晶粒尺寸由碳质量分数为0.002%、卷取温度为730℃时的22μm减小至碳质量分数为0.008%、卷取温度为580℃时的11μm,第二相TiC粒子平均尺寸半径由碳质量分数为0.002%、卷取温度为730℃的35 nm减小至碳质量分数为0.008%、卷取温度为580℃时的10 nm。在碳质量分数为0.008%、卷取温度为730℃时,钢板的屈服强度达到230 MPa以上,计算得出其细晶强化值为64.5 MPa、析出强化值为56.8 MPa。工业生产数据显示,碳质量分数为0.008%时,超低碳钢的力学性能水平可满足高强IF钢的标准要求。     

热轧工艺对钛析出强化钢表面色差的影响

冷轧高钛成分体系析出强化钢表面色差影响成品质量,分析了热轧工艺对表面色差缺陷的影响和机理。表面色差是由带钢表层晶粒大小差异造成的,在热轧过程中,表层钛二相粒子析出量不同使得在退火过程中对晶粒细化作用不同,并造成表面色差。通过不同终轧温度和卷取温度对色差程度的影响试验表明,终轧温度低有利于成品色差缺陷的改善,卷取温度对色差缺陷改善不明显,860℃的终轧温度对应成品表面没有色差缺陷。     

Development of 600MPa grade Nb- Ti microalloyed high formability crossbeam steel

The 600MPa grade crossbeam steel with the composition of low Mn, low Si and Nb- Ti microalloyed was designed, and the microstructures and precipitates were analyzed by OM and TEM. The results show that the mechanical properties can meet the technical requirements under finishing temperature of 860?? or 830??, and the mechanical properties of coil show good stability with small fluctuation. The microstructures are mainly composed of ferrite and a small amount of pearlite. With the decrease of finishing temperature, the ferrite grains are obviously refined, and the amounts of second phase particles of size 3-60nm are increased, which increase the effect of fine grain strengthening and precipitation strengthening. The 600MPa grade Nb- Ti microalloyed highly formable crossbeam steel shows the best mechanical properties when the finish rolling temperature and coiling temperature are 830 and 600?? respectively. Meanwhile, the yield strength, tensile strength and elongation are respectively 536MPa, 612MPa and 30. 5% and the impact energy values under the temperature range of room temperature to -60?? are above 125J.     

600 MPa级热轧双相钢组织与性能优化分析

 通过热轧厂实际生产试制,研究了钛、铌微合金元素对600 MPa级低成本低温卷取型铁素体/马氏体双相钢组织和性能的影响,并与同强度级别中温卷取双相钢进行对比。研究结果表明,沿晶界分布的纳米级（Nb,Ti）C第二相显著细化了铁素体/马氏体两相组织,由此解决了不含钛、铌元素的低温卷取双相钢马氏体岛粗大的问题,提高其强度和塑性。此外,试制生产对比发现,中温卷取双相钢存在晶粒尺寸较粗,马氏体体积分数较少,强度相对略低等特征,并提出了相应的热轧工艺改进思路。     

Ti微合金化高强度热轧带钢组织性能及强化机理

The continuous cooling transformation behavior, the effect of coiling temperature on microstructure and mechanical properties, and strengthening mechanisms of Ti microalloyed high strength hot strip steel were systematically investigated by thermal simulation testing machine, laboratory rolling mill, SEM and HR-TEM. The dynamic CCT curve was established. The results show that the austenite to ferrite and pearlite transformation takes place when the cooling rate is less than 1??/s. The austenite to bainite transformation accompanied with austenite to ferrite and pearlite transformation takes place when the cooling rate is in the range of 5 ??/s to 10 ??/s. The bainitic transformation temperature is about 600??. The amount of granular bainite decreases, while the amount of lath bainite increases with the increase of cooling rate in the range of 20??/s to 50??/s. Furthermore, the study on the effect of coiling temperature on the microstructure and mechanical properties of experimental steel has shown that the strength and plasticity of tested steel are improved with decreasing the coiling temperature. When the coiling temperature is 550?棬the experimental steel possesses optimal mechanical properties owing to the grain refinement and precipitation of nano-scale TiC particles. And the tensile strength, yield strength and elongation of tested steel were 742MPa, 683MPa and 22??5%, respectively.     

1800MPa级低合金超高强度工程机械用钢显微组织与力学性能

 设计了一种新型的超高强度工程机械用钢,在中试轧机上进行了不同工艺模拟轧制,对比研究了工艺1（80%变形量+直接淬火+250℃回火）、工艺2（90%变形量+层流冷却快冷至650℃/1h+空冷+250℃回火）和工艺3（90%变形量+空冷至650℃/1h+空冷+250℃回火）3种不同控轧控冷工艺对试验用钢的显微组织和力学性能的影响。结果表明：工艺1条件下试验钢的抗拉、屈服强度最高,塑韧性最好,分别可达到1816,1473MPa,伸长率为9.5%,断面收缩率为45%,室温冲击功为28J,-40℃冲击功为21J,硬度值达到50HRC,认为获得的是板条马氏体+残余奥氏体的复相组织和析出的复合微合金碳化物、ε-碳化物强韧化机制的综合作用;工艺2,3分别得到的是板条马氏体+块状贝氏体+残余奥氏体、板条马氏体+针状铁素体+片层状珠光体+残余奥氏体,力学性能下降明显;第二相析出物主要是Nb,V,Ti的复合析出颗粒。     

Effects of micro-alloying and production process on precipitation behaviors and mechanical properties of HRB600

Effects of micro-alloying elements and production process on microstructure,mechanical properties and precipitates of 600 MPa grade rebars were studied by using pilot test,metallographic observation,tensile test,thermodynamic calculation and transmission electron microscopy. The results show that the tested steels are composed of ferrite and pearlite,in which the content range of pearlite is 33%-45%. For vanadium microalloyed steel,interphase precipitation strengthening effect of V can be promoted and the yield strength of tested steels can be increased with increasing V content and decreasing finishing rolling temperature. The temperature of terminated cooling should be more than 700 °C when the water cooling is used. When niobium is added to the steel,more coarse( Nb,V) C,N precipitates are generated at high temperature,so that the solid solubility of precipitated phases of vanadium is reduced and the precipitation strengthening effect of vanadium is weakened.     

冷轧压下量和退火温度对Ti-IF钢性能的影响

采用正交试验法研究了冷轧压下量(65%～80%)和退火温度(660～780℃)对Ti-IF钢(/%:0.02C、0.012Si、0.10Mn、0.013P、0.011S、0.064Ti、0.0020N)组织、力学和成形性能的影响。试验结果表明,≥700℃退火Ti-IF钢再结晶基本完成,当压下量75%700℃退火时,该钢具有较好的综合性能:屈服强度120 MPa,屈强比0.38,应变硬化指数n值0.25,塑性应变比r值1.65。     

Nb-Ti微合金化对热轧0.5~0.7Cr铲斗刀板型钢组织和性能的影响

试验0.5~0.7Cr铲斗刀板型钢（/%:0.22~0.30C,0.25~0.45Si,0.95~1.20Mn,0.006~0.009P,0.008~0.010S,0.5~0.7Cr,0.015~0.065Nb,0~0.040Ti）由50kg真空感应炉熔炼,热轧成16mm厚板,终轧温度850~900℃,空冷。通过光学显微镜、扫描、透射电镜和力学性能测试研究了Nb-Ti含量（0.015Nb,0.035Nb-0.010Ti,0.065Nb-0.040Ti）对热轧态铲斗刀板钢组织和力学性能的影响。结果表明,试验钢组织为F+P,随Nb-Ti含量增加,钢板的晶粒细化,珠光体片层间距降低,（Nb,Ti）C和（Nb,Ti）(C,N)析出物增多,强度增加,0.065Nb-0.040Ti钢板的力学性能为屈服强度632MPa,抗拉强度916MPa,延伸率17.7%,K_AV40 J,HB硬度值234。     

CSP生产C-Mn钢薄带组织与表面裂纹研究

在武钢CsP生产线上,通过控轧控冷工艺生产低成本低碳C-Mn钢薄板.结果表明,生产出的薄板屈服强度大于313 MPa,抗拉强度高于400MPa,伸长率超过37%,屈强比低于0.83,冷弯性能良好,满足塑性要求,但常出现表面裂纹.从热力学角度分析出尺寸大于83nm的硬脆粒子会引起裂纹,而钢中析出物尺寸约为30nm,不足以...     

控轧控冷工艺对高强度锚杆钢组织和性能的影响

随着矿井深度的增加,对锚杆支护强韧性的要求越来越高,为了应对这一情况,需要研发出更高强度的锚杆钢。利用锚杆钢研究了轧制工艺、冷却工艺与珠光体、铁素体相比例,析出相析出行为及力学性能的关系。研究结果表明,在中轧后、精轧前采用适当水冷+回复段处理的复合工艺可使晶粒更细小、组织更均匀。对超高强度锚杆钢进行热压缩变形试验,由热模拟试验结果确定相转变温度为A_c1=737 ℃、A_c3=886 ℃。最终筛选出入精轧温度为810 ℃、回复段温度为800 ℃时,可获得的晶粒尺寸达4 μm,珠光体体积分数为66.8%,铁素体体积分数为33.2%,珠光体片层间距达200 nm;另外调整V、Cr、N等析出以提高锚杆钢的强韧性,较低的回复温度有利于细小、弥散、V(C/N)析出相的析出,V(C/N)的析出可进一步改善锚杆钢的力学性能。由该控轧控冷工艺轧制的锚杆钢屈服强度为780 MPa、抗拉强度为930 MPa、硬度为291HV、伸长率为20%。     

Deformation Behavior of Fe-36Ni Steel during Cryogenic (123-173 K) Rolling

Microstructural evolution and mechanical properties of cryogenic rolled Fe-36Ni steel were investigated. The annealed Fe-36Ni steel was rolled at cryogenic temperature( 123-173 K) with 20%- 90% rolling reduction in thickness.The deformation process was accompanied by twinning at cryogenic temperature,and the mean thickness of deformation twins was about 200 nm with 20% rolling reduction. When the rolling reduction was above 40%,twinning was suppressed due to the stress concentration in the tested steel. Deformation microstructure of Fe-36Ni steel consisted of both twin boundaries and dislocations by cryogenic rolling( CR),while it only contained dislocations after rolling at room temperature( RT). The tensile strength of Fe-36Ni steel was improved to 930 MPa after 90% reduction at cryogenic temperature,while the tensile strength after 90% reduction at RT was only 760 MPa. More dislocations could be produced as the nucleation sites of recrystallization during CR process.