粘土矿物负载型复合催化剂的研究进展

利用粘土矿物的结构和物理化学特性负载纳米颗粒以制备高性能的功能矿物材料,是目前材料科学、矿物加工、化学工程等多学科交叉的研究前沿。粘土矿物大的比表面积、丰富的孔道结构和优越的离子交换性能为其用于矿物型复合催化材料提供了充分的保证。综述了国内外粘土矿物负载型复合催化剂的最新进展,整理分析了凹凸棒石、高岭土、蒙脱石、海泡石、硅藻土、沸石等多种复合催化剂的制备方法、应用方向及性能评价,并结合目前存在的一些问题提出见解,为深入研究提供了一定的思路。     

矿物基负离子发生材料的结构和组成特征

用X射线粉末衍射仪、X射线能谱仪和等离子体原子发射光谱仪分析了多种矿物基材料的主物相结构和元素组成,并用离子检测仪测定了各材料的负离子发生量.研究表明,具有负离子发生功能的矿物基材料可以由具有明显压电、热电效应的矿物组成,也可以由含有一定量稀土元素和天然原生放射性核素的矿物组成.矿物中适量天然原生放射性核素的存在对于制备高性能的矿物基负离子发生材料是有益的.     

合理掺入矿物掺合料对提高混凝土性能的可行性研究

利用"矿物掺合料在提高混凝土性能的应用"课题的研究成果,在施工实践中进行了大面积地推广应用,取得了显著的经济和社会效益。矿物掺合料的应用、制备已牵涉到水泥基材料科学研究的各个方面。在现代混凝土技术中,经过一定质量控制的矿物掺合料已成为高性能混凝土不可或缺的组分之一。本文通过对矿物掺合料研究历史和研究现状的分析,探讨了当前研究的主要缺陷及存在的问题,并展望了下一步的研究方向。     

矿物掺合料研究进展及存在的问题

矿物掺合料的应用、制备已牵涉到水泥基材料科学研究的各个方面.在现代混凝土技术中,经过一定质量控制的矿物掺合料已成为高性能混凝土不可或缺的组分之一.通过对矿物掺合料研究历史和研究现状的分析,探讨了当前研究的主要缺陷及存在的问题,并展望了下一步的研究方向.     

微粉矾渣在高性能混凝土中的应用

随着我国经济建设的蓬勃发展 ,高层的、高质量的建筑物日益增多 ,这对主要建筑材料———混凝土提出更高的要求。高性能混凝土正是这种社会需求的产物。所谓高性能混凝土是指混凝土具有高强度、高耐久性、易施工和良好的体积稳定性。混凝土要达到高性能的主要技术手段是采用极少量的高效减水剂和适量的微粉非金属矿物作为掺合料 (包括微粉高炉渣、矾渣、锂渣和磷渣 )。采用高效减水剂能降低水灰比 ,增加塌落度 ,赋予混凝土高的密实度和流动性 ,从而提高混凝土的抗压强度和施工性能。而微粉非金属矿物能填充水泥颗粒之间的空隙 ,并参与水泥的…     

拜耳法低铁赤泥在电石渣-脱硫石膏体系中的水化硬化特性

为促进拜耳法赤泥在胶凝材料中的大宗化和高附加值利用,以山西孝义拜耳法低铁赤泥为研究对象,借助XRD、FTIR、SEM、ICP-OES等现代测试手段,研究了拜耳法赤泥在电石渣-脱硫石膏体系中的水化硬化特性。研究表明,拜耳法低铁赤泥具有潜在活性,氧化铝为其活性的最主要来源,在电石渣-脱硫石膏体系中,通过电石渣的补钙作用和脱硫石膏的促进激发作用,赤泥中的氧化铝得以有效激发,其水化产物主要为钙矾石、C-S-H凝胶、水化硫铁酸钙、钙霞石、无水芒硝和氢氧化铝。     

插层法制备膨润土-有机复合高性能吸水材料的试验研究

研究了膨润土插层聚合制备吸水材料的过程中各因素对膨润土-有机复合高性能吸水材料吸水性能的影响，探索低成本、工艺简单的方法制备出高性能吸水材料，通过XRD、SEM对材料进行了表征，该高性能吸水材料的推广将使有助于新疆优势矿产资源得以利用，可以推动当地的经济发展。     

镍渣资源化利用现状及发展趋势分析

镍渣含Fe 40%~45%,SiO_232%~36%,MgO 1%~11%,CaO 1%~3%(质量分数),并含少量的镍、铜、钴等有价金属,是重要的二次资源。介绍了典型镍渣成分及物相,总结了镍渣提取有价金属、作井下填充材料、生产微晶玻璃、制备建材等资源化利用工艺的技术要点,分析了现有工艺存在的问题,提出了镍渣直接还原提铁及协同制备胶凝材料的绿色利用思路,介绍了初步研究结果,探讨了进一步资源化的方向。     

锂渣粉作为辅助胶凝材料在水泥基材料中的研究进展

锂渣是生产锂盐过程中产生的工业废渣,其含有大量活性SiO_2和Al_2O_3,有作为辅助胶凝材料的应用潜力。从物理性质、化学成分与矿物组成、活性评价与活性激发等方面介绍了锂渣自身的物理化学特性和水化活性潜质。从力学性能、工作性、耐久性、水化反应与微结构四方面重点综述了锂渣粉对水泥基材料各方面性能的影响,并进行了理论分析与总结。最后指出锂渣粉用于水泥基材料需要在活性提高、高含量SO_3和多孔结构的改善及利用等方面加强研究。     

混凝土高性能减水剂的绿色与节能制备方法研究进展

随着“双碳”战略目标和“节能环保”理念的实施，近年来基于绿色材料代替石化原料以及利用新技术手段实现高性能减水剂的节能制备与应用得到了显著进步和飞速发展，展现出巨大的应用潜能。为此，文中从绿色制备及低能耗合成技术两大方面系统综述了高性能减水剂的绿色与节能制备的优势特点，归纳了化学方法和技术原理，分析了其应用效果并展望了未来发展方向，为高性能减水剂材料的绿色与节能制备方法的研究开发提供设计依据。     

The Research of Anti-Wear Properties of Organomolybdenum Compounds in the Engine Oils

A four-ball tester was used to evaluate the anti-wear performance of three kinds of organomolybdemun compounds in the engine oils, i. e., molybdenum dialkyldithiophosphate (MoDDP), molybdenum dialkyldithiocarbamate ( MoDTC), and sulphur and phosphorus freeorganomolybdeum (Molybdate). The results indicate that a low concentration of MoDDP doesn' t improve the anti-wear properties of the commercial engine oils, but a high concentration of MoDDP can obviously improve the anti-wear properties and the load-carrying capacity of the engine oils. MoDTC doesn' t improve the antiwear properties of the engine oils, but worsens the anti-wear properties of the oils. Signifi can timprove ment of frictional and wear characteristics is obtained with Molybdate added in the commercial engine oils and the formulated oils.     

Certification Institutions Expected to Update and Transfer Information on Present Standards

Standards are the basis for production enterprises to organize production, ex-factory inspection, trade (delivery) and technical exchanges, product certification, quality arbitration and supervision.……     

Optimum-Simulation von Ernteprozessen

Zusammenfassung Bei der Gestaltung von Ernteprozessen — beispielsweise des Prozesses Mähdrusch, Körnertransport und -abnahme — als transportverbundene Fließarbeitsverfahren mit mindestens zwei verschiedenen Arbeitsmitteln gibt es einen großen Optimierungsspielraum. Solche Prozesse sind mehrstufige Bedienungsprozesse mit gemischter Anordnung der Bedienungseinrichtungen. Außerdem besitzen sie stark ausgeprägte räumliche Aspekte. Es wird vor allem gezeigt, welche Merkmale solcher Prozesse in Simulationsmodellen abgebildet sein müssen, welche Zielgrößen in Abhängigkeit von welchen Einflußgrößen unter Berücksichtigung welcher Prozeßbedingungen ermittelt werden sollten und wie der Bewertungsprozeß zur Ermittlung der gewünschten Informationen gestaltet werden muß.     

Certification Becomes Important for the I Quality; and Safety Supervision of the Chinese Liquor Sector

The end of 2007, over 200 unit products of more than 80 Chinese firms have passed the quality grade certification for liquor products. These products involve distilled spirits, beer, wine, yellow wine, fruit syrup wine and others, and cover over 80% of the national top-branded liquor products.……     

Deposition and Coating Properties on CVD Tungsten

Surface characterization and microstructure studies are performed on chemical vapor deposited (CVD) tungsten coating. There is about 2 μm thickness diffusion layer of tungsten in the molybdenum substrate. The thermal shock test shows tungsten coating has good adhesion with molybdenum substrate, but the elements of oxygen and carbon in the tungsten coating have the bad affection to the adhesion. The result of high-temperature diffusion experiment is the diffusion rate from molybdenum substrate to tungsten coating is faster.     

Analysis of marine hydrobiont lipid extracts as possible cryoprotective agents

We studied a combined effect of the cryoprotectants both of lipid and carbohydrate origin at the presence of DMSO or without it on cell viability and the RNA synthesis in the embryonic mollusc and echinoderm cell cultures obtained at different developmental stages. Cryoprotective properties of exogenous lipids correlated with their thermotropic behavior. Lipid extracts from marine hydrobiontes, which thermal transitions are characterized by relatively small part of calorimetric thermogram area lying at temperatures above 0 °C (6–18%), were found to possess a considerable cryoprotective activity. The results are discussed in relation to the prediction of the cryoprotective activity of lipid extracts for marine animal cells. In addition, it was found that marine invertebrate cells can be cryopreserved without DMSO at the presence of trehalose and lipid extracts of some marine hydrobiontes.     

Low-Temperature Properties of Silver

Pure silver is used extensively in the preparation of high-temperature superconductor wires, tapes, films, and other configurations in which the silver not only shields the superconducting material from the surrounding materials, but also provides a degree of flexibility and strain relief, as well as stabilization and low-resistance electrical contact. Silver is relatively expensive, but at this stage of superconductor development, its unique combination of properties seems to offer the only reasonable means of achieving usable lengths of conductor. In this role, the low-temperature physical (electrical, thermal, magnetic, optical) and mechanical properties of the silver all become important. Here we present a collection of properties data extracted from the cryogenic literature and, to the extent possible, selected for reliability.     

Early ironwork in Biscay: Survey,excavation, experimentation and materials characterization. An integral study of the mountainside ironworks (ferrerías de monte or “haizeolak”)

ABSTRACT

The production of iron in Biscay (Basque Country, Spain) has been a hallmark of this territory of the North of the Iberian Peninsula throughout its history. The Archaeology team of the Basque Country Mining Museum has spent 13 years, so far, studying the origins of this activity through the evidences left at the old pre-hydraulic iron production workshops known as mountainside ironworks (ferrerías de monte) or haizeolak. It has catalogued 170 archaeometallurgical sites of this type in Biscay, and the archeological excavation of some of them has led to the knowledge of the different stages of the production process that took place in these workshops. The team has also experimentally reproduced the work carried out in a mountainside ironworks from the High Middle Ages, and it has currently started the characterization process of this type of activity through the study of the collected materials.     

Brainstorming for ISO Strategy 2016-2020

正Responding to ISO’s appeal for survey for the to-be-developed ISO Strategy Plan for 2016-2020,SAC hosted a special workshop over the needs and comments of various fi elds on June 8 in Beijing.The workshop was attended by ISO President-elect and Ansteel General Manager Zhang Xiaogang,SAC Vice-Administrator Yu Xinli,and 30 experts from     

CNAS Passes APLAC's PTP Review

正The review group of Asia Pacific Laboratory Accreditation Cooperation(APLAC)carried out a 4-day peer review of the proficiency testing provider(PTP)for China National Accreditation Service for Conformity Assessment(CNAS)from July 28 to 31,2014.CNAS passed the PTP review with excellent performance.Two senior peer reviewers of APLAC made a comprehensive,rigorous and detailed review of CNAS’s PTP accreditation activities,and made the on-spot inspection of the review groups in Shanghai and Shenzhen respectively.