共查询到20条相似文献,搜索用时 15 毫秒
1.
实验室常用静力称重法对微量液体容量进行检测,该方法在1μL容量的精确度达到2.18%,重复性为1.85%,但该方法无法在实验室外进行。现有的光学测量微量液体容量法的在1μL的精度为6.09%,重复性为1.31%。该法可实现在线检测,但其精度不如静力称重法。对光学测量微量液体容量的方法进行研究分析,提出了一种新的标定容量参照标准的方法,该标定方法将静力称重法与光学测量法两者结合,以静力称重法容量测量结果为参照标准,代替光学法原先的标准液。新的标定方法在原理上将参照标准由点扩展到线,可将光学测量法在10μL点的精度提高到2.014%,重复性1.30%。 相似文献
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冻干工艺中升华结束点和残余水分测量方法简述 总被引:9,自引:0,他引:9
升华结束点和残余水分的在线测定是冷冻干燥科学实验及其工艺中的重点和难点 ,着重对其常用确定方法理论模型法、产品温度响应法、压力升高法、湿度传感器法、残余气体分析仪、脉冲核磁共振法 (NMR)、称重法 (重量传感器法 )等 7种方法加以总结和概括。指出脉冲核磁共振法和湿度传感器法将为冻干理论研究和实验研究拓展新思路 相似文献
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This paper concerns with a combination method of the boundary element method and the finite element method for elastic-plastic
analyses. The combination method proposed here is based on the substructure method using the conjugate gradient method. This
combination method has the advantage of saving CPU time and memory storage size over the finite element method. The combination
method is applied to a J-integral analysis of a crack in an adhesive joint. The effect of bond thickness on the J-integral
is discussed. 相似文献
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纳米Fe3O4磁性颗粒的制备进展 总被引:1,自引:0,他引:1
概述了纳米Fe3O4磁性颗粒的制备工艺:机械球磨法、微乳液法、水热法、微乳-水热法、溶胶-凝胶法、沉淀法(共沉淀法、氧化沉淀法、超声沉淀法)、水解法等,归纳了各种制备方法的特点,并对其前景进行了简要评述. 相似文献
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超细NiO粉体的制备及其应用研究进展 总被引:2,自引:0,他引:2
综述了超细NiO粉体近年来的制备方法及其特点(主要有固相反应法、沉淀法、微乳液法、喷雾热解法、热分解法和电化学法),介绍了超细NiO粉体的应用现状. 相似文献
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本文研究了乙酸纤维滤膜、混合纤维滤膜和玻璃纤维滤膜对浮游植物叶绿素a测定结果的影响,比较了丙酮浸提法、丙酮研磨法、乙醇法和热乙醇法四种方法的稳定性和可替代性。研究表明,三种滤膜对丙酮浸提法和研磨法的测定结果无显著影响,可选择任一种滤膜。丙酮浸提法和研磨法测定结果无显著差异,可相互替换,丙酮研磨法平均损耗率为32.91%,误差较大。乙醇法和热乙醇法可相互替换,但热乙醇法的平行性较差,加热过程难控制。丙酮法测定结果普遍偏高,其中丙酮浸提法的结果明显高于乙醇法,鉴于数据的可比性和简便操作,可采用丙酮浸提法,而乙醇法值得在日后水质监测中推广。 相似文献
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提出边界元-有限元-统计能量(BEM+FEM+SEA,简称BFS)混合方法模拟驻波管,即BFS驻波管模拟法,计算材料的隔声量。探究了不同边界条件对BFS驻波管模拟法隔声量计算结果的影响;通过与有限元(FEM)驻波管模拟法、有限元-统计能量(FEM+SEA,简称FS)混响室模拟法以及瑞利-李兹理论法所得隔声量对比,验证BFS方法的有效性和精度。结果表明,BFS驻波管模拟法能够较为准确地模拟驻波管,得到待测材料的隔声量,相对于有限元(FEM)驻波管模拟法,能够有效解决震荡问题,减小计算量,提升计算速度,可适用于全频段声学材料性能的计算和评估,弥补实验手段耗时费力的缺点,尤其是在新产品的开发阶段具有一定的实际意义。 相似文献
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A Numerical-analytic Method for Quickly Predicting Springback of Numerical Control Bending of Thin-walled Tube 总被引:2,自引:0,他引:2
Mei ZHAN He YANG Liang HUANG 《材料科学技术学报》2006,22(5):713-720
Springback is one of important factors influencing the forming quality of numerical control (NC) bending of thin-walled tube. In this paper, a numerical-analytic method for springback angle prediction of the process was put forward. The method is based on springback angle model derived using analytic method and simulation results from three-dimensional (3D) rigid-plastic finite element method (FEM). The method is validated through comparison with experimental results. The features of the method are as follows: (1) The method is high in efficiency because it combines advantages of rigid-plastic FEM and analytic method. (2) The method is satisfactory in accuracy, since the field variables used in the model is resulting from 3D rigid-plastic FEM solution, and the effects both of axial force and strain neutral axis shift have been included. (3) Research on multi-factor effects can be carried out using the method due to its advantage inheriting from rigid-plastic FEM. The method described here is also of general significance to other bending processes. 相似文献
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田菁胶是从田菁种子胚乳中提取的一种天然多糖类高分子有机物。天然的化学结构反映出的理化性质限制了其应用和推广。化学结构式的修饰改进是扩大其应用的有效手段。修饰改进后的田菁胶无毒、无污染,在石油开采、煤开采、纺织、印刷、造纸和食品等领域得到了广泛应用。文中对羧甲基法、羟乙基法、羟丙基法、交联法、羟烷基-羧甲基法、羧甲基-羟烷基法、阳离子法、酶解法、氧化法和两性法等田菁胶化学结构式的主要修饰改进方法进行了详述。总结了修饰改进技术注意事项,并对前景进行了展望。 相似文献
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本文采用碘显色法、双酶水解-高效液相色谱法和酸水解法对13种肉松样、自制肉松样和加标样进行淀粉含量测定,分析结果,并进一步对肉松制品淀粉含量测定中多糖、抗性糊精等可能干扰物质进行研究。结果表明:采用双酶水解-高效液相色谱法和淀粉显色相结合,可以有效地排除多糖类物质的干扰,避免测定假阳性,从而真实准确地反应肉制品中淀粉含量。 相似文献
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研究了石油储罐罐底腐蚀声发射源的定位方法.针对有限空间液态场中水声信号的多途效应严重影响声源目标定位问题,提出一种基于粒子滤波的到达时间差(TDOA)声源定位方法,充分考虑广义互相关结果中多途效应导致的多个峰值,采用高斯似然函数进行重要性采样,实现对多途效应影响的抑制.水池实验结果表明这种方法比传统的Chan方法具有更高的定位准确性和精度,定位结果的均方根误差(RMSE)为Chan方法的10%,提高了定位性能. 相似文献
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A boundary density evolutionary topology optimization of continuum structures with smooth boundaries
Xueping Li Chuhao Qin Peng Wei Cheng Su 《International journal for numerical methods in engineering》2022,123(1):158-179
Based on the variable density method, this article proposes a boundary density evolutionary topology optimization method. The method uses a material interpolation model without penalization. Combined with the density grading filtering method, an optimal topology with only 0/1 cells can be obtained. Compared with the solid isotropic microstructures with penalization method (SIMP), no penalty factor is required in the material interpolation model; compared with the evolutionary structural optimization method (ESO), intermediate-density elements are allowed in the optimization process, but the concept of gradually removing the low-utilization materials near the boundary in the ESO method is retained. After the optimal result is obtained, the structural boundary element is processed by the level set of nodal strain energy, and the optimization result with smooth boundaries similar to the level set method (LSM) can be obtained. The proposed method has the superiority of the variable density method, and it also combines the advantages of the evolutionary method and the level set method, so which is named as boundary density evolution (BDE) method. The four static and one dynamic optimization examples illustrate the stability and efficiency of the proposed method. 相似文献
19.
Han-Taw Chen Cha'O-Kuang Chen 《International journal for numerical methods in engineering》1988,26(6):1433-1447
The new method involving the combined use of the Laplace transform and the finite difference method is applicable to the problem of time-dependent heat flow systems. The present method removes the time derivatives from the governing differential equation using the Laplace transform and then solves the associated equation with the finite difference method. The transformed temperature is inverted numerically by the method of Honig and Hirdes to obtain the result in the physical quantities. The present results are compared in tables with exact solutions and those obtained from the combined use of the Laplace transform and the finite element method. It is found that the present method is reliable and efficient. 相似文献