铝合金钻杆旋转弯曲疲劳断口特征

首先对铝合金钻杆进行了不同应力幅值的旋转弯曲疲劳试验,然后采用扫描电镜观察其断口微观形貌特征。结果表明:在170 MPa低应力下,铝合金钻杆的疲劳断口可分为疲劳源区、裂纹扩展区及瞬断区3个区域,微裂纹在试样次表面相界处萌生,裂纹稳态扩展区面积较大,占60%以上;在290 MPa高应力下,铝合金钻杆的疲劳断口上有多个疲劳源区,微裂纹于试样表面或近表面位置形核,裂纹扩展区面积仅占15%~30%。对于同一试样,随着裂纹的扩展,断口上疲劳滑移台阶变宽,疲劳条带逐渐清晰;对于不同试样,随着应力的提高,裂纹扩展速率增大,疲劳条带间距变宽,更易出现二次疲劳裂纹,断口上裂纹扩展区面积明显减小,相应的疲劳寿命也大幅降低。     

室温大气环境下峰时效态3J21合金疲劳行为

在MTS万能实验机上对室温大气环境下峰时效态3J21合金的疲劳行为进行研究,并采用扫描电镜(SEM)对宏观断口及微观断口进行分析。结果表明,峰时效态3J21合金的疲劳裂纹主要呈穿晶扩展,沿晶扩展的所占比例较小,疲劳裂纹萌生寿命较低,扩展路径比较平直,扩展速率较大,裂纹扩展抗力较小,疲劳寿命较低;峰时效态3J21合金疲劳断口由疲劳源、疲劳裂纹扩展区和瞬断区组成。在低速扩展区,峰时效态断口呈现冰糖状花样,在中速扩展区未看到长的疲劳条纹,仅发现个别细且短小的疲劳条纹,瞬断区可观察到二次裂纹、准解理和韧窝。     

18CrNiMo7-6合金钢的弯曲微动疲劳特性

对18CrNiMo7-6合金钢进行弯曲微动疲劳实验,建立弯曲微动疲劳S-N曲线,并对实验结果进行分析。结果表明:该合金钢的弯曲微动疲劳S-N曲线不同于中碳钢材料,也不同于常规弯曲疲劳,而是呈"ε"型曲线特征。随着弯曲疲劳应力的增加,微动运行区域由部分滑移区向混合区和滑移区转变,损伤区的磨损机制以剥层、磨粒磨损和氧化磨损为主。在混合区内,裂纹最易萌生和扩展,且裂纹均萌生于材料接触区次表面。受接触应力和弯曲疲劳应力影响,弯曲微动疲劳裂纹的萌生和扩展可分为三个阶段:初期,在接触应力控制下,裂纹萌生于次表面;随后,裂纹受接触应力和弯曲疲劳应力共同控制,转向更大角度方向扩展;最后,裂纹完全受弯曲疲劳应力控制而垂直于接触表面扩展,直至断裂失效。     

纯铜低周疲劳中的温度响应与微观形貌变化

为了研究纯铜在低周疲劳中的温度响应与微观形貌,借助于红外热像仪及远距离高倍显微镜同步监测工业纯铜的表面疲劳变化,同时运用扫描电子显微镜(SEM)对试样断口进行微观分析.研究结果表明:试样表面温度的变化与表面微观形貌的变化具有明显的相关性,并受应力水平及加载频率的影响,表面最高温升与加载频率呈线性关系;试样断口出现明显的裂纹扩展区和瞬断区,且随着应力水平及加载频率的增加而形成较大的瞬断区及较多的韧窝.     

载荷方向和焊缝余高对氩弧焊缝疲劳性能的影响

采用疲劳寿命测试和观测断口方法,研究焊接方向和焊缝余高对TC2钛合金氩弧焊缝疲劳性能的影响。结果表明:同种焊接方向,保留焊高试件的疲劳寿命低于去焊高试件;同种焊缝余高处理方式,斜焊试件的疲劳寿命高于直焊试件。去焊高试件于气孔缺陷处萌生裂纹,保留焊高试件疲劳裂纹起源于焊趾。裂纹扩展初期,裂纹均在焊缝内扩展,有明显的疲劳条带;扩展后期,斜焊试件裂纹穿过焊缝进入母材,存在典型的韧性疲劳条带。直焊试件疲劳瞬断区韧窝少而浅;斜焊试件在母材瞬断,韧窝多且密。     

Z6CNT18-10奥氏体不锈钢扩散管在蒸汽疏水环境中的疲劳开裂特征

采用金相显微镜、扫描电镜、X射线衍射仪等对Z6CNT18-10奥氏体不锈钢扩散管在蒸汽疏水环境下的疲劳断口特征进行了研究。结果表明:与常见的疲劳裂纹常起源于外壁不同,在蒸汽疏水环境下的奥氏体不锈钢扩散管的疲劳裂纹起源于内壁,裂纹源处存在明显的氧化现象;裂纹附近的显微组织中存在一定量的驻留滑移带,疲劳条带间距很窄,几乎不存在瞬断区,属于高周疲劳。     

S135钻杆钢的拉扭复合加载疲劳行为

采用疲劳实验和回归分析相结合的方法,研究了S135钻杆钢在拉扭复合加载条件下的疲劳行为,并对疲劳断口进行了微观分析。结果表明:当τa/σeq=0.7时,由拉扭应力幅对应的当量应力表示的疲劳寿命公式可很好地描述S135钻杆钢的拉扭疲劳寿命规律;疲劳断口由疲劳源区、疲劳裂纹稳定扩展区和快速瞬断区组成,疲劳裂纹从试样表面萌生,并向试样内部扩展,且常为多疲劳源,不同疲劳源断口的连接和复合加载形成所谓的"屋脊"状特征;拉扭疲劳断裂试样裂纹源区的微观断口特征为明显的河流花样,裂纹扩展区的微观断口特征为疲劳条带与涟波状花样。     

多轴复杂应力形式下TB6高强钛合金耳片的微动疲劳断裂研究

本实验研究了TB6高强钛合金在拉-扭多轴应力条件下的微动疲劳断裂机理,并结合宏微观观察、残余应力测试、计算机模拟分析了不同工艺条件的耳片在拉-扭疲劳试验应力下的微动疲劳寿命差异,研究了微动疲劳裂纹的萌生及扩展特性,揭示了耳片裂纹萌生机制。结果表明:二次挤压耳片的断口扩展区面积比例较大,说明其拉-扭疲劳扩展更为充分。经二次挤压后,耳片的拉-扭微动疲劳总寿命得到延长,且裂纹萌生寿命均占总寿命的95%以上;二次挤压后耳片的裂纹萌生驱动力较低,呈现较高的裂纹萌生抗力。各断口均起源于耳片内孔微动磨损印迹较重处,大面积连续片状的微动磨损印迹表明二次挤压后的钛合金微动疲劳敏感性大大降低。经挤压强化后,孔壁形成了较高幅值的残余压应力层和组织强化层,可以有效地抑制裂纹的萌生和扩展。耳片内孔微动磨损层的形成是机械诱导机制和热诱导机制共同作用的结果,其最终磨损形式为疲劳磨损。     

2A12铝合金的多轴加载疲劳行为

采用SDN100/1000电液伺服拉扭复合疲劳试验机对2A12铝合金进行多关键参数的多轴疲劳性能研究,通过对断口的微观分析探究疲劳失效机理。结果表明:等效应力加载条件下,随拉扭相位差的增加疲劳寿命降低,0°相位差下断面裂纹源区能观察到轮胎状、鱼骨状以及钟乳石状的特殊形貌,裂纹扩展区存在二次裂纹和模糊的疲劳条带;分别改变拉、扭平均应力,多轴疲劳寿命均降低,裂纹源区能看到白色絮状的氧化物,瞬断区存在二次裂纹和剪切型韧窝;不同加载波形条件下,正弦波对应最长的多轴疲劳寿命,三角波次之,方波时最短且体现出最大的结构耗能。低-高两级加载条件下,材料产生"锻炼效应"。     

应力幅对退火态Mg-3Al-2Sc合金疲劳行为的影响

在不同应力幅下对退火处理后的Mg-3Al-2Sc合金进行应力控制的疲劳实验,研究应力幅对合金的裂纹扩展行为和断裂机制的影响。结果表明:在12～75MPa应力范围内,当控制应力比为0.2,随着应力幅增加,裂纹扩展速率增加,Mg-3Al-2Sc合金的疲劳断裂寿命降低。在裂纹萌生区合金主要表现为解理断裂机制,进入裂纹稳定扩展阶段的疲劳断裂主要为准解理断裂。而在瞬断区,低应力幅时主要表现为准解理断裂,高应力幅时主要表现为微孔聚合断裂。     

The Research of Anti-Wear Properties of Organomolybdenum Compounds in the Engine Oils

A four-ball tester was used to evaluate the anti-wear performance of three kinds of organomolybdemun compounds in the engine oils, i. e., molybdenum dialkyldithiophosphate (MoDDP), molybdenum dialkyldithiocarbamate ( MoDTC), and sulphur and phosphorus freeorganomolybdeum (Molybdate). The results indicate that a low concentration of MoDDP doesn' t improve the anti-wear properties of the commercial engine oils, but a high concentration of MoDDP can obviously improve the anti-wear properties and the load-carrying capacity of the engine oils. MoDTC doesn' t improve the antiwear properties of the engine oils, but worsens the anti-wear properties of the oils. Signifi can timprove ment of frictional and wear characteristics is obtained with Molybdate added in the commercial engine oils and the formulated oils.     

Certification Institutions Expected to Update and Transfer Information on Present Standards

Standards are the basis for production enterprises to organize production, ex-factory inspection, trade (delivery) and technical exchanges, product certification, quality arbitration and supervision.……     

Certification Becomes Important for the I Quality; and Safety Supervision of the Chinese Liquor Sector

The end of 2007, over 200 unit products of more than 80 Chinese firms have passed the quality grade certification for liquor products. These products involve distilled spirits, beer, wine, yellow wine, fruit syrup wine and others, and cover over 80% of the national top-branded liquor products.……     

Deposition and Coating Properties on CVD Tungsten

Surface characterization and microstructure studies are performed on chemical vapor deposited (CVD) tungsten coating. There is about 2 μm thickness diffusion layer of tungsten in the molybdenum substrate. The thermal shock test shows tungsten coating has good adhesion with molybdenum substrate, but the elements of oxygen and carbon in the tungsten coating have the bad affection to the adhesion. The result of high-temperature diffusion experiment is the diffusion rate from molybdenum substrate to tungsten coating is faster.     

Analysis of marine hydrobiont lipid extracts as possible cryoprotective agents

We studied a combined effect of the cryoprotectants both of lipid and carbohydrate origin at the presence of DMSO or without it on cell viability and the RNA synthesis in the embryonic mollusc and echinoderm cell cultures obtained at different developmental stages. Cryoprotective properties of exogenous lipids correlated with their thermotropic behavior. Lipid extracts from marine hydrobiontes, which thermal transitions are characterized by relatively small part of calorimetric thermogram area lying at temperatures above 0 °C (6–18%), were found to possess a considerable cryoprotective activity. The results are discussed in relation to the prediction of the cryoprotective activity of lipid extracts for marine animal cells. In addition, it was found that marine invertebrate cells can be cryopreserved without DMSO at the presence of trehalose and lipid extracts of some marine hydrobiontes.     

Low-Temperature Properties of Silver

Pure silver is used extensively in the preparation of high-temperature superconductor wires, tapes, films, and other configurations in which the silver not only shields the superconducting material from the surrounding materials, but also provides a degree of flexibility and strain relief, as well as stabilization and low-resistance electrical contact. Silver is relatively expensive, but at this stage of superconductor development, its unique combination of properties seems to offer the only reasonable means of achieving usable lengths of conductor. In this role, the low-temperature physical (electrical, thermal, magnetic, optical) and mechanical properties of the silver all become important. Here we present a collection of properties data extracted from the cryogenic literature and, to the extent possible, selected for reliability.     

Early ironwork in Biscay: Survey,excavation, experimentation and materials characterization. An integral study of the mountainside ironworks (ferrerías de monte or “haizeolak”)

ABSTRACT

The production of iron in Biscay (Basque Country, Spain) has been a hallmark of this territory of the North of the Iberian Peninsula throughout its history. The Archaeology team of the Basque Country Mining Museum has spent 13 years, so far, studying the origins of this activity through the evidences left at the old pre-hydraulic iron production workshops known as mountainside ironworks (ferrerías de monte) or haizeolak. It has catalogued 170 archaeometallurgical sites of this type in Biscay, and the archeological excavation of some of them has led to the knowledge of the different stages of the production process that took place in these workshops. The team has also experimentally reproduced the work carried out in a mountainside ironworks from the High Middle Ages, and it has currently started the characterization process of this type of activity through the study of the collected materials.     

Optimum-Simulation von Ernteprozessen

Zusammenfassung Bei der Gestaltung von Ernteprozessen — beispielsweise des Prozesses Mähdrusch, Körnertransport und -abnahme — als transportverbundene Fließarbeitsverfahren mit mindestens zwei verschiedenen Arbeitsmitteln gibt es einen großen Optimierungsspielraum. Solche Prozesse sind mehrstufige Bedienungsprozesse mit gemischter Anordnung der Bedienungseinrichtungen. Außerdem besitzen sie stark ausgeprägte räumliche Aspekte. Es wird vor allem gezeigt, welche Merkmale solcher Prozesse in Simulationsmodellen abgebildet sein müssen, welche Zielgrößen in Abhängigkeit von welchen Einflußgrößen unter Berücksichtigung welcher Prozeßbedingungen ermittelt werden sollten und wie der Bewertungsprozeß zur Ermittlung der gewünschten Informationen gestaltet werden muß.     

Mechanism Study on the Wear of CrAlTiN Coated High-Speed Steel Twist Drills Under Dry Cutting Conditions

As demands about environment protection are growing up, dry cutting technology is getting more and more concerns from all over the world. Main works performed here are study on dry cutting performances and wear mechanisms of M2high-speed steel (HSS) twist drills with CrAlTiN multicomponent coatings, which was deposited using magnetron sputter ion plating system, in drilling 45 and 30CrMnSiA steel, and their comparisons to those in drilling the same steel but using monolayer CrN and commercial TiN coated drills. Drilling performances of drills are evaluated mainly through the measurements of width on outer corner flank land and the cutting forces. Results show that performances of CrAlTiN coated drills are better than those of monolayer CrN and TiN coated drills. In drilling 45 and 30CrMnSiA steel, the average tool life of the CrAlTiN coated drills are 17.2 and 11.8 times higher than those of the uncoated drills. Observing wear of the drill with scanning electronic microscope, results show that there is no crack or spallation of the CrAlTiN coatings in wear zones. Main mechanism of the wear here is adhesion.     

Structural Characteristics of TiO2 Ceramic Coating by Micro-Plasma Oxidation

TiO2 ceramic coatings with thickness of 20 μm were formed on the surface of pure titanium by micro-plasma oxidation. Their micro-structures were investigated by by using X-ray diffraction and their surface images were detected by using scan electronic microscope. There were three kinds of TiO2 coatings, pure anatase type TiO2 phase, mixed phases consisted of rutile type TiO2 phase and anatase type TiO2 phase, pure rutile type TiO2 phase. The coating surface with the pure anatase type TiO2 phase is rough, while the coating surface with the pure rutile type TiO2phase is smooth. The upper coating surface with the mixed type TiO2 phases is anatase type TiO2 structure and the subsurface of the TiO2 coating is rutile type TiO2structure.