钛网添加对镁/铝复合板微观组织和力学性能影响研究

目的 有效抑制镁/铝复合板界面处金属间化合物的形成。以钛网为中间金属夹层,研究它对镁/铝复合板微观组织和力学性能的影响。方法 利用复合轧制技术制备以钛网为中间金属夹层的镁/铝-钛复合板,采用扫描电子显微镜(SEM)、电子背散射衍射仪(EBSD)、万能试验机等对复合板退火前后的微观组织和力学性能进行表征和分析,系统研究中间层钛网对轧制态和退火态复合板微观组织、织构、拉伸性能、界面结合强度的影响规律。结果 中间层钛网均匀分布在镁/铝-钛复合板界面处,钛网的添加能有效抑制复合板退火过程中镁-铝金属间化合物的连续生长,减少金属间化合物的数量。与镁/铝复合板相比,钛网的添加对轧制态和退火态复合板中镁层和铝层的平均晶粒尺寸和织构类型的影响较小。与镁/铝复合板相比,钛网的添加降低了轧制态复合板的界面剪切强度和延伸率,但极大提升了退火态复合板的界面剪切强度、拉伸强度和延伸率。结论 中间层钛网的添加可有效减少复合板界面处金属间化合物的数量,提升退火态复合板的综合力学性能。     

电子封装用Cu/Mo/Cu复合材料的工艺研究

研究了浸涂助复剂(铝基合金)和室温轧制工艺对Cu/Mo/Cu复合界面结合强度的影响,简述了Cu/Mo/Cu复合板室温轧制成形工艺过程,详细分析了表面和界面清理、初道次轧制临界变形率及热处理工艺等因素对复合板结合强度的影响.实验结果得出,钼板浸涂Al-Mn-Zn-Sn合金助复剂后的热处理温度为800～850℃;初道次轧制变形率为45%最佳;复合轧制后合适的退火工艺为450℃,保温60 min.     

高性能钛/铝复合板的关键制备技术

目的 研究TA2纯钛/6061铝合金复合界面的微观组织和力学性能,以及热处理对复合板组织和力学性能的影响.方法 在1×10-2 Pa高真空度下,对钛/铝复合坯进行搅拌摩擦焊封装,并在轧制温度为426℃和总压下率为80％下进行热轧复合;然后,对复合板进行T6热处理,即在540℃固溶及177℃时效5 h.随后,对热处理前后的复合界面进行扫描电镜和电子探针分析,明确元素扩散机制,并对复合板进行拉剪性能测试.结果 热轧后复合板的界面平直,无气孔、裂纹等缺陷,界面剪切强度为94.2 MPa.热处理后复合板铝基体力学性能提高,界面剪切强度达141.2 MPa.结论 采用真空轧制复合技术制备出了板形好、无缺陷的钛/铝复合板,经T6热处理后,钛/铝复合板的界面结合性能大幅改善,提高约50％.     

热加工工艺对钛-钢复合板界面力学性能和显微组织的影响

研究了热加工工艺对钛-钢复合板界面力学性能和显微组织的影响.测试了在A,B,C,D 4种温度下热轧复合板界面的力学性能,用金相显微镜及扫描电镜观察了界面显微组织并分析了界面的成分.结果表明,在A,B 2种温度下轧制的钛-钢复合板界面机械性能良好,延伸率高,其剪切强度不但可保持坯料原有的水平,甚至还略有增加.在C,D 2种温度下轧制的钛-钢复合板界面机械性能相对较低,延伸率较高,但剪切强度要比爆炸复合坯料低,尤其是D加热温度,轧制后界面剪切强度急剧下降.热轧的终轧温度也是影响钛-钢复合板界面结合性能的重要因素.在低于相转变温度的合适温区热轧,且终轧温度合适,获得的钛-钢复合板结合界面无爆炸波纹,没有污染,生产的脆性化合物极细小,组织类同于钛材完全退火的等轴组织.     

翼缘板钢非对称冷轧及再结晶退火实验研究

对翼缘板钢采用非对称冷轧,在压下率78%时,对轧件进行微观显微组织观察,结果表明:随着异速比增大,晶粒长度和宽度比值也增大;提出了在异步轧制条件下,晶粒长宽比值可以反映轧件所受附加剪切变形的大小.对冷轧后的轧件进行拉伸实验与不同温度的退火实验,并进行透射电镜观察,结果表明:随着异速比增加,规定非比例延伸强度增加,退火后...     

层状镁/铝复合板轧制工艺研究进展

镁/铝复合板具有密度小、比强度高和耐腐蚀性好等优点,广泛应用于航空航天、汽车制造等领域.轧制法是目前生产镁/铝复合板最为广泛的一种方法,该法设备简单、操作容易、成本低廉.介绍了普通轧制法、异步轧制法、爆炸+轧制法、累积叠轧法、固-液铸轧法、波-平轧制法6种轧制工艺,以及这些工艺在制备镁/铝复合板时的优缺点.波-平轧制工艺可以提高复合板的平直度,有利于板材后续加工成形.也研究了轧制温度、轧制压下率、轧制速度、轧后退火处理对镁/铝复合板力学性能的影响,镁/铝界面金属间化合物的形成因素,以及化合物层厚度对镁/铝复合板力学性能的影响.     

铝/钢轧制复合有限元二次开发模拟与实验研究

目的 针对铝/钢两种金属性能差异大,轧制复合存在严重的变形不协调及结合强度低的问题,研究轧辊同径与异径及单辊驱动对复合板协调变形及结合强度的影响.方法 通过有限元二次开发进行模拟建模,并结合同步和异步轧制实验分析板翘曲机理.结果 与铝板接触的轧辊作为主驱动辊可使板变形更协调且结合强度更高,变形翘曲度为0.048,结合强度为34.2 MPa.结论 采用接触铝侧轧辊单侧驱动,双金属界面实现复合的位置更靠近轧辊出口,复合后的双金属界面间的剪应力和所受弯矩较小,制备的铝/钢复合板变形协调性更好,且结合强度更高.     

铝/钛/铝三层复合板热轧工艺及微观组织研究

钛/铝层状复合材料具有两种材料优异的特性,能够满足一些特殊工程需要。开发了热轧复合技术,成功制备了铝(1100)/钛(TA2)/铝(1100)三层复合板。研究了复合板轧制过程中的关键轧制技术参数(临界压下率和轧制复合工艺条件)。利用光学显微镜和SEM观察了钛/铝复合板及结合界面形貌,分析了不同退火温度对复合板力学性能的影响。基于实验结果,描述了影响复合板质量和有助于提高复合板结合强度的关键工艺过程。     

爆炸-轧制钛/钢复合板界面结合性能研究

爆炸-轧制法是先通过爆炸复合制坯,再进行轧制生产复合板的一种方法。本文研究了爆炸-轧制法生产的钛/钢复合板的界面金相、结合界面的元素分布情况以及退火温度对界面结合强度的影响等问题,结果表明:爆炸轧制法生产的钛钢复合板的界面近似呈平直状,在界面钢侧有一脱碳层,引起界面附近碳元素的重新分布,对结合性能有重要影响;获得高强度结合的界面特征是:剥离界面钢层上的Ti元素含量在一定范围内,钛层大量粘铁;退火温度对界面的结合强度影响较大,而在相应保温下保温时间影响不明显。     

喷射轧制钢/Al-Pb复合轴瓦带材的组织与性能

采用喷射轧制工艺制备了钢/Al-8.5Pb-4Si-Cu-0.5Sn复合轴瓦带材,分析了所制备材料的组织及性能.结果表明,用喷射轧制工艺制备的轴瓦合金Al-Si基体中分布有均匀细小的Pb相粒子,经过50%变形量的轧制和在320℃后续退火5h的处理,在复合轴瓦带材的界面处发生了合金元素的扩散,形成了良好的冶金结合层,界面强度高,剪切强度达到72MPa.用喷射轧制工艺制备的轴瓦合金具有良好的耐磨性能.     

Estimation of Parameters of Universal Distribution of Moments of Failure of Products

A method is proposed for estimating the parameters of a mixture of exponential and Weibull distributions for which the accuracy of preliminary estimates obtained by graphical analysis is refined in accordance with the criterion of maximum likelihood. The efficiency of the proposed method is supported by the results of statistical modeling.     

Evaluation of optical properties of highly scattering media by moments of distributions of times of flight of photons

A novel method for the determination of the optical properties of tissue from time-domain measurements is presented. The data analysis is based on the evaluation of the first moment and the second centralized moment, i.e., the mean time of flight and the variance of the measured distribution of times of flight (DTOF) of photons injected by short (picosecond) laser pulses. Analytical expressions are derived for calculation of absorption and of reduced scattering coefficients from these moments by application of diffusion theory for infinite and semi-infinite homogeneous media. The proposed method was tested on experimental data obtained with phantoms, and results for absorption and reduced scattering coefficients obtained by the proposed method are compared with those obtained by fitting of the same data with analytical solutions of the diffusion equation. Furthermore, the accuracy of the moment analysis was investigated for a range of integration limits of the DTOF. The moment analysis may serve as a comparatively fast method for evaluating optical properties with sufficient accuracy and can be used, e.g., for on-line monitoring of optical properties of biological tissue.     

Assessment of intakes of mixtures of radionuclides

Australia has several uranium mines and a large number of mineral sand mines, with associated processing facilities. Exposures resulting from these mining and processing operations usually involve intakes of mixtures of radionuclides. This work describes the development of a suite of first order, linear compartment models, based on the ICRP Publication 66 respiratory tract model, and an analytical solution to the decay equations, for assessing the consequences of such intakes. The computer programs based on these models directly compute excretion, organ retention and organ and whole-body doses for intakes of either single radionuclides or any mixture of radionuclides belonging to the same radioactive decay chain. The intake can be via inhalation, ingestion or injection, and can be acute, chronic or of limited duration. The starting concentration and degree of secular (dis)equilibrium can be specified for each radionuclide. No assumptions need to be made about the relative magnitudes of the radioactive half-lives of the different nuclides.     

Estimation of potentialities of methods of summation of direct measurement errors

Conventional methods for summation of direct measurement errors are considered. Conditions under which these methods provide consistent results are stated. It is proposed to utilize for characteristic of the total error, its interval estimator or the half-sum of the value obtained by adding up its arithmetic and geometric random errors.Translated from Izmeritel'naya Tekhnika, No. 4, pp. 10–12, April, 1995.     

卧式金属罐容量的测量结果不确定度

本文根据多年的实践检定经验 ,参照JJF1 0 59- 1 999《测量不确定度评定与表示》以及《测量不确定度表达 1 0讲》 ,对卧式金属罐容量的测量结果不确定度进行了评定。     

盐酸浓度不确定度的评估

通过对盐酸浓度标定的过程分析，找出影响结果的各个分量，进行不确定度的评定，按照计量技术规范给出标准的表示法。     

Analysis of the rate of propagation of the wave of change of boiling modes

An approximate analytical expression is derived for the velocity of the front of the wave of change of boiling modes on a rod and on a plate. The impact of the Thomson effect and of the heater orientation in the gravity field is included. Adequate agreement is demonstrated between the derived relations and experimental data.