新型推挽激励的谐振式微机械静电场传感器

为了提高传感器的信噪比(signal-to-noise ratio,SNR),降低器件的耦合干扰,基于表面微机械工艺设计制作了一种新型推挽激励方案的谐振式微型静电场传感器.该传感器敏感结构主要包括静电梳齿激励电极、屏蔽电极和感应电极3部分.工作时,在该传感器敏感结构同一侧梳齿的固定端上加入反相相等的激励信号,实现差分激励,使屏蔽电极在谐振频率处振动,从而在感应电极上感应出差分电流信号,通过相关检测方式检测出传感器该输出信号的二次谐波分量,即可获得被测静电场强度大小.该传感器的新型结构设计和激励检测方案可获得最大电场响应灵敏度,并有效抑制了同频耦合串扰和共模噪声.常压室温(约25℃)测试结果表明,在量程(-15 kV/m～15 kV/m)内,只需要5 Vpp激励电压,其中线性度(端基线性度)达到了1.03%,分辨率优于200 V/m.     

新型便携式薄膜体声波谐振气体传感器的研制与应用

基于MEMS工艺的新型阵列化薄膜体声波谐振器(FBAR),可实现对多种挥发性气体的高通量检测.本文通过对薄膜体声波谐振器表面进行不同的化学官能团修饰,形成了传感器阵列,挥发性气体可以在不同化学官能团修饰的器件界面进行选择性沉积,通过监测传感器的谐振频率变化,形成气体响应的特征条形码,由此实现了对不同挥发性气体更加准确的检测.相对于传统的气体检测手段,由于采用了MEMS工艺,该传感器具备体积小巧、反应快捷、灵敏度高等优势,同时通过多化学官能团修饰的阵列化传感器可以实现一套传感装置对不同气体的检测,大大提高了气体检测的效率、识别能力和准确性.     

高灵敏Love波传感器及其关键材料

Love波传感器是声表面波传感器的一种,其灵敏度最高.对Love波生物、化学传感器的研究现状进行了综述,着重分析了波导材料及其厚度、基板材料及其切向对传感器的灵敏度及温度稳定性的影响关系.指出采用高频谐振型的器件结构并结合聚合物波导的方案可进一步提高Love波传感器的灵敏度.     

一种基于光纤F-P腔的石墨烯谐振式压力传感器

谐振式传感器具有良好的重复性、分辨率和稳定性,全光纤谐振式微型传感器则集合了微纳结构与光纤传感特性两者的优点。石墨烯作为近年来发现的一种新型材料,具有良好的热学和力学特性,可以作为谐振式传感器中的敏感元件。本文提出了一种基于光纤F-P结构的石墨烯谐振式压力传感器,其兼具微机械传感器和光纤谐振器的优点,具有较高的谐振频率,在测量压力的实验中展现出良好的性能,压力灵敏度最高可达2. 93Hz/Pa,具有重要的应用价值。     

新型高灵敏度GLV光学电流传感器设计与性能分析

本文结合GLV技术设计了一种适于检测高压交流电的新型光学电流传感器.这一设计具有温度稳定性好、大电流下灵敏度高、频率响应范围宽等特点,且测量芯片制作工艺简单、成本低廉.通过有限元分析和数值计算对器件的模态、工作性能、热膨胀特性等进行了分析模拟,结果表明:测量芯片量程达500A～2000A,并可通过改变设计参数灵活调整;一阶固有频率接近60kHz,大电流下灵敏度接近0.2dB/A,外界温度变化±50K时传感器测试误差在0.7%以内.     

基于集成氮化硅微腔的光学传感芯片研究

近年来随着传感器在生物探测领域的应用,提高传感器芯片的灵敏度成为研究的热点。利用氮化硅微腔灵敏度高、成本低、易于集成的优点,设计制造了1550 nm波长下二维、三维结构品质因子分别为1.6×104和4×103的悬空耦合传感器芯片,并详细研究了集成氮化硅微腔光学传感芯片在折射率测量方面的应用。     

共平面低功耗CO气体传感器的设计及制作

设计了一种新型的共平面微结构气体传感器,利用MEMS技术制作了传感器样品.实验测得该传感器对于体积分数为50×10~(-6)CO气体的灵敏度为8.6(R0/R),功耗为82mW,响应时间约5s,恢复时间约22s,该传感器的灵敏度是同种敏感材料烧结型传感器(测体积分数50×10~(-6) CO气体)的2.5倍,而功耗却是同种敏感材料烧结型传感器的1/2,是一种具备了体积小、重量轻、功耗低、灵敏度高、便于与其它器件集成等特点,而且制作工艺简单,成本较低的微结构CO气体传感器.     

工艺特性对二维微加速度传感器性能的影响

工艺特性在很大程度上决定了MEMS器件最终的功能特性.本文针对自主设计的二维微加速度传感器,在概念设计阶段定量分析了工艺特性对传感器性能的影响,主要包括质量偏心、梁加工误差、结构对称性、非平行效应等.结果表明:质量偏心会引起角位移变化,但对主轴刚度无影响,传感器不会有输出;在现有工艺条件下,可忽略梁厚误差的影响,但需严格控制梁宽误差;各种不对称方案对传感器主轴刚度和横向灵敏度的影响程度不同,不对称方案对横向灵敏度的影响随着不对称性的加剧而增大;非平行效应使得在相同外载荷作用下敏感轴向位移减小,但静态灵敏度却有所增加.     

用于挥发性有机化合物探测的微悬臂梁传感器

在研制成功的用于化学气体探测的热驱动微悬臂梁谐振器的基础上,提出了基于这种微悬臂梁谐振器,并以聚合物涂层作为挥发性有机化合物吸附敏感层的谐振式气体传感器.利用3种聚合物材料：聚氧化乙烯（PEO）、聚乙烯醇（PVA）和聚乙二醇乙醚醋酸酯（PEVA）,在微悬臂梁谐振器上制备气体敏感层,探测6种挥发性有机化合物：甲苯、苯、乙醇、丙酮、己烷和辛烷.通过有限元分析估计了聚合物涂层的工作温度.用喷射法制备了PVA和PE-VA涂层,用点滴法制备了PEO涂层.测试了传感器的开环幅频特性,实验检测了气体传感器的谐振频率变化与分析物蒸气浓度的关系以及传感器对相对湿度的响应,分析了传感器的灵敏度和线性度.实验结果表明,这种涂覆聚合物敏感层的热驱动微悬臂梁谐振器为探测挥发性有机化合物提供了良好的平台.根据实验结果,可开发几种基于不同聚合物敏感层的高灵敏度微型气体传感器.     

新型谐振式硅微机械加速度计

制作出一种新型结构的谐振式硅微加速度计，其输出频率信号可以克服微机电系统器件输出微弱信号检测的困难、采用双端固定音叉作为谐振器，在加速度作用下，质量块的惯性力通过悬臂梁施加于音叉轴向，利用音叉谐振频率的变化测量加速度．在每个音叉臂上制作了梳齿结构，用梳齿间的静电力激励音叉产生谐振，并利用其构成的电容检测其振动频率．该加速度计采用体硅工艺制作，文中给出了工艺流程、用有限元方法仿真估算，得到传感器的灵敏度约为2／gHz．     

The Research of Anti-Wear Properties of Organomolybdenum Compounds in the Engine Oils

A four-ball tester was used to evaluate the anti-wear performance of three kinds of organomolybdemun compounds in the engine oils, i. e., molybdenum dialkyldithiophosphate (MoDDP), molybdenum dialkyldithiocarbamate ( MoDTC), and sulphur and phosphorus freeorganomolybdeum (Molybdate). The results indicate that a low concentration of MoDDP doesn' t improve the anti-wear properties of the commercial engine oils, but a high concentration of MoDDP can obviously improve the anti-wear properties and the load-carrying capacity of the engine oils. MoDTC doesn' t improve the antiwear properties of the engine oils, but worsens the anti-wear properties of the oils. Signifi can timprove ment of frictional and wear characteristics is obtained with Molybdate added in the commercial engine oils and the formulated oils.     

Certification Becomes Important for the I Quality; and Safety Supervision of the Chinese Liquor Sector

The end of 2007, over 200 unit products of more than 80 Chinese firms have passed the quality grade certification for liquor products. These products involve distilled spirits, beer, wine, yellow wine, fruit syrup wine and others, and cover over 80% of the national top-branded liquor products.……     

Deposition and Coating Properties on CVD Tungsten

Surface characterization and microstructure studies are performed on chemical vapor deposited (CVD) tungsten coating. There is about 2 μm thickness diffusion layer of tungsten in the molybdenum substrate. The thermal shock test shows tungsten coating has good adhesion with molybdenum substrate, but the elements of oxygen and carbon in the tungsten coating have the bad affection to the adhesion. The result of high-temperature diffusion experiment is the diffusion rate from molybdenum substrate to tungsten coating is faster.     

Analysis of marine hydrobiont lipid extracts as possible cryoprotective agents

We studied a combined effect of the cryoprotectants both of lipid and carbohydrate origin at the presence of DMSO or without it on cell viability and the RNA synthesis in the embryonic mollusc and echinoderm cell cultures obtained at different developmental stages. Cryoprotective properties of exogenous lipids correlated with their thermotropic behavior. Lipid extracts from marine hydrobiontes, which thermal transitions are characterized by relatively small part of calorimetric thermogram area lying at temperatures above 0 °C (6–18%), were found to possess a considerable cryoprotective activity. The results are discussed in relation to the prediction of the cryoprotective activity of lipid extracts for marine animal cells. In addition, it was found that marine invertebrate cells can be cryopreserved without DMSO at the presence of trehalose and lipid extracts of some marine hydrobiontes.     

Low-Temperature Properties of Silver

Pure silver is used extensively in the preparation of high-temperature superconductor wires, tapes, films, and other configurations in which the silver not only shields the superconducting material from the surrounding materials, but also provides a degree of flexibility and strain relief, as well as stabilization and low-resistance electrical contact. Silver is relatively expensive, but at this stage of superconductor development, its unique combination of properties seems to offer the only reasonable means of achieving usable lengths of conductor. In this role, the low-temperature physical (electrical, thermal, magnetic, optical) and mechanical properties of the silver all become important. Here we present a collection of properties data extracted from the cryogenic literature and, to the extent possible, selected for reliability.     

Early ironwork in Biscay: Survey,excavation, experimentation and materials characterization. An integral study of the mountainside ironworks (ferrerías de monte or “haizeolak”)

ABSTRACT

The production of iron in Biscay (Basque Country, Spain) has been a hallmark of this territory of the North of the Iberian Peninsula throughout its history. The Archaeology team of the Basque Country Mining Museum has spent 13 years, so far, studying the origins of this activity through the evidences left at the old pre-hydraulic iron production workshops known as mountainside ironworks (ferrerías de monte) or haizeolak. It has catalogued 170 archaeometallurgical sites of this type in Biscay, and the archeological excavation of some of them has led to the knowledge of the different stages of the production process that took place in these workshops. The team has also experimentally reproduced the work carried out in a mountainside ironworks from the High Middle Ages, and it has currently started the characterization process of this type of activity through the study of the collected materials.     

Mechanism Study on the Wear of CrAlTiN Coated High-Speed Steel Twist Drills Under Dry Cutting Conditions

As demands about environment protection are growing up, dry cutting technology is getting more and more concerns from all over the world. Main works performed here are study on dry cutting performances and wear mechanisms of M2high-speed steel (HSS) twist drills with CrAlTiN multicomponent coatings, which was deposited using magnetron sputter ion plating system, in drilling 45 and 30CrMnSiA steel, and their comparisons to those in drilling the same steel but using monolayer CrN and commercial TiN coated drills. Drilling performances of drills are evaluated mainly through the measurements of width on outer corner flank land and the cutting forces. Results show that performances of CrAlTiN coated drills are better than those of monolayer CrN and TiN coated drills. In drilling 45 and 30CrMnSiA steel, the average tool life of the CrAlTiN coated drills are 17.2 and 11.8 times higher than those of the uncoated drills. Observing wear of the drill with scanning electronic microscope, results show that there is no crack or spallation of the CrAlTiN coatings in wear zones. Main mechanism of the wear here is adhesion.     

Study on Bond Ability of Arc-Spraying Coatings with Different Surface Pretreatment on Cast-Iron

Arc spraying coatings are widely used in various applications, but uncommon in cast iron substrate. Different surface pretreatment technology is tested on substrates of gray cast iron. Surface roughness and residual stress were measured by TR200 and X-ray diffraction analyzer. Influence of different surface pretreatment methods ( dry blasting and fusebond) on roughness and residual stress was analyzed. The arc-sprayed coatings of wire 3Cr13 (φ2mm) on gray cast iron substrate is studied. The microstructure and interface of bonding layer were observed by SEM. The bond strength was taken by tensile test. Results show that bond strength with grit blasting is higher than fuse-bond; it is feasible to make wire 3Cr13 coating with arc spraying on cast iron substrate roughened by grit blasting.     

Structural Characteristics of TiO2 Ceramic Coating by Micro-Plasma Oxidation

TiO2 ceramic coatings with thickness of 20 μm were formed on the surface of pure titanium by micro-plasma oxidation. Their micro-structures were investigated by by using X-ray diffraction and their surface images were detected by using scan electronic microscope. There were three kinds of TiO2 coatings, pure anatase type TiO2 phase, mixed phases consisted of rutile type TiO2 phase and anatase type TiO2 phase, pure rutile type TiO2 phase. The coating surface with the pure anatase type TiO2 phase is rough, while the coating surface with the pure rutile type TiO2phase is smooth. The upper coating surface with the mixed type TiO2 phases is anatase type TiO2 structure and the subsurface of the TiO2 coating is rutile type TiO2structure.     

Evaluation of fatigue life of steel using steel grain size

The insightful discussion of the relationship between the construction of metallographic and fatigue life and proposition of mathematical relationships describing this relationship was conducted in the paper. This paper presents a method for estimating the fatigue life, based on the construction of the microstructural material taking into account the grain size and the participation of ferrite and pearlite phase.