Ti17合金电子束焊接接头的力学性能

通过室温拉伸试验、室温缺口拉伸、室温冲击试验以及金相分析对Ti17合金电子束焊接接头的显微组织和室温力学性能进行了研究.试验结果表明:用电子束焊方法焊接Ti17合金可获得室温性能良好的焊接接头,其接头的抗拉强度不低于母材,焊缝的缺口敏感系数均小于1,焊缝具有较高的冲击韧度.焊缝区组织与母材组织基本相同,都是α相上分布着沿晶界及晶内析出的细针状β相,焊缝区的晶粒度要比母材的晶粒度粗大.     

Incoloy 825镍基高温合金电子束焊工艺及接头组织与力学性能分析

采用电子束焊，对空冷器管箱Incoloy 825镍基高温合金进行对接焊试验. 通过对焊接接头的组织观察，并结合拉伸力学性能以及接头的冲击韧性等试验，分析镍基高温合金电子束焊接头的组织和力学性能. 结果表明, 采用电子束焊焊接镍基高温合金可以得到良好的焊接接头，焊缝区组织由大片等轴晶和少量柱状晶组成；焊缝区没有出现明显的元素烧损现象；焊缝、热影响区硬度达到母材硬度值；焊缝接头抗拉强度达到600 MPa，接近母材抗拉强度，接头断裂形式为韧性断裂；焊缝和热影响区的冲击吸收能量高于母材区，其中焊缝区的冲击吸收能量达到了262 J，冲击断口形貌为韧窝状.     

700MPa级低合金高强钢低匹配焊接接头组织和性能研究

按照低匹配设计原则,采用熔化极气体保护焊对屈服强度为700 MPa级的低合金高强钢进行了焊接。采用光学显微镜、扫描电镜和力学性能试验研究了焊接接头的组织和性能。结果表明,焊缝区组织主要为针状铁素体和少量先共析铁素体,粗晶热影响区组织为上贝氏体;焊缝区显微硬度明显低于母材,焊缝区-40℃时的冲击韧度(AKV)为58 J,抗拉强度达到了母材抗拉强度的92.4%,焊接接头的综合力学性能良好。     

35CrMnSi钢电子束焊接头显微组织和力学性能研究

研究了35CrMnSi 钢电子束焊接头的组织和力学性能.试验结果表明:该钢电子束焊焊缝为典型的针状马氏体+残余奥氏体组织,HAZ为中温组织;2种厚度钢板焊接接头各区域的硬度值基本一致,且焊缝硬度高于热影响区的,热影响区的硬度高于母材的.经电子束焊后,2种厚度35CrMnSi钢板接头塑性比母材的塑性低,这与其显微组织有关;35CrMnSi钢电子束焊焊缝的冲击韧度低于母材.     

2205双相不锈钢的激光-MIG复合焊接头性能

常规的高能束焊接方法因焊后冷速较快易导致双相不锈钢焊缝及热影响区两相比例失衡,接头性能恶化.采用激光-MIG复合焊接方法对2205双相不锈钢进行焊接,焊后对接头微观组织、力学性能和腐蚀性能分析发现,焊缝及热影响区铁素体相比例控制在40%～70%合理范围内,接头硬度和抗拉强度高于母材,焊缝、熔合线、热影响区的～40℃冲击...     

7 mm厚TC4钛合金电子束焊接头组织和性能

采用真空电子束焊对7 mm厚TC4钛合金板进行焊接,利用光学显微镜对焊接接头显微组织进行表征,分析不同区域显微组织,通过显微硬度、拉伸试验、冲击试验、弯曲试验对力学性能进行测试,借助扫描电镜对拉伸、冲击断口形貌进行观察,对焊接接头显微组织演变规律和性能进行研究。结果表明,真空电子束焊焊接接头成形良好,TC4钛合金母材组织由α相和β相组成,焊缝区组织由原始的β相转变而成α′相（针状马氏体）,为粗大的柱状晶组织,热影响区组织由均匀且细小的针状马氏体α′相及原始的α相和β相组成;焊缝区显微硬度高于热影响区和母材区,从焊缝顶部到根部显微硬度逐渐下降;焊接接头抗拉强度高于母材抗拉强度;V形缺口在焊缝区的冲击试样具有较好的韧性。     

T91/P91窄间隙热丝TIG焊接工艺对接头力学性能的影响

通过对T91/P91窄间隙热丝TIG焊试验,对比研究了焊接接头各区包括焊缝、热影响区、母材的显微组织,以及各项力学性能比如常温拉伸、高温拉伸、硬度及冲击性能,从而探究窄间隙热丝TIG焊对T91/P91钢焊接性的影响.试验结果表明,焊接接头组织均匀,主要为回火马氏体;抗拉强度达到了母材水平甚至比母材更强;焊缝区域硬度分布比较均匀,硬度值高于热影响区和母材;焊缝的冲击韧性也与母材相当.研究结果表明,窄间隙热丝TIG焊可以改进T91/P91焊接接头的焊接质量,焊接接头各项力学性能均满足使用需求,从而获得了较高质量的焊接接头.     

焊接工艺对高强度贝氏体钢激光-电弧复合焊接头组织和性能的影响

针对高强度贝氏体钢,对比研究了单层单道和两层两道激光-电弧复合焊对焊接接头组织和硬度、拉伸、冲击等力学性能的影响。结果表明:两种工艺下所得到的接头焊缝区组织存在明显差异,而热影响区组织未见明显不同;两种工艺下的接头全厚度试样和分层试样的抗拉强度接近,而单道焊接头全厚度试样塑性较差;两种工艺下焊缝区和焊接热影响区的冲击吸收功均低于母材,且单道焊焊缝的不同区域的韧性存在较为明显的差异。     

20g与P91异种金属焊接接头组织及其性能分析

通过对20g和P91异种金属进行埋弧自动焊试验,研究了焊接接头各区域包括母材、热影响区和焊缝的显微组织,并对焊接接头进行了硬度测试、拉伸试验和冲击试验等力学性能测试。结果表明,20g侧焊缝组织为珠光体和针状铁素体,P91侧焊缝组织是块状铁素体、珠光体以及马氏体;焊缝区的显微硬度值要明显高于两侧母材以及热影响区的显微硬度值;焊缝金属的抗拉强度要明显高于两侧母材的抗拉强度,断裂位置发生在母材20g侧;接头20g侧母材、焊缝区和P91侧母材的冲击功分别185.2、239.6和13.0 J,表明焊缝的冲击韧性明显高于两侧母材的冲击韧性,但是和焊前相比较,20g侧母材焊后冲击韧性得到大幅提高,而P91侧母材焊后冲击韧性显著降低。     

TC4钛合金电子束焊接头性能研究

采用真空电子束焊方法进行TCA钛合金的焊接，借助OM、SEM设备观察焊缝金属显微组织和断口形貌，测试了焊接接头硬度并进行了冲击试验，分析了焊接接头性能、显微组织及焊缝中气孔的形成。结果表明，采用真空电子束焊焊接TCA钛合金时，焊缝和热影响区金属中较粗大的原始β相一部分转变为过饱和的针状马氏体；焊缝中心有少量的针状α’相，并形成了编织状α组织；焊缝金属的硬度值比母材金属的高，但冲击韧度比母材金属的低。     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

Theoretical Analysis for the Motion and Temperature of Melt Droplets in Spray Degassing Process

The motion of melt droplets in spray degassing process was analyzed theoretically. The height of the treatment tank in spray degassing process could be determined by the results of theoretical calculation of motion of melt droplets. To know whether the melt droplets would solidify during spraying process, the balance temperature of melt droplets was also theoretically analyzed. Then proof experiments for theoretical results about temperature of melt droplets were carried. In comparison, the experimental results were nearly similar to the calculation results.     

Growth Kinetics of Single Inclusion Particle in Molten Melts

On the basis of the single-particle framework, a new theory on inclusion growth in metallurgical melts is developed to study the kinetics of inclusion growth on account of reaction and collision. The studies show that the early growth of inclusion depends on reaction growth and Brawnian motion collision, and where the former is decisive, the late growth depends on turbulence collision and Stokes＇ collision, and where the former is dominant; collision growth is very quick during the smelting process, lessened in the refining process, but nearly negligible in the continuous casting process.     

An Easy Way to Quantify the Adhesion Energy of Nanostructured Cu/X(X=Cr,Ta,Mo,Nb,Zr) Multilayer Films Adherent to Polyimide Substrates

An approach based on film buckling under simple uniaxial tensile testing was utilized in this paper to quantitatively estimate the interfacial energy of the nanostructured multilayer films(NMFs) adherent to flexible substrates. The interfacial energies of polyimide-supported NMFs are determined to be *5.0 J/m2 for Cu/Cr, *4.1 J/m2 for Cu/Ta,*2.8 J/m2 for Cu/Mo, *1.1 J/m2 for Cu/Nb, and *1.2 J/m2 for Cu/Zr NMFs. Furthermore, a linear relationship between the adhesion energy and the interfacial shear strength is clearly demonstrated for the Cu-based NMFs, which is highly indicative of the applicability and reliability of the modified models.     

High-Speed Friction Stir Welding of SiC_p/Al–Mg–Si–Cu Composite

A 17 vol% SiCp/Al–Mg–Si–Cu composite plate with a thickness of 3 mm was successfully friction stir welded(FSWed) at a very high welding speed of 2000 mm/min for the first time. Microstructural observation indicated that the coarsening of the precipitates was greatly inhibited in the heat-affected zone of the FSW joint at high welding speed, due to the significantly reduced peak temperature and duration at high temperature. Therefore, prominent enhancement of the hardness was achieved at the lowest hardness zone of the FSW joint at this high welding speed, which was similar to that of the nugget zone. Furthermore, the ultimate tensile strength of the joint was as high as 369 MPa, which was much higher than that obtained at low welding speed of 100 mm/min(298 MPa). This study provides an effective method to weld aluminum matrix composite with superior quality and high welding efficiency.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

A STUDY OF TEMPERATURE-DEPENDENT VALENCE BOND STRUCTURE OF TITANIUM

On the basis of energy and shape method for the determination of the valence bond (VB) structures of crystal, the valence bond structure of titanium is redetermined at room temperature and calculated in the whole temperature range of 0-1943K. The outer shell electronic distribution of Ti is e_c~(2.9907) · (s_c~(0.4980) d_c~(2.4927)) ef1.0093 in crystal. The temperature dependences of the VB structures of hcp and bcc phases are the same. The VB structures of hcp and bcc phases monotonically increase or decrease with the increase in temperature, but show discontinuous changes at the phase-transformation temperature 1155K.     

Structural Optimization of Electromagnetic Swirling Flow in Nozzle of Slab Continuous Casting

During the slab continuous casting process, the flow field of molten steel in the mold plays a decisive role in the quality of the slab. In this paper, electromagnetic swirling flow in nozzle technology is proposed to control the flow field in mold.This technology can drive molten steel to rotate inside the submerged entry nozzle by electromagnetic force, thereby controlling the flow field. This research shows that it can reduce the impact of molten steel on the bottom of nozzle and partly reduce the negative pressure at the upper part of nozzle outlet which is even eliminated by optimizing the structure and angle of nozzle. The area of heat flux of the mold wall becomes larger, and the crest value of heat flux gets lower than that without swirling in nozzle and any nozzle optimization. The meniscus fluctuates smoothly, and the flow velocity at the top surface is within a reasonable range. The temperature field distribution in the mold is uniform which was beneficial to the growth of equiaxed crystal and decreased element segregation.     

Effect of Rare Earth Doping on Impedance,Modulus and Conductivity Properties of Multiferroic Composites:0.5(BiLa_xFe_(1-x)O_3)–0.5(PbTiO_3)

The Lanthanum-doped bismuth ferrite–lead titanate compositions of 0.5(Bi LaxFe1-xO3)–0.5(Pb Ti O3)(x = 0.05,0.10,0.15,0.20)(BLxF1-x-PT) were prepared by mixed oxide method.Structural characterization was performed by X-ray diffraction and shows a tetragonal structure at room temperature.The lattice parameter c/a ratio decreases with increasing of La(x = 0.05–0.20) concentration of the composites.The effect of charge carrier/ion hopping mechanism,conductivity,relaxation process and impedance parameters was studied using an impedance analyzer in a wide frequency range(102–106Hz) at different temperatures.The nature of Nyquist plot confirms the presence of bulk effects only,and non-Debye type of relaxation processes occurs in the composites.The electrical modulus exhibits an important role of the hopping mechanism in the electrical transport process of the materials.The ac conductivity and dc conductivity of the materials were studied,and the activation energy found to be 0.81,0.77,0.76 and 0.74 e V for all compositions of x = 0.05–0.20 at different temperatures(200–300 °C).