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1.
Kai Liu Chenyang Zhou Jiaming Hu Song Zhang Qingqing Zhang Ce Sun Yusheng Shi Huajun Sun Changxia Yin Yuzhen Zhang Yu Fu 《Journal of the European Ceramic Society》2021,41(12):5909-5917
A digital light processing (DLP) technology has been developed for 3D printing lead-free barium titanate (BTO) piezoelectric ceramics. By comparing the curing and rheological properties of slurries with different photosensitive monomer, a high refractive index monomer acryloyl morpholine (ACMO) was chosen, and a design and preparation method of BTO slurry with high solid content, low viscosity and high curing ability was proposed. By further selecting the printing parameters, the single-layer exposure time was reduced and the forming efficiency has been greatly improved. Sintered specimens were obtained after a nitrogen-air double-step debinding and furnace sintering process, and the BTO ceramics fabricated with 80 wt% slurry shows the highest relative density (95.32 %) and piezoelectric constant (168.1 pC/N). Furthermore, complex-structured BTO ceramics were prepared, impregnated by epoxy resin and finally assembly made into hydrophones, which has significance for the future design and manufacture of piezoelectric ceramic-based composites that used in functional devices. 相似文献
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Electronic Commerce Research - We consider a platform providing free content for users and earning profit from the sale of advertising. The platform can collect and analyze personal data to... 相似文献
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Mitigating gibbsite particle cracking and breakage during industrial alumina production can increase the quality of smelter grade alumina product by reducing the ultrafine particle content. Therefore, it is essential to investigate the particle cracking during static calcination and the breakage of calcined gibbsite particles under external force. In this work, we investigated the impact of the calcination ramping rate and the crystallite size on gibbsite particle cracking during static calcination. A slow ramping rate and a large pristine crystallite size tend to increase particle cracking. Apart from the study of particle cracking behaviour, we also investigated the breakage of calcined gibbsite particle under external force. Cracks on the particle surface can initiate breakage within the crystallite and along the grain boundary under external force. The breakage within crystallite occurs as the cleavage of the crystallite, while the breakage along the grain boundary leads to the shedding of a whole crystallite. We further explored the factors influencing the strength of calcined gibbsite particles. With increasing calcination temperature, the strength of particle increases when gibbsite converts to boehmite, and then decreases when boehmite converts into amorphous alumina. Particles containing smaller crystallites and calcined with fast ramping rates exhibit higher resistance to breakage. 相似文献
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道教洞天福地作为中国名山风景的经典类型之一,在宗教山岳景观中占据独特地位。浙东天台山水神秀,历代高道以入山隐修为主要目的,形成了道教在区域山林的景观文化基础。从天台山“神仙之乡”的文化背景出发,从“想象与实践”的视角切入,梳理了天台山洞天福地的景观流变:分析其“不死之福庭”地域性景观的形成经历了“赤城→桐柏”的信仰转移过程;以天台山为坐标,洞天福地格局打破了区域“层级”分布特征,而呈现大范围“州郡”空间格局。作为“联结点”的天台山,洞天世界沟通了宇宙、山、人3个基本场域,由此衍生出“洞宫”式和“周回”式山岳空间营建典范。旨在挖掘洞天福地中典型案例的价值,为中国洞天福地体系的构建提供理论依据。 相似文献
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Zhongyu Qiu Xiaowen Ge Naibao Huang Shixian Zhou Junjie Zhang Jiaping Xuan 《International Journal of Hydrogen Energy》2021,46(3):2952-2959
Polyethylene oxide (PEO)-polypropylene oxide (PPO)-polyethylene oxide block copolymer having different molecular weights are used as precursors of carbon materials to prepare Hollow -Derivatives carbon material as an electrocatalyst through block copolymer self-assembly. The composition and microstructure of the prepared catalysts are shown by Raman spectroscopy, X-ray diffraction (XRD), Test of nitrogen adsorption and desorption curves, High resolution transmission electron microscopy (HR-TEM) and scanning electron microscopy (HR-SEM). Oxygen was passed into alkaline electrolyte solution until the solution reached saturation state. With molecular weight increasing, the obtained sample gradually changed from block to hollow and spherical. When the molecular weight was 12600 g mol?1, the evenly hollow carbon nanocages was acquired (C-12600). In O2 saturated alkaline electrolyte (0.1 M KOH solution), C-12600's limited current density,half-wave potential and initial potential are 5.23 mA cm?2@0.4 V, 0.72 V and 0.81 V, respectively. And most important is that half-wave potential and onset potential have barely change after 2000 cycles of cyclic voltammetry. As a result, the porous carbon materials exhibited excellent electrocatalytic activity while maintaining high stability in alkaline KOH solution. 相似文献
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