Selective O-methylation of phenol with dimethyl carbonate over X-zeolites

The O-methylation of phenol with dimethyl carbonate proceeds selectively in the vapor phase over alkali ion exchanged X-zeolites. Thus, a 76% yield of anisole was obtained with a 93% selectivity over NaX at 553 K. The participation of basic sites in the O-methylation is suggested.     

水文监测创新在2016年长江洪水测报中的作用

2016年,长江中下游发生了区域性大洪水。为保证洪水预报的水文资料需求,长江委水文局通过建立的由水文监测管理体系、水文监测服务体系、水文监测技术支撑体系、水文监测质量保障体系等四大部分组成的水文监测体系创新与关键技术,以“巡测优先、驻巡结合、测报自动、应急补充”的新型水文监测模式,大大提升了防洪监测的能力和水平。与往次防洪监测比较,在应对2016年的大洪水的过程中,长江水文测验的新型模式带来了测洪能力、技术水平、准确度、时效性的系统性提升,其中,流量测验时间缩短了73%~83%,水情信息到报率和准确率达到99.95%,远远高于国家标准。     

图解法和卡丘金法库岸塌岸分析对比研究

分析库水冲蚀、浪蚀作用下库岸的塌岸类型及其主要因素,对其主要破坏方式进行预测,利用图解法和卡丘金法分别对该库岸的20个剖面塌岸宽度进行计算情况.计算结果表明,通过卡丘金法计算得到的库岸塌岸宽度与实际情况相差很大,而图解法的计算结果符合实际情况.对于实际工程,可以灵活分析和运用.     

二(2-氨基乙基)-(3-氨基丙基)胺的合成新方法

以二(氰基甲基)胺及丙烯腈为原料，通过亲核加成、氢化反应合成了不等臂有机多胺化合物二(2-氨基乙基)-(3-氨基丙基)胺，标题化合物及其中间产物经多种谱学手段表征确证。在优化条件下，产物的总收率为67％，含量99.5％(HPLC)。     

波节式换热管压缩失稳试验研究

通过对不同材料、直径和壁厚的波节式换热管进行压缩失稳试验,绘出应力和应变强度关系曲线,指出直光管经胀管成型为波节管后,应力状态分布明显不同于光管,壁厚和直径等规格尺寸的不同会影响波纹管的强度性能.     

HNC-1新型光敏剂的合成与表征

合成了一种光敏剂2-三氯甲基-5-[β-(2-苯并呋喃)乙烯基]-1，3，4-噁二唑(HNC-1)。并用紫外光谱、红外光谱、核磁共振(氢、碳)谱，对产物进行了结构表征。     

由双酚A结晶母液的裂解产物合成双酚A反应过程研究

对反应过程所需催化剂种类及其各影响因素进行了考察。研究表明，大孔强酸性离子交换树脂可替代无机酸作为催化剂用于该反应，其中以未经硫基化处理者为佳；原料中水分的存在不利于产物收率和质量，应控制水的质量分数在1％以下。本研究确定的较佳工艺条件为反应温度65℃，停留时间15min、苯酚／对－异丙烯基苯酚摩尔比20，对应的反应收率为98．5％。对双酚A副产物的处理提供了有效方法。     

Improving SEM Inspection Performance in Semiconductor Manufacturing Industry

Scanning electron microscope (SEM) station is one of the major quality control tasks in wafer manufacturing process. During the process of examining defects on a screen for a certain period of time, SEM inspectors frequently complain about visual fatigue problems. The purpose of the study was to evaluate the effect of wafer‐coating condition (noncoating treatment and gold‐coating treatment) and liquid crystal display (LCD) monitor size (14‐inch and 19‐inch monitor) from the aspects of objective visual fatigue measures (NPA and CFF), subjective eye fatigue rating, and inspection performance. Twelve SEM inspectors participated in this experiment. The results indicated that the treatment of gold‐coating wafer showed significant difference on reducing objective visual fatigue in NPA and CFF change. Using a 19‐inch LCD monitor also demonstrated the effect on reducing eye fatigue as well as improving inspection performance. The improvement of using a gold‐coating treatment wafer and a 19‐inch LCD monitor to reduce SEM inspectors' visual fatigue and to increase inspection performance is thus recommended. © 2012 Wiley Periodicals, Inc.     

Synthesis of antenna arrays with an efficient multiobjective differential evolution algorithm

An efficient multiobjective differential evolution algorithm for array synthesis is proposed in this article. By introducing novel strategies in the generalized differential evolution (GDE3), the proposed algorithm can generate a better converged and distributed Pareto front than the standard GDE3. Five typical benchmark functions are optimized by the proposed improved GDE3 (IGDE) to verify its effectiveness. Furthermore, the proposed algorithm is applied in two‐pattern synthesis problems, including an unequal spaced linear array and a conformal array. The superior performance of the proposed IGDE demonstrates that it is an efficient and competitive algorithm in the function optimization, pattern synthesis, and other electromagnetic problems. © 2013 Wiley Periodicals, Inc. Int J RF and Microwave CAE 24:161–169, 2014.     

碳化物陶瓷的研究现状及发展趋势

本文综述了现阶段碳化物陶瓷超细粉末的主要制备工艺以及烧结方法,同时指出了碳化物陶瓷今后的发展趋势。