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《Biomass & bioenergy》2006,30(10):870-873
Amorphous zirconia catalysts, titanium-, aluminum-, and potassium-doped zirconias, were prepared and evaluated in the transesterification of soybean oil with methanol at 250 °C, and the esterification of n-octanoic acid with methanol at 175–200 °C. Titanium- and aluminum-doped zirconias are promising solid catalysts for the production of biodiesel fuels from soybean oil because of their high performance, with over 95% conversion in both of the esterifications. 相似文献
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Preparation of gold/polyaniline/multiwall carbon nanotube nanocomposites and application in ammonia gas detection 总被引:1,自引:0,他引:1
Qifei Chang Kai Zhao Xing Chen Minqiang Li Jinhuai Liu 《Journal of Materials Science》2008,43(17):5861-5866
Composites of multiwall carbon nanotubes (MWNTs), polyaniline (PANI), and gold nanoparticles were prepared by one pot synthesis.
Based on the interaction between aniline monomers and MWNTs, aniline molecules were adsorbed and polymerized on the surface
of MWNTs. The nanocomposites were characterized by transmission electron microscopy (TEM), X-ray diffraction analysis (XRD),
Fourier transform infrared spectroscopy (FT-IR), and X-ray photoemission spectroscopy (XPS). The sensors based on Au/PANI/MWNT
nanocomposites were tested for on-line monitoring of ammonia gas. The results show that the as-prepared sensors have superior
sensitivity, and good repeatability upon repeated exposure to ammonia gas. 相似文献
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Highly porous cadmium oxide (CdO) nanowires have been prepared by calcining the hydroxy-?and carbonate-containing cadmium compound precursor nanowires. The large-scale precursor nanowires were synthesized through a hydrothermal method. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were employed to characterize and analyze the as-synthesized precursor nanowires as well as the calcined products. It was revealed that the wire-like morphology of the precursor was fundamentally retained during the process of calcination and the CdO nanowires obtained were polycrystalline with highly porous structures. In order to illustrate the formation mechanism of the porous structures, the morphology and composition evolutions of the precursor nanowires under different stages of the calcining process were further investigated via SEM, x-ray diffraction (XRD) and infrared (IR) absorbance spectroscopy. Gas sensing has been explored for the sensor device fabricated with highly porous CdO nanowires, which demonstrates that it has good response owing to its special structures and great selectivity to NO(x). Furthermore, the UV-visible and photoluminescence spectra of highly porous CdO nanowires have also been investigated. 相似文献
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Hollow and porous In(2)O(3) nanospheres have been prepared by the hydrolysis of InCl(3) using carbonaceous spheres as templates in combination with calcination. Based on the observation of scanning electronic microscopy (SEM) and transmission electron microscopy (TEM), it has been revealed that the as-prepared In(2)O(3) nanospheres have a uniform diameter of around 200?nm and hollow structures with thin shells of about 30 nm consisting of numerous nanocrystals and nanopores. Owing to the hollow and porous structures, In(2)O(3) nanospheres possessing more active surface area exhibit a good response and reversibility to some organic gases such as methanol, alcohol, acetone and ethyl ether. In addition, the response mechanism of hollow and porous In(2)O(3) nanospheres to organic gases has been proposed. Furthermore, these prepared In(2)O(3) spheres showed a UV-visible absorption peak centered at around 309?nm, and their photoluminescence spectra have also been investigated. 相似文献
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以半导体氧化物SnO2为基体材料加入40%的活性La2O3材料,制备出了对CO2具有敏感性的气体敏感材料,其检测体积分数范围为(0~5000) ×10-6.实验结果表明:在SnO2-La2O3敏感材料的基础上掺杂适量CeO2,Ag2O,SiO2等氧化物,不仅提高了其对CO2气体的灵敏度,而且可以提高其稳定性,从而大大改... 相似文献