Volatile organo-halogen trace analysis in beverages by thin-layer headspace enrichment and electron-capture gas-chromatography

Applicability of thin-layer headspace (TLHS) procedure giving an aqueous concentrate and also classical purge and trap (PT) in off-line mode to isolate and enrich volatile organohalogen compounds in common beverages was tested. Both enrichment tech-niques were used in combination with gas chromatography – electron capture detection (GC-ECD). TLHS, combined with direct aqueous injection (DAI)-GC-ECD, proved applicable in the determination of volatile organohalogen compounds in all studied beverages, while the PT in a version with no preliminary sample pre-treatment was of limited applicability. Detection limits of the TLHS-based procedure were in the order of 1 ppt. Content of volatile organohalogen compounds in a number of beverages available on the Polish market including mineral waters, beers, juices, carbonated and non-carbonated soft drinks, etc. was determined by means of TLHS-DAI-GC-ECD.     

天津钢管公司DRC直接还原厂生产工艺与自动控制

天津钢管公司DRC直接还原厂将采用英国戴维国际工程公司的DRC煤基直接还原技术,以铁矿石、煤、石灰石为原燃料,用回转窑来生产直接还原铁(DRI)。该厂将由两条回转窑生产线组成,每条生产线的生产能力为15万tDRI/年,回转窑规格为φ5.0m×80m。工厂生产主线将采用计算机集散控制系统(DCS)以实现对生产过程的自动控制。     

Reduction of Stibnite at Moderate Temperature

Reduction of stibnite with hydrogen in the presence of calcium oxide has been experimentally inves-tigated at moderate temperature. The results reveal that the effluent generated in the reduction pro-cess contains much less air-polluting substance H_2S, and that the reaction activation energy is63. 3 kJ/mol. The form of antimony changes considerably when the reaction temperature varies.     

The performance of a direct-sequence spread-spectrum acquisition system using a linear prediction filter for narrowband interference suppression

The coarse acquisition performance of a direct sequence spread-spectrum receiver is analyzed when a linear prediction filter is used for narrowband interference suppression. We show that once an appropriate matching strategy is identified, the linear prediction filter can provide favorable performance when narrowband interference is present over a considerable range of both interference power and bandwidth. In addition, the presence of the filter dramatically improves the performance over the case where there is no filter, except when the interference bandwidth and the power are both small (i.e., when the processing gain provides sufficient interference immunity without the filter). If long spreading sequences are used with moderately sized observation windows, the acquisition performance can be severely degraded when a parallel acquisition scheme is used due to the linear predication filter. We show, however, that a slower serial receiver will provide reliable performance.This work was supported in part by the Office of Naval Research under contract ONR N00014-91-J-1234, the Army Research Office under contract ARO DAAL03-91-0071, and the NSF Center for Ultra-High Speed Circuits and Systems (ICAS).     

钒钛磁铁精矿的烧结特性及强化措施

阐述了钒钛磁铁精矿的矿石特点，烧结特性及其与烧结矿质量之间的关系，并提出了强化烧结的措施。     

PTS瞬态流动与换热数值模拟研究

为了研究压水堆因“直接安注”冷水注入压力容器下降环腔而导致的承压热冲击（PTS）热工水力问题,基于1:10比例模型,应用计算流体力学软件FLUENT5.4进行了紊流流动换热的数值模拟分析,同时进行了常压瞬态传热实验研究。针对下降环腔折算流速0.5 m/s,安注流速10m/s的典型工况,研究了安注水开启后下降环腔内的瞬态流动换热特性,数值模拟与实验结果吻合良好。考察了压力容器安注接管出口区环形焊缝区及堆芯段筒体中子强辐照区所承受的热冲击状况,基于稳态流动研究了下降环腔内流体混合特性及流动机理,为热冲击分析提供参考。     

直流励磁机电刷打火的常见原因及对策

主要介绍了中铝公司山西分公司自备热电厂6台发电机组的励磁机电刷打火的常见原因的分析和处理方法。     

催化反应精馏制备乙酸乙酯

利用反应精馏装置研究了乙酸和乙醇直接酯化法合成乙酸乙酯的转化条件:加热温度200 ℃,浓硫酸质量占混和物总质量0.6%,回流比为3∶1,乙酸与乙醇的摩尔比为1.15∶1.以反应精馏方式进行时,乙醇转化率、乙酸乙酯收率分别为94.09%和60.45%,明显高于普通蒸馏法,而乙醇转化为乙酸乙酯的选择性变化不大.     

直接成像技术在PCB中的应用

电子产品日趋小型化、轻量化、多功能化，使电路板线路密度增加，从而对电路板的制作技术有了更高的要求，普通的接触曝光成像技术不能满足高密度电路的要求，激光直接成像（LDI）技术正迎合了精细线路的要求，而在PCB制作中得到应用。介绍了LDI的成像原理、存在的优缺点及其在PCB制作中的应用。     

通过直接栅电流测量研究PMOSFET's热载流子损伤

通过直接栅电流测量方法研究了热载流子退化和高栅压退火过程中PMOSFET's热载流子损伤的生长规律.由此,给出了热载流子引起PMOSFET's器件参数退化的准确物理解释.并证明了直接栅电流测量是一种很好的研究器件损伤生长和器件参数退化的实验方法.