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81.
82.
杜仲籽油混合脂肪酸制备工艺优化及脂肪酸组成分析 总被引:1,自引:0,他引:1
以杜仲籽油为原料,在常压下皂化水解并用正己烷萃取制备杜仲籽油混合脂肪酸.在单因素超碱量、KOH-乙醇溶液/油的比例、皂化温度、皂化时间和酸化pH研究的基础上,选取超碱量、皂化温度、皂化时间和酸化pH四个因素,应用响应面设计中的Box-Behnken设计对皂化工艺进行优化并得到回归模型,通过气质联用仪分析杜仲籽油脂肪酸的组成.结果表明,制备杜仲籽油混合脂肪酸的优化工艺条件为:超量碱52%,皂化温度77℃,皂化时间82min,酸化pH2.7,在此优化条件下,测得混合脂肪酸的酸值为159.19mg KOH/g.气质联用仪分析结果显示杜仲籽油混合脂肪酸中α-亚麻酸的相对含量可达60.14%,可以作为进一步分离提取杜仲籽油α-亚麻酸的原料. 相似文献
83.
《分离科学与技术》2012,47(17):2639-2648
Comminution is an energy intensive process. A small change in efficiency can lead to substantial benefits in an overall economy of the process plant. This study focused on the comparison of vertical stirred mill agitator designs. A double helical screw agitator was designed for this purpose. A series of stirred mill experiments were performed with two types of agitator designs a standard pin type and CSIRO’s designed double helical screw stirrers. The effects of operating parameters such as grinding time, stirrer speed, and pulp density on grinding performance was investigated using a magnetite concentrate. Grinding performance was analyzed by considering the product fineness and the energy consumption. The test results show that the grinding time and stirrer speed played a significant role; however, the pulp density had little impact on grinding performance in both cases of agitator designs. The 80% passing target product size of 38 μm was obtained with double helical screw agitator in 20 min of grinding with an expend of 10.53 kWh/t specific energy, whereas, the target product size of 38 μm was achieved with the pin type stirrer at the rate of 21.73 kWh/t. It is evident that grinding in a vertical stirred mill with a double helical screw is more efficient than that using a pin type stirrer in terms of the product size distribution and the specific energy consumption. It is concluded that the double helical screw design provides better energy efficiency compared to the pin type stirrer design. The models were developed for the responses P80 and Ecs. Both models show high regression coefficients thus ensuring a satisfactory of models with experimental data. The model equations developed were then optimized using a quadratic programming to minimize the P80 size at minimum specific energy. 相似文献
84.
85.
利用响应面分析法优化产酸丙酸杆菌发酵产酸培养基.在单因素试验的基础上,采用Box-Behnken试验设计,选定甘油、混合氮源(酵母提取物:胰酶大豆肉汤=2∶1)和磷酸氢二钾3个关键因子为响应因子,以丙酸产量为响应值建立多元二次回归方程,在分析各个因素的显著性和交互作用后,确定了产酸丙酸杆菌发酵产酸的最优培养基为:甘油44.4g/L、混合氮源(酵母提取物:胰酶大豆肉汤=2∶1)27.0g/L、K2HPO4 2.0g/L,丙酸产量最大预测值为20.75g/L.经过优化,丙酸产量提高了151%,实验值与预测值基本相符. 相似文献
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87.
It is well known that ozone can be used as a bleaching agent for cellulosic textile materials. In the context of this study, investigations were undertaken to optimize bleaching of linen fabrics using Box-Behnken Experimental Design. The bleaching process involved two distinct steps where linen fabrics were ozonated under different treatment times then the latter in a subsequent step were subjected to hydrogen peroxide bleaching under a variety of conditions. As a result of study, three optimum recipes were achieved and pretreatment with ozone for 15 min before peroxide bleaching supplies time and chemical savings. 相似文献
88.
89.
研究碳源、氮源、无机盐对红曲霉M2固态发酵产生淀粉酶的酶活性影响。在单因素试验的基础上,采用响应面试验设计对红曲霉固态发酵产生淀粉酶的培养基进行优化,并建立乳糖、(NH4)2SO4、K2HPO4变化的二次回归方程,探讨各因素对生淀粉酶酶活力的影响。在固态发酵基础培养基中,最终确定适宜的培养基条件为:乳糖添加量为8.18%、(NH4)2SO4添加量为6.36%、K2HPO4添加量为0.91%;在该条件下可得到红曲霉M2产生淀粉酶的最大酶活力,预测值为680.29 U/g,对实验结果进行验证,得到生淀粉酶酶活力为662.21 U/g。 相似文献
90.
Pravin WAKTE Ajit PATIL Bhusari SACHIN Munnaza QUAZI Shraddha JABDE Devanand SHINDE 《Frontiers of Chemical Science and Engineering》2014,8(4):445
The response surface methodology was employed to study the optimization of microwave-assisted extraction of picroside I and picroside II from Picrorrhiza kurroa Royle rhizomes. The effects of solid to solvent ratio, and extraction temperature, time and solvent on the yields of picroside I and picroside II have been investigated using Box-Behnken experimental design. The experimental data were fitted to second-order polynomial equations using multiple regression analysis and analyzed using the appropriate statistical method. By solving the regression equation and analyzing 3-D plots, the optimum extraction conditions were found to be: solid to solvent ratio, 10 : 90 (w/v); temperature, 60 °C; and extraction time, 60 s. Under the optimal conditions, the yields of picroside I and picroside II are 41.23 and 6.12 mg·g–1 feed respectively, which are in good agreement with the predicted values. The ratio of solid to solvent significantly affects the yields of picroside I and picroside II. Application of microwave-assisted extraction of picroside I and picroside II from P. kurroa would dramatically reduce extraction time and solvent consumption. 相似文献