MDI聚氨酯/聚硅氧烷IPN的结构与力学性能

用MDI聚醚氨酯和含少量苯基的聚二甲基硅氧烷合成了一系列的聚氨酯／聚硅氧烷IPN阻尼弹性体，研究了材料的结构与力学性能．结果表明，当聚氨酯与聚硅氧烷的质量比为90：10时。IPN的抗张强度达41．57MPa，断裂伸长率为376％，并具有良好的阻尼性能，玻璃化转变温度范围大于80℃．聚氨酯／聚硅氧烷IPN具有细微的微相分离结构，聚硅氧烷在IPN中的微相尺寸为微米级，并趋向于分布在IPN的表面．     

Review on testers for measuring flow properties of bulk solids

 The author was asked by the International Fine Particle Research Institue (IFPRI) to write a critical review on shear testers for IFPRI-members. The review was delivered to IFPRI in summer 1999. Following the contract with IFPRI it was not allowed to publish the review elsewhere for at least two years. Granular Matter invited the author to submit the review in the original form; during the refereeing process (besides other changes) it turned out that some remarks should be added here for clarification: - Since 1999, the author is not aware of a really new device for testing bulk solid properties, which could lead to a change of the general comments and conclusions provided in the review. It was argued, that the review is referring too much to the work of Jenike, while the works of Johanson and Peschl were not adequately cited. Both are excellent engineers with a lot of experience, but their basic ideas are not available in published form, and if, they are not set in relation to alternative approaches so that an objective comparison in detail would be a future research issue rather than a topic in this report. A discussion on the influence of electrostatic charges was missing. There hardly is an influence, since the particles are in continuous contact. Only with non-conducting plastic particles electrostatic charges could cause problems. But no relevant experiments and results are known. In closed systems, the effect of electric charges is thus mainly neglected, but it is clear that electrostatic forces are eminent in flows with a free surface – an issue not addressed in this review. Received: 1 November 2002     

L-乳酸和聚乳酸的研究进展

综述了乳酸发酵和提取工艺以及聚乳酸的合成进展,分析了L-乳酸及合成聚乳酸两种产品的市场前景,对进一步的技术开发提出了建议。     

等径弯角挤压工艺(ECAEP)研究现状

等径弯角挤压是制备块状细晶材料的一种大塑性变形工艺，目前得到国内外高度重视．本文简要介绍了等径弯角挤压工艺的基本原理和变形特点，从理论上对其变形方式和机理进行了分析，并详细介绍了该工艺的应用领域。     

硫酸锆、碳酸锆的性质、应用及生产技术综述

综述了硫酸锆，碳酸锆产品的性质，生产技术及应用，收集整理了国内外部分厂家和公司该产品的化学指标与生产技术；介绍了“分步液相沉淀法”生产工艺，与“一步法”生产工艺相比，其具有流程短，投入少，操作简单，制造成本低等优点。     

化学气相沉积铜薄膜研究进展

本文综术了集成电路工艺的Cu布线中Cu薄膜化学气相沉积(CVD)的研究背景,详细介绍了CVD生长Cu金属薄膜的国内外研究进展及CVD对前趋物的要求,并对前趋物的一些物理、化学性质进行了总结,最后,对薄膜沉积的计算机摸拟作了简要介绍。     

Understanding and Modeling the Effect of Surfactants in Enhanced Particle Removal from Surfaces in Aqueous Media

The removal of particulate contamination is a critical issue for many manufacturing processes. It is particularly critical to the electronics industry in which small pieces of microscopic debris remaining after chemical mechanical planarization (cmp) using submicron polishing particles can cause device failure. One way to enhance particle removal following the cmp process is to utilize surfactants. Recent research has shown ways to model the effect of surfactants on enhanced particle removal. However, previous research has not demonstrated the effect of ionic strength on enhanced particle removal associated with surfactant use. Past research has also not shown the combined effects of ionic strength and surfactant concentration on enhanced particle removal using surfactants. This article summarizes the parameters affecting particle removal, and it provides data and analysis on the effect of ionic strength as well as the combined effects of ionic strength and surfactant concentration on particle removal following cmp processing.     

Study of the morphology and mechanical properties of polypropylene composites with silica or rice‐husk

The mechanical, morphological behavior and water absorption characteristics of polypropylene (PP) and silica, or PP and rice‐husk, composites have been studied. The silica used in this study as filler was a commercial type produced from soluble glass or rice husks. The compatibilizing effect of PP grafted with monomethyl itaconate (PP‐g‐MMI) and/or with vinyltriethoxysilane (PP‐g‐VTES) as polar monomers on the mechanical properties and water absorption was also investigated. In general, a high loading of the studied fillers in the polymer matrix increases the stiffness and the water absorption capacity. This effect is more noticeable in the tensile modulus of the PP/silica composite with PP‐g‐VTES as compatibilizer. However, the increase of the rice‐husk charge as a natural filler in the PP matrix decreases the stiffness, and in the presence of PP‐g‐MMI as compatibilizer in PP/rice‐husk, the tensile modulus and water absorption of the composite were improved. The better adhesion and phase continuity in the PP/silica and PP/rice‐husk composites with different compatibilizers was confirmed by the morphological study. Copyright © 2004 Society of Chemical Industry     

应用于空间关联规则挖掘的ILP方法

文章介绍了应用于空间关联规则挖掘的ILP方法。ILP方法全称为归纳逻辑程序设计,这种方法有利于从空间领域发现有价值的知识,系统地研究地理层的层次结构,处理诸多空间对象的空间特性。这种方法已在一个ILP系统SPADA中实现,该文将通过SPADA应用空间数据的一些实例来说明ILP方法的特点。     

玉米须单体成分纯化及类别鉴定

以玉米须浸膏为原料,采用萃取和液相制备色谱相结合的办法分离得到高纯度玉米须黄酮单体,并优化出纯化工艺。