使用毛细管电泳定量分析黑白显影液衰退反应中的对苯二酚和对苯二酚单磺酸盐

使用毛细管电泳分离并定量分析了对苯二酚——— 1种黑白显影液中的显影剂和它的衰退反应产物对苯二酚单磺酸盐。优化了的毛细管电泳分离。     

油田采出水的精细过滤技术

低渗透油层渗透率〈0．1μm^2，孔喉半径小，容易被堵塞，对注入水质要求高，目前缺乏对含有原油、化学添加剂、粉质颗粒和无机盐的油田采出水适应性强的精细过滤设备。本文介绍了油田采出水回注精细过滤材料试验和采用旋流配水、脉冲水流反洗技术的改性聚四氟乙烯滤芯过滤装置的小试和中试研究情况，研究开发的改性聚四氟乙烯精细过滤装置，当进水含油量〈20mg／L、悬浮物含量〈20mg／L时，出水达到了（《碎屑岩油藏注水水质推荐指标》（SY5329-94）规定的A1级注水水质标准。     

(Ag)_核·(Au)_壳复合纳米粒子的制备

以银原子团簇作晶种,采用微波高压液相合成法制备了分散性好、规则球形的(Ag)核·(Au)壳复合纳米粒子。研究了(Ag)核·(Au)壳复合纳米粒子的紫外可见吸收光谱和共振散射光谱特性。结果表明,液相(Ag)核·(Au)壳复合纳米粒子和高压微波合成的液相金纳米粒子的最强共振散射峰均在580nm处,它们的吸收光谱图相似,最大吸收分别在518.5nm和524.8nm。     

Swelling kinetics of a hydrogel of poly(ethylene glycol) and poly(acrylamide‐co‐styrene)

A hydrogel incorporating the hydrophilic polymer poly(ethylene glycol) and a copolymer of acrylamide and styrene was synthesized, and the dynamics of the water‐sorption process were studied. The effects of the composition of the hydrogel and the temperature of the swelling medium were investigated with respect to the water‐sorption characteristics of the hydrogel, and the kinetic parameters, including the swelling exponent and diffusion constant, were evaluated. The hydrogel was also judged for the antithrombogenic property of its surface. The experimental findings were explained on the basis of the core–shell polymeric structure of the hydrogel. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 1419–1428, 2002     

基于AMBA总线的IIC协议IP核设计与验证

介绍了一种基于AMBA总线verilogHDL实现的IIC主机模式的IP核设计。该模块能够在标准和快速模式下运行,能够灵活配置为十位地址寻址或七位地址寻址模式。详细说明了该IP核的架构,各部分设计及状态转换过程。最后该模块通过了系统验证,并在xilinxFPGA上转化为硬件电路实现了所有功能。     

基于谈判集的模糊合作博弈的收益分配方案

为了弥补核心作为博弈解可能为空集的缺陷,将经典合作博弈中的谈判集解拓展到模糊合作博弈中,提出了模糊合作博弈的模糊谈判集的概念.探讨模糊网络博弈的模糊谈判集和核心的等价性质,并对相关结论加以证明.研究表明,模糊合作博弈的模糊谈判集是经典合作博弈谈判集的自然拓展,该结果丰富了对模糊合作博弈的解的研究,也表明了模糊网络博弈核心的非空性,进而保证其最优分配方案的存在性.     

一种交互式的岩心图像修补方法

传统的岩心图像修补方法往往无法对不同宽度的待修补域达到理想效果,并且难以对待修补区域做出选择,这在实际应用中很难满足需要。针对这些问题,提出基于联合一阶与二阶全变差（Combined TV-TV2）的交互式岩心修补方法。该方法首先进行均值漂移对图像进行预分割,然后使用基于区域合并的交互式最大相似度算法确定待修补的区域,最后以联合TV-TV2修补模型为基础,应用分裂Bregman迭代进行求解。实验结果表明,待修补的区域能够被确定,而对于不同宽度的修补区域,该算法能够获得满意的修补效果。     

Investigation of the effect of surface phosphate ester dispersant on viscosity by coarse-grain modeling of BaTiO slurry

To understand the role of phosphate ester dispersant, we investigated the rheology of a BaTiO slurry. For the model case, a coarse-grain molecular dynamics (CGMD) simulation was performed with the butyral polymer didodecyl hydrogen phosphate (DHP) in the toluene/ethanol solvent. By systematically analyzing the effect of DHP from an atomic-scale first principle and from all-atom MD to microscale CGMD simulation, we investigated how the adsorption of a DHP dispersant on a BaTiO surface affects the microstructure rheology of a BaTiO slurry. The first-principle and all-atom MD simulation suggests that DHP molecules prefer to locate near the BaTiO surface. CGMD simulation shows a reduction in viscosity with an increase in dispersants, suggesting that the dispersant population near the BaTiO surface plays a key role in controlling the rheology of the BaTiO slurry. In this study, we propose an approach for understanding the BaTiO slurry with molecular-level simulations, which would be a useful tool for efficient optimization of slurry preparation.     

Grafting poly(t‐butyl acrylate) to poly(allylamine) by inverse microemulsion radical polymerization: From comb‐polymer to amphiphilic shell crosslinked polymer nanocapsule

An interfacial grafting radical polymerization method for amphiphilic comb copolymer and shell crosslinked polymer nanocapsules was reported. Macropolyradicals on a water soluble long chain polyamine were generated with hydrogen peroxide in the water phase and subsequent grafting radical polymerization of a vinylic monomer at the water/oil interface proceeded at 65°C. In the presence of a crosslinker, the resulting graft copolymer formed a defined core‐shell structure with hydrophilic aqueous core functionalized by the polyamine and a hydrophobic crosslinked polymer shell. The structure of the core‐shell material was characterized by NMR, FTIR, DSC, TGA, SEM, TEM, and the mechanism of the graft polymerization is proposed. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 1905–1911, 2007     

新型碳纤维复合芯导线在输电线路中的应用分析

新型碳纤维复合芯导线具有良好的力学性能和电气特性,与等径钢芯铝绞线相比,其主要有芯线强度高、导电率高、载流量大、质量轻、耐腐蚀、弧垂小等优点;与普通碳纤维导线相比,新型碳纤维复合芯导线采用铝包覆技术,在配套金具、导线压接和施工工艺等方面都有较大改进。以110～500 kV新建线路为例,对185～800 mm~2截面的新型碳纤维复合芯导线进行了全面的经济性比较。研究结果得到:对于500 kV新建双回线路,推荐采用JLRX1/F2A-710/50、JLRX1/F2A-800/50导线;对于220 kV新建双回线路,推荐采用JLRX1/F2A-400/50、JLRX1/F2A-450/50导线;对于110 kV新建双回线路,推荐采用JLRX1/F2A-300/40、JLRX1/F2A-360/40导线。