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The apparent density and porosity of four rice cultivars, Koshihikari, Yumepirika, Habutaemochi, and Kitayukimochi, decreased and increased, respectively, with the increasing temperature in the range of 5 °C to 60 °C. Especially large changes in both apparent density and porosity were observed at 60 °C, which can be ascribed to the starch gelatinization of rice. The swelling pressures of wet rice grains were estimated to be 7.5, 6.3, 6.2, and 5.9 MPa at 25 °C for Koshihikari, Yumepirika, Habutaemochi, and Kitayukimochi, respectively, from the distribution coefficients of solutes with different molar volumes. Rice grains having higher amylose content exhibited a weak tendency toward higher swelling pressure. The distribution coefficients of fructose for the Koshihikari and Habutaemochi cultivars were larger at higher temperatures, but the temperature dependence of the swelling pressure was not significant for both cultivars. These results suggested that the increase in the distribution coefficient was caused by the gradual relaxation of the interior structure of rice with increasing temperature. 相似文献
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Zuo-Peng Zhang Ye Zhong Zhen-Bin Han Lin Zhou Hua-Sheng Su Jian Wang Yang Liu Mao-Sheng Cheng 《International journal of molecular sciences》2021,22(11)
A series of saccharide-modified thiadiazole sulfonamide derivatives has been designed and synthesized by the “tail approach” and evaluated for inhibitory activity against carbonic anhydrases II, IX, and XII. Most of the compounds showed high topological polar surface area (TPSA) values and excellent enzyme inhibitory activity. The impacts of some compounds on the viability of HT-29, MDA-MB-231, and MG-63 human cancer cell lines were examined under both normoxic and hypoxic conditions, and they showed certain inhibitory effects on cell viability. Moreover, it was found that the series of compounds had the ability to raise the pH of the tumor cell microenvironment. All the results proved that saccharide-modified thiadiazole sulfonamides have important research prospects for the development of CA IX inhibitors. 相似文献
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Natural polysaccharides (NPS) are regarded as biomolecular and structural components for preparing high-performance tough hydrogels. But the one-step fabrication of NPS-containing hydrogels in seconds and the template-free design of complicated high-resolution structures are still significant challenges in this field. To meet these requirements, various NPS-containing tough hydrogels are fabricated and processed into 2D/3D structures via the combination of Ru(bpy)32+-mediated photochemistry and extrusion 3D printing technique. The whole fabrication process is one-step, completed in tens of seconds under visible light irradiation. It is found that the used NPS plays a key role in achieving the fabrication of high-performance structured tough hydrogels. The high reactivity of functional groups in the used NPS can shorten their gelation times. Long rigid chains of the used NPS, their hierarchical assemblies, and contrasting multinetworks benefit from the efficient dissipation of mechanical energy and enhancement of its operational stability. Strong supramolecular interactions enable hydrogel precursors to have high viscosities, therefore providing good controllability to design high-resolution and complicated tough hydrogel structures via extrusion 3D printing. It is anticipated that this straightforward fabrication strategy and findings will open new horizons for NPS-containing materials. 相似文献
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Wey Yang Teoh Frans Denny Rose Amal Donia Friedmann Lutz Mädler Sotiris E. Pratsinis 《Topics in Catalysis》2007,44(4):489-497
A comparative photocatalytic analysis was carried out on TiO2 made in a Flame Spray Pyrolysis (FSP) process and flame-made Degussa P25. Both have similar crystallinity, phase composition,
phase segregation and a non-porous surface. Hence comparison was made based on their difference in specific surface area,
organic adsorption and the amount of OH• generated upon illumination. The photocatalytic activity tests were carried out using
the following series of organic compounds: sucrose, glucose, fructose, maleic acid, glyoxylic acid, oxalic acid, isobutyric
acid, phenol and methanol. FSP-made TiO2 outperformed P25 for saccharides mineralisation, while for phenol and methanol mineralisation P25 was better than FSP-made
TiO2. Similar mineralisation rates were observed for both FSP-made and P25 TiO2 for the mineralisation of carboxylic acids. This shows that the relative performance of the photocatalysts depends on the
type of organic compounds to be degraded. The high surface area and possibly a more efficient interfacial charge transfer
of FSP-made TiO2 provided an efficient pathway for saccharides mineralisation. As for phenol and methanol, the mineralisation rates were higher
when using P25 due to the greater amount of OH• radicals generated by this photocatalyst. The fast mineralisation rates of
carboxylic acids made degradation of these organic compounds to be less affected by the TiO2 photocatalyst properties and conditions tested in this work. 相似文献
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Dr. Vimary Vázquez‐Dorbatt Juneyoung Lee En‐Wei Lin Prof. Heather D. Maynard 《Chembiochem : a European journal of chemical biology》2012,13(17):2478-2487
Natural saccharides are involved in numerous biological processes. It has been shown that these carbohydrates play a role in cell adhesion and proliferation, as well as protein stabilization, organization, and recognition. Certain carbohydrates also serve as receptors for viruses and bacteria. They are over expressed in diseases such as cancer. Hence, a lot of effort has been focused on mimicking these sugars. Polymers with pendent saccharide groups, also known as glycopolymers, are studied as oligo‐ and polysaccharide mimics. Controlled radical polymerization (CRP) techniques such as atom transfer radical polymerization (ATRP), reversible addition–fragmentation chain transfer (RAFT) polymerization, and nitroxide‐mediated polymerization (NMP), as well as cyanoxyl‐mediated free radical polymerization have allowed chemists to synthesize well‐defined glycopolymers that, in some cases, have particular end‐group functionalities. This review focuses on the synthesis of glycopolymers by these methods and the applications of glycopolymers as natural saccharide mimics. 相似文献
9.
目的 建立竹芋粉中总还原糖含量的 3,5-二硝基水杨酸(DNS)比色测定方法。 方法 以葡萄糖为标
准品, 以 3,5-二硝基水杨酸(DNS)为显色剂, 用分光光度法测定竹芋粉中总还原糖的含量。 结果 在最大吸收
波长为 480 nm, 测得回收率为 98.3%~101.2%, 相对标准偏差为?1.7%, 竹芋粉中总还原糖含量为 77.83%, 竹
芋粉中淀粉含量为 70.05 %。结论 本方法适用于竹芋粉中总还原糖含量的测定。 相似文献
10.
与常用的玉米、木薯淀粉比较 ,用TermamglTypeLSPlus高温α -淀粉酶作用糯、粳、籼等品种的稻米粉 ,以高效液相色谱测定其液化过程糖组分的变化 ,研究了米粉液化水解速度和程度的规律 ,以及“α -淀粉酶极限糊精”的存在 相似文献