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Chemical modification (CM) and deposition-precipitation (DP) methods were used for the dispersion of active Au nanoparticles on mesoporous silica materials in this work. XRD, TEM, N2 adsorption isotherms and UV-Vis absorption spectra were used to characterize in detail Au-SBA-15 materials prepared by the two methods. The analysis results showed that high loading (1.7%, by mass) and uniform Au nanoparticles (approximately 3 nm) were dispersed in the channels of mesoporous SBA-15 by the CM method. While for the DP method, most of Au nanoparticles with the size of 10—15nm were aggregated outside of the channels of SBA-15 and the actual loading of Au was only 0.38% (by mass). 相似文献
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样品漂移是影响透射电子显微镜分辨率的重要因素之一。近年来有一系列关于透射电镜图像漂移校正的算法,如Unblur、MotionCor和MotionCor2等,在冷冻电镜三维重构方面应用效果显著,但无法应用于材料表征电镜通常配备的CCD相机的图像漂移校正。本文提出了一种基于图像分割和盲反卷积的透射电镜图像漂移校正方法,在Goldstein和Fattal提出的利用功率谱的统计不规则性估计卷积核算法的基础上,利用图像分割解决了电镜图像样品部分和背景部分的运动方式不一致问题,能够应用于CCD相机的图像漂移校正。实验结果表明,本文的方法能够有效提高电镜图像的分辨率。 相似文献
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