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微合金钢连铸过程频发铸坯角部裂纹缺陷是钢铁行业的共性技术难题。基于微合金钢铸坯角部裂纹组织结构与析出特征检测,以及铸坯在结晶器与二冷铸流内的凝固热/力学行为演变规律定量化模拟,开发形成了基于新型角部高效传热曲面结晶器和铸坯二冷高温区角部晶粒超细化控冷工艺与装备的微合金钢连铸坯角部裂纹控制技术。研究结果表明,传统板坯连铸工艺下,窄面直线型结晶器无法充分补偿坯壳收缩,致使厚保护渣膜与气隙在坯壳角部集中生成,大幅降低了结晶器中下部坯壳角部传热,引发微合金碳氮化物沿奥氏体晶界析出。传统二冷配水条件下,奥氏体晶界不可避免生成先共析铁素体膜低塑性组织。两者共同作用致使铸坯角部高温塑性不足而引发裂纹。通过开发新型曲面结晶器,坯壳角部于其内高效传热,凝固全程冷却速度大于5℃/s,弥散化了微合金碳氮化物高温析出。同时,基于窄面足辊超强冷新控冷结构,对铸坯角部实施γ→α→γ循环相变,铸坯角部晶粒显著超细化,高塑化控制了铸坯角部裂纹产生。 相似文献
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微合金钢连铸过程频发铸坯角部裂纹缺陷是钢铁行业的共性技术难题。基于微合金钢铸坯角部裂纹组织结构与析出特征检测,以及铸坯在结晶器与二冷铸流内的凝固热/力学行为演变规律定量化模拟,开发形成了基于新型角部高效传热曲面结晶器和铸坯二冷高温区角部晶粒超细化控冷工艺与装备的微合金钢连铸坯角部裂纹控制技术。研究结果表明,传统板坯连铸工艺下,窄面直线型结晶器无法充分补偿坯壳收缩,致使厚保护渣膜与气隙在坯壳角部集中生成,大幅降低了结晶器中下部坯壳角部传热,引发微合金碳氮化物沿奥氏体晶界析出。传统二冷配水条件下,奥氏体晶界不可避免生成先共析铁素体膜低塑性组织。两者共同作用致使铸坯角部高温塑性不足而引发裂纹。通过开发新型曲面结晶器,坯壳角部于其内高效传热,凝固全程冷却速度大于5℃/s,弥散化了微合金碳氮化物高温析出。同时,基于窄面足辊超强冷新控冷结构,对铸坯角部实施γ→α→γ循环相变,铸坯角部晶粒显著超细化,高塑化控制了铸坯角部裂纹产生。 相似文献
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采用金相分析方法对低合金高强度钢(/%:0.16~0.18C,0.20~0.40Si,1.42~1.55Mn, ≤0.025P, ≤0.012S,0.015~0.025Nb,0.100~0.115V,0.010 0~0.0150N)连铸板坯窄面微裂纹的产生机理进行了分析研究。结果表明:板坯窄面表层显微组织不合理如奥氏体晶粒粗大、奥氏体晶界处先共析铁素体膜的形成以及第二相质点在奥氏体晶界处的偏析等是微裂纹产生的机理。通过优化连铸板坯窄面冷却工艺,将窄面冷却水量增加35%;细化了晶粒,抑制了铁素体膜的产生,改变了第二相质点析出,改善了铸坯表层组织,消除了铸坯窄面微裂纹缺陷。 相似文献
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本文论述了通过控制连铸板坯的显微组织来预防横向裂纹的技术。所谓裂纹就是由于众所周知的沿奥氏体晶粒边界析出的薄层状铁素体所造成的。为更清楚了解裂纹敏感性和铸坯组织结构之间的关系,对铸坯冷却和连铸坯冷却都进行了试验,同时也讨论了冷却方式对铸坯显微组织的影响。同普通连铸中二次冷却的弱冷变化相比,在浇注后直接进行强冷将阻止薄层状铁素体的形成。由于可将裂纹源-薄层状铁素体变短小,故可防止横向裂纹的产生。在各 相似文献
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为明确不同速度冷却时表面奥氏体的长大规律和在第Ⅲ脆性区的热塑性,用Gleeble-3500热模拟机分别对钛铌微合金钢进行了奥氏体长大热模拟试验和第Ⅲ脆性区热拉伸试验。研究结果表明,当冷却速率小于5℃/s时,钛铌微合金钢铸坯表面容易形成粗大的(大于1mm)奥氏体晶粒;随着冷却速率的增大,奥氏体边界析出细小的Ti(C,N),能有效地钉扎限制奥氏体的长大。在热拉伸试验过程中,当冷却速率为1和5℃/s时,钛铌微合金钢铸坯在800℃热拉伸时断面收缩率仅为29.7%和23.0%,2种冷速下都伴随有70~200nm矩形或不规则形的(Ti,Nb)(C,N)和40~100nm针状的Nb(C,N)析出。铸坯角部振痕谷底处在高温低冷速下形成粗大奥氏体晶粒,并在第Ⅲ脆性区矫直,是导致钛铌微合金钢角部横裂纹敏感性高的主要原因。 相似文献
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本文基于薄板坯连铸连轧流程物理冶金特征,系统地研究了V的析出规律和V微合金钢的强化机理.结果表明,均热前铸坯中有大量细小V析出物,均热过程中部分析出物溶解,颗粒略有长大;铸坯中的细小析出物对抑制变形奥氏体再结晶晶粒长大有明显的作用,使试验钢具有晶粒尺寸为3~4μm的超细晶组织;组织超细化是导致薄板坯连铸连轧流程V微合金钢强度提高的主要原因.采用薄板坯连铸连轧流程V微合金化技术开发了屈服强度550MPa级HSLAS-F80高强钢,其组织均匀、晶粒超细化、强度高、成型性能和焊接性能优良. 相似文献
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《钢铁》2018,(11)
为了研究铌钛微合金钢铸坯表面横裂纹产生的原因,采用金相观察、扫描电镜观察和电子背散射衍射(EBSD)等研究方法,对比分析铌钛微合金钢连铸坯和实验室铸锭的晶界铁素体微观组织特征。结果发现了两类晶界铁素体,一类是晶界一侧呈线性清晰另一侧曲折不清晰类型(称之为晶界一侧清晰型,GF-I型);第二类是晶界两侧均为曲折不清晰类型(称之为晶界两侧不清晰型GF-II型),在晶界铁素体中均观察到了呈链状线性分布的微孔洞。在GF-I型晶界铁素体中,微孔洞沿晶界清晰一侧呈链状一列分布;在GF-II晶界铁素体中,微孔洞呈链状分布在晶界铁素体中间部位。晶界铌钛微合金粒子的析出促进了晶界铁素体的形核,是导致晶界铁素体中的链状微孔洞形成的重要因素。由于铌钛微合金粒子沿着原奥氏体晶界析出钉扎了原奥氏体晶界,同时也钉扎了晶界铁素体的清晰一侧晶界,改变了晶界铁素体的生长方向,使GF-I型的生长方向向着曲折一侧或沿着原奥氏体晶界生长。对于GF-II型铁素体,由于析出粒子的钉扎作用,奥氏体晶界没有发生移动,铁素体是向两侧奥氏体内长大机制。晶界微孔洞是连铸坯表面横裂纹产生和扩展的原因。 相似文献
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为了控制梅钢1 650板坯连铸包晶钢过程铸坯内裂纹发生,基于梅钢1 650板坯连铸机生产实际,建立了1 560mm×230mm断面包晶钢铸坯凝固过程三维热/力耦合有限元模型,揭示了铸坯凝固过程各冷却区内的温度场分布规律和铸坯压下过程应力与变形行为演变规律。结果表明,铸坯在结晶器及零段内冷却强度大,沿拉坯及其垂直方向的温度分布梯度大;在实施铸坯凝固末端压下过程中,铸坯宽面中心与宽向1/4处的表面变形及应力变化较为同步,且靠近铸坯内弧侧凝固前沿的塑性应变最大,铸坯应力最大值集中在角部区域;目前梅钢包晶钢连铸压下区间设置不当,易引发铸坯产生内部裂纹。 相似文献
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基于唐钢中厚板厂含铌钢板坯连铸生产实际,采用数值模拟方法研究了Q345B- Nb含铌钢板坯连铸过程实施铸坯角部二冷高温区角部组织多相变晶粒细化控冷工艺的可行性。结果表明,通过在结晶器窄面足辊下方增加6组针对铸坯角部强喷淋冷却的喷嘴结构,可使铸坯角部温度下降至约600 ℃,而后减少立弯段中下部3区与4区冷却水量,可使铸坯角部温度回升至900 ℃以上,满足铸坯角部多相变温度控制条件。在此基础上,将新控冷工艺应用于现场实际,实施铸坯二冷高温区多相变控冷新工艺后,铸坯角部距表面0~20 mm范围内的组织均可由传统工艺下“奥氏体+先共析铁素体膜”结构转变成“铁素体+珠光体”结构,且晶粒细化至不大于20 μm,铸坯抗裂纹能力大幅提高,含铌钢连铸坯角部裂纹率由原工艺的5.89%稳定控制在小于0.1%水平。 相似文献
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铸坯表层异常长大的奥氏体晶粒是产生横裂纹的重要原因之一,研究冷却过程对其生长行为的影响对科学制定连铸工艺、降低铸坯裂纹敏感性有重要意义。采用原创连铸坯凝固过程热模拟方法,再现了EH40低碳船板钢板坯的凝固过程,观察在传统板坯连铸条件下,2种结晶器冷却强度对铸坯表层奥氏体晶粒长大行为的影响。结果表明,在结晶器冷却阶段,热模拟坯表层5 mm的绝大多数奥氏体晶粒短轴尺寸均不超过0.5 mm,但已出现粗大晶粒,且强冷条件下奥氏体晶粒尺寸平均值和极大值均更大,分别为弱冷条件下的2.5倍和2.0倍。在足辊区到矫直点区间,表层奥氏体晶粒生长非常缓慢,平均尺寸仍未超过0.5 mm。矫直点处,结晶器强冷热模拟坯表层20 mm的晶粒短轴最大尺寸为2.2 mm,为弱冷条件下的1.7倍。综上,奥氏体晶粒在连铸不同阶段表现为不同的生长行为,且采用结晶器弱冷更有利于EH40钢板坯获得相对细小的表层奥氏体晶粒。 相似文献
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采用连铸圆坯冷送轧制Q345E圆钢,发现表面存在较多裂纹,裂纹长度为20 ~80 mm,呈离散型分布。经检测,裂纹两边发现较严重的脱碳层,裂纹根部存在较多高温氧化质点,未发现非金属夹杂物。理论研究表明,初生奥氏体晶界析出网状铁素体膜是导致钢材断面收缩率降低的根本原因,而Q345E中的Nb含量在特定的温度段降低了钢材的塑性,更加剧了钢材的开裂倾向性。当预热段温度较高(850~900 ℃)时,铸坯快速升温,表面局部发生α→γ的转变,体积收缩不均匀,产生拉应力。当拉应力超过钢材所能承受的极限时,产生表面裂纹。通过对铸坯的预热缓解了内外温度差,有效解决了Q345E热轧圆钢的表面裂纹问题。 相似文献
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�ս��� ������ ����������ʥ�ң���Ԩ�� 《钢铁研究学报》2014,26(10):35-39
The precipitation behavior of MnS and AlN in low-temperature high magnetic induction grain-oriented silicon steel produced by thin slab casting and rolling process with ??acquired inhibitor method?? during continuous casting and soaking was studied by thermodynamic calculation. The calculated results show that AlN is likely to precipitate in ferrite after solidification. However, MnS can precipitate only in the two phase region of ferrite and austenite. Meanwhile, MnS and AlN in the steel can not be completely dissolved during the soaking stage. In addition, the abnormal growth of primary grain is not obvious after high-temperature nitriding, which indicates the number of inherent inhibitor in the steel is relatively sufficient before nitriding. 相似文献
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The surface quality of continuously cast material is strongly depending on the initial solidification of the steel. Oscillation marks are formed at the very early stages of the strand shell growing process, thus influencing the microstructure and cracking behaviour of the surface and subsurface region. An industrial study of the oscillation mark morphology and the surface structure of peritectic medium carbon steel slabs was performed. The formation of oscillation marks and their effect on the surface quality was examined by metallographic investigations of slab samples. Although constant casting and oscillation conditions were applied, a variation of oscillation mark geometry along the narrow faces of the slabs was measured. A relation between the depth of the oscillation marks and the thickness of a layer of segregated melt situated inside the bottom of the marks was found. Measuring the distribution and length of surface and subsurface segregated cracks in the vicinity of the marks, existing theories of oscillation mark formation could be confirmed. The austenite grain size was found to increase with increasing oscillation mark depth. There was no clear correlation between the austenite and the δ‐ferrite grain size. 相似文献
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《钢铁冶炼》2013,40(7):521-528
AbstractGrowth irregularities in continuous casting are believed to be associated with crack formation and breakouts. Differential thermal analysis on 310S stainless steel samples indicated primary precipitations of both austenite and ferrite during solidification. In tensile tests on solidifying samples, abrupt shrinkages in volume were detected in the peritectic range of temperatures. Micrographic and microsegregation analysis on samples extracted from a breakout shell revealed high ratios of primary-precipitated austenite in the thick sections of the shell, and high ratios of primary-precipitated ferrite in the thin sections. Alternating precipitations of austenite and ferrite are proposed to occur during solidification. Regions of the shell with high ratios of primary austenite remain in contact with the mould and exhibit high growth rates, whereas regions with high ratios of primary ferrite shrink in volume due to the ferrite to austenite transformation, which results in the formation of air gaps between the shell and the mould and reductions in growth rate. 相似文献
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During the continuous casting of low‐carbon Nb–Ti microalloyed steel, control of the slab surface microstructure and the behavior of the second‐phase precipitation are significantly influenced by the cooling rate. Through confocal laser scanning microscopy, the effect of the cooling rate on the behavior of ferrite precipitation both at the grain boundary and within the austenite was observed in situ and analyzed. The relationship between the cooling rate and precipitation of the microalloying elements on the slab surface microstructure was further analyzed by transmission electron microscopy. The results showed that the effect of microalloying element precipitation on proeutectoid ferrite phase transformation is mainly manifested in two aspects: (i) the carbonitrides of microalloying elements act as inoculant particles to promote nucleation of the proeutectoid ferrite and (ii) the carbon near the grain boundary is depleted when the microalloying elements precipitate into carbonitrides, inducing a decrease in the local carbon concentration and promoting ferrite precipitation. 相似文献