固体材料低温热导率测试系统

研制出工程材料低温热导率测试系统.测试采用稳态纵向热流法,高真空绝热恒温器,并利用热开关装置,解决了传统测试方法降温速率慢的问题.通过与标准样品比对,证明测试误差在5%以内.利用该测试系统研究了不锈钢、钛合金及镁合金的低温热导率.     

非金属绝热材料低温热导率测试装置

建立了一套非金属绝热材料低温热导率测试装置,测试采用稳态轴向热流法,高真空绝热,通过可控气体热开关提高了样品的降温速度,运用该装置对聚氨酯隔热材料液氮到室温温区热导率进行了测量,并对装置的重复性以及漏热和误差进行了分析。     

单台G-M制冷机为冷源力学性能测试系统研究

以单台G-M制冷机为冷源,研究设计了一套可满足8—300 K温区内任意温度点稳定可控的材料力学测试系统,满足对材料的拉伸、压缩、弯曲等力学性能的测试要求。该系统利用少量氦气作为导冷介质,为系统内的夹具、样品等降温,降低至最低温度8 K用时14小时。选取8—300 K内多个温度点对系统进行控温测试,验证该系统在8—300 K内具有可连续稳定控温能力。利用电子万能试验机对该系统的性能进行测试,以77 K为低温的典型温度点对5a06铝合金进行拉伸测试,并与平台测试结果进行对比分析,证明该低温力学测试系统的测试结果具有较高的可信度。     

液体低温热导率的测试

介绍了非稳态法测试液体在低温下（－１００～５０℃）的热导率的测试原理、方法，测试了全氟三乙胺的低温热导率。为了提高测试的重复性，采用了相对比较法，并给出了测试装置及测试结果和误差分析。     

制冷机做冷源的低温热导率测量装置研制

设计研制了1套以4.2 K制冷机为冷源的低温热导率快速测量装置.该装置采用可拆卸的具有独立真空环境的样品测试杆,使得样品测试部件与低温冷源部件分离,从而实现不破坏制冷机冷源真空环境及制冷机不复温的情况下快速更换样品.高真空绝热恒温样品杆通过高导热柔性热桥与制冷机冷头良好热耦合.热导率测试采用稳态绝热纵向热流法.除快速测...     

低温阀热锚位置优化及漏热分析

气动低温调节阀是大型氦低温系统中最重要的执行机构,工作在极低温状态下(液氢/液氦温区:20—4 K),低温漏热量是其最重要的技术参数之一。通过在低温阀外管焊接77 K热锚,可以有效降外管的漏热量损失。通过引入热力完善度,优化热锚在外管的相对位置,结果显示:热锚安装的最佳相对位置为0.40,此时外管在4 K温区相对漏热量损失减少了82.5%。     

兰州物理研究所1983年招收攻读硕士学位研究生(低温测试技术)试题(每题20分)

1.低温装置(包括管道、容器等)的绝热方式,常用的有哪几种?举例说明其特点,并作比较评述。 2.简述用稳态法测定固体材料低温热导率的原理,画出装置简图并作简要说明。试作误差分析,由误差分析指出在设计装置和测试中应注意之点。 3.简述固体比热理论,低温下晶格比热和电子比热各遵循何种规律? 4.画出标定温度计用的低温恒温器简图并略加以说明,今欲在4—273K范围分度金铁—镍铬热电偶,回答以下问题:     

纳米AlN分散的Bi_(85)Sb_(15)低温热电性能研究

利用机械合金(MA)和放电等离子(SPS)烧结方法,制备出Bi85Sb15/x mol%AlN(x=0,0.1,0.2,0.3)块体材料。在77—300 K温区内,测试了块体材料的电导率、Seebeck系数、霍尔系数和热导率,并由此计算出材料的zT值。结果表明:纳米AlN分散的Bi85Sb15材料,随着AlN含量的增加,样品的迁移率升高,从而明显提高材料的电导率,但Seebeck系数绝对值呈减小趋势。适量的纳米AlN的引入可以形成散射中心,增加对声子的散射作用,降低热导率。当基体Bi85Sb15中加入0.1mol%AlN时,其zT值在250 K取得最大值~0.32,比基体在此温度下的zT值提高了45%。     

可伐合金复银铜焊料复合带材的研制

可伐合金复银铜焊料是一种电真空用复合材料,它由4J29可伐合金和Ag72Cu28合金焊料组成,采用冷压结合方式将这两种组成合金按一定比例厚度结合,制成薄带供应.这种复合材料兼有4J29可伐合金和Ag72Cu38合金焊料的特性.是半导体晶体管用的理想封接材料.主要应用于场效应晶体管、混频管和小功率管等作为管壳结构材料. 文中介绍了4J29可伐合金和银铜合金焊料的主要特性,以及生产工艺的选择.以及研制出的复合材料的力学性质、深冲引伸性、不同退火制度的晶粒度等.     

液氮传导冷却型高温超导电流引线研制

80 A和200 A液氮传导冷却型高温超导(HTS)电流引线由铜引线段、中间过渡段和高温超导段组成,HTS热端采用液氮传导冷却,HTS冷端采用液氦传导冷却。铜引线段工作在室温到中间温度(~80 K),高温超导段工作温区6—80 K。介绍该传导冷却型电流引线的结构设计和低温性能测试。实验结果表明,中间过渡段温度~78 K,高温超导热端温度77 K;80 A、200 A电流引线液氦下稳态测试电流分别为100 A和250 A。     

Insertion of triangulated surfaces into a meccano tetrahedral discretization by means of mesh refinement and optimization procedures

In this paper, we present a new method for inserting several triangulated surfaces into an existing tetrahedral mesh generated by the meccano method. The result is a conformal mesh where each inserted surface is approximated by a set of faces of the final tetrahedral mesh. First, the tetrahedral mesh is refined around the inserted surfaces to capture their geometric features. Second, each immersed surface is approximated by a set of faces from the tetrahedral mesh. Third, following a novel approach, the nodes of the approximated surfaces are mapped to the corresponding immersed surface. Fourth, we untangle and smooth the mesh by optimizing a regularized shape distortion measure for tetrahedral elements in which we move all the nodes of the mesh, restricting the movement of the edge and surface nodes along the corresponding entity they belong to. The refining process allows approximating the immersed surface for any initial meccano tetrahedral mesh. Moreover, the proposed projection method avoids computational expensive geometric projections. Finally, the applied simultaneous untangling and smoothing process delivers a high‐quality mesh and ensures that the immersed surfaces are interpolated. Several examples are presented to assess the properties of the proposed method.     

Flow calorimeter for enthalpy increment measurements on condensed gases

A flow calorimeter for enthalpy increment measurements on condensed gases is presented. A better knowledge of the properties of the liquefied natural gas is needed, and therefore a liquid loop has been designed for our flow calorimeter. The fluid loop in the calorimeter is designed in order to avoid the two-phase region, since two phases would give compositional disturbances in the measurements. The avoidance of the two-phase region is made possible by increasing the pressure of the test fluid after the measurement section, then heating the fluid at super-critical pressure past the critical point. Finally, the fluid is throttled to the low-pressure gas state at the inlet condition of the compressor that circulates the fluid. To perform the pressure increase, a new cryogenic pump has been designed. To evaluate the new equipment, measurements were taken on liquid ethane over the temperature range 146–256 K at pressure between 0.9 and 5.1 MPa.     

Effect of Permeable Crystalline Material on Steel Reinforcement Corrosion of Concrete

Permeable crystalline materialcan permeate into pores and cracks of concrete and catalyze the reaction between Ca(OH) 2and unhydrated cement to generate a great quantity needle non-soluble crystals, which can stop up the pores and cracks of concrete, and increase the impermeability of concrete. This paper reported the results of a study conducted to evaluate steel reinforcement corrosion of concrete specimens uncoated and coated with permeable crystalline material as well as mixed with the permeable crystalline material. The properties evaluated for corrosion test were water impermeability, water absorption, compressive strength and potential. The results of water impermeability, water absorption, compressive strength clearly showed that the permeable crystalline material could prohibit water, any soluble salts and moisture from penetrating the concrete to cause corrosion, leaking, and other problems, and it did increase the compressive strength, which was favorable for protection of corrosion of reinforcing steel. Moreover, it was concluded from the potential-time curve that the steel reinforcement of uncoated specimen was in the state of activation whereas that of other specimens coated and mixed with the permeable crystalline material was in the state of inactivation. Above all, it was indicated that the permeable crystalline materialis very effective to protect the steel reinforcement of concrete from corrosion.     

The Research and Application About "Dry Peeling Off" Technology for Airplane Surface Paint Layer

In this paper, the principle of spurting take off lacquer were introduced; and with orthogonal method the unsaturate polyester was prepared ;it was easy to peel airplane paint layer off with this material and equipment.     

Refrigerators Enter a New Era of Health Preservation Frestech initiates the establishment of China's first standard for household sterilization refrigerators

On November 30, 2007, the China Association for Standardization (CAS) held a press conference at Beijing Diaoyutai State Guest House. Leaders from the China Household Electric Appliance Research Institute, the China Household Electric Appliance Association, and the China Consumers' Association attended and made speeches.……     

Quality Study of Honeycomb Core Shaping Without Wax Stabilization

Sandwich panels utilizing honeycomb cores result in lightweight, high-strength units that are very rigid. Indeed, they give honeycomb panels the best strength-to-weight ratio of any construction type available. Conventionally, the wax is poured into the cell of the core to strengthen the structure and prevent the core from being crushed during milling. Much time and labor is required to wax, mill, and clean the cores. In this study, the process of pouring wax into the core was skipped. In other words, the cutter directly milled the core. Experiments showed that the compressive strength of the core produced without wax stabilization was only 3% lower than that of cores produced using the traditional method. In addition, the drum peel strengths of cores produced without wax stabilization were 38.4% higher than cores produced using the traditional method, in which residual wax seriously polluted the adhesive. It was also found that eliminating the wax process can reduce costs.     

In-process thermal treatment of polylactic acid in fused deposition modelling

Polylactic acid (PLA) is one of the most widely used open source fused filament fabrication materials due to its ease of extrusion, biodegradability, and mechanical strength. The mechanical strength of PLA largely depends on the proper growth of its semi-crystalline structure, which can be severely impaired by a low rate of crystallization, particularly in open source printers. This can be further aggravated by the non-uniform thermal distribution of heat that causes improper curing among the extruded beads of the printing material. As a result, PLA printed on open source printers does not achieve the best mechanical properties. This research, for the first time, proposes an additive-free solution implemented through a detailed set of experimentation to improve the curing rate through in-process temperature variations to cure the joints among the beads. Scanning electron microscopy (SEM), differential scanning calorimetry (DSC) and Fourier transform infrared (FTIR) spectroscopy is used to confirm the improvements in the bead joints. This work is conducted in two phases of experiments. In the first phase, a full factorial ANOVA is used to investigate various process parameters and the important variables are used in the second phase to print test specimens in four different sets.     

A study of centrifugal cast high boron high speed steel

In the present study a high‐boron high speed steel (HSS) roll material was designed. Many expensive alloy elements have been substituted by cheap boron alloy, and high‐boron high speed steel roll has been manufactured by centrifugal casting method. The microstructures, mechanical properties and wear resistance of centrifugal casting high‐boron high speed steel roll have been investigated by optical microscopy (OM), scanning electron microscopy (SEM), and X‐ray diffraction (XRD) analysis, hardness test, impact test and wear test. The results indicated that the solidification microstructures of high‐boron high speed steel roll consisted of M₂(B,C), (W,Mo)₂(B,C), M₃(B,C), M₂₃(B,C)₆ type borocarbides and martensite, a small amount of retained austenite. Borocarbides were continuously distributed over the grain boundary. After quenching from 1050 °C, local broken network appeared in partial borocarbides, and fine secondary borocarbide precipitated from the matrix. After tempering from 525 °C, the amount of precipitated borocarbide increased significantly. After heat treatment, the hardness of high‐boron high speed steel roll excelled 60 HRC, and its impact toughness excelled 8.0 J/cm². The single groove steel rolling amount of high‐boron high speed steel rolls increases by 500% than that of bainite cast iron roll, when the rolls are used in K₁ mill housing of bar mill.     

Investigation of the Corrosion Behaviors of HVOF-Sprayed Carbide Cernet Coatings in Molten Al-Zn-Si Alloy Bath

In continuous hot-dip galvanization process the corrosion and chemical stability of the sink roll in the galvanizing bath are important problem which effects on the quality and productivity. In order to protect the sink roll the carbide cermet and/or ceramic coatings were deposited on the surface of the sink roll. The WC-, Cr3 C2-cermet coatings were deposited by high velocity oxygen fuel (HVOF) spray, respectively. The coating samples were immersed in molten Zn-alloy containing 50 wt % aluminum at 833 K for 24 hr and 144 hr, respectively. The inter-diffusion and inter-reaction of Zn, Al and elements in coating and corrosion behaviors of these coatings were investigated by XRD, SEM and EPMA etc. The corrosion mechanisms of the carbide cermet coatings and ceramic coatings in molten High Al-Zn-alloy were approached.