卤化银光纤式CO2激光手术刀

卤化银多晶光纤「ＡｇＣｌｘＢｒ（１－ｘ），０≤ｘ≤１」是一种性能优良的中红外传能光纤。光纤原料采用高真空熔炼、氯气气氛下区域融熔和高真厂长发瓿内单昌生长等特殊工艺方法提纯，光纤用热挤压法成型。已制成的直径Φ１．０（ｍｍ）光纤Ｌ＝１．６４（ｍ）输出ＣＯ２激光功率〉２０（Ｗ），损耗０．３￣０．５ｄＢ／ｍ，Ｆｏｒｕｒｉｅｒ红外光谱（ＦＴＩＲ）测量结果显示，光纤在４￣１６μｍ波段内有良好的透过率，用光纤制     

全反射型空芯光纤材料的选择及性能的评价

讨论了以红外折射率在CO2激光波长处小于1的玻璃为空芯光纤包皮材料的选择方法和原则,以及评价光纤性能的模型,为更进一步研究提供了有效的途径。     

卤化银光纤原料的超提纯

高纯原料的制备是制造高品质光纤最重要的环节,本文采用氯气氛下水平区熔法生长单晶的提纯方法对卤化银原料进行超提纯．区域熔融提纯后的卤化银原料红外吸收光谱测量显示在800～4000cm^－1范围内吸收随波长的增加而降低．经CO₂激光量热计法测量提纯后的卤化银原料在10．6μm处的吸收系数为5×10^－4Cm^－1,较提纯前降低两个数量级,制成的光纤传输损耗03～0．5dB／m     

光纤耦合问题的研究及球形端面光纤的应用

介绍了光源与光纤耦合的几种方法以及球形光纤的制作方法，采用射线理论分析了圆球形端面多模光纤的端面效应，给出了半导体激光器（LD）与圆球形端面光纤耦合的应用实例。实验结果表明该方法结构简单、调整方便，有实际应用的潜力。     

非对称光纤反射镜的可调谐光纤激光器

提出一种非对称窄带光纤环形反射镜结构的可调谐掺铒光纤激光器。980nm泵浦光对掺铒有源光纤进行抽运,高双折射光纤、偏振控制器（PC）和光纤耦合器构成窄带光纤反射镜,窄带光纤反射镜和普通光纤反射镜组成激光谐振腔,利用窄带光纤反射镜工作带宽纳米量级的特性得到单纵模激光。调整偏振控制器改变反射镜对不同波长的反射率,实现可变波长的激光输出。实验表明,该激光器的工作带宽为8nm,120mW泵浦光条件下最大输出功率为4mW,3dB带宽（脉冲的半高宽度）小于0．2nm,边模抑制比为20dB以上,在1527nm～1535nm的波长范围内观察到稳定激光输出。     

卤化银多晶光纤传输CO2激光性能的研究

通过采用高真空熔炼、反应气氛下区域融熔和高真空石英安瓿内单晶生长等特殊工艺方法对卤化银原料进行提纯,并用热挤压成型方法制得卤化银光纤．本文研究了卤化银原料的提纯和光纤成型工艺对损耗的影响,研究结果表明,增加提纯次数可降低卤化银光纤预制棒的吸收系数．通过合理控制工艺参数,提纯后的卤化银原料制成的光纤预制棒,经ＣＯ_２激光量热计法测量在１０．６μｍ处的吸收系数＜５×１０^－4ｃｍ^－１,热挤压成型的光纤在１０．６μｍ处的损耗为０.３～０.５ｄＢ／ｍ,直径φ１０ｍｍ、长度１．６４ｍ的光纤可传输ＣＯ_２激光功率＞２０Ｗ．     

光纤折射率分布和几何参数标准测量装置的研究

介绍了中国计量科学研究院建立的光纤折射率分布和几何参数标准测量装置，该装置采用“光反馈激光开关干涉-计算机光功率组分”测量微位移，并采用“干涉逼近法”和“插值法”测量折射率差的方法，分别使光纤的几何参数测量和折射率差测量溯源到He-Ne激光波长，测量光纤皮径和芯径的不确定度（2σ）分别为±0.25um和±0.5um。测量折射率的不确定度达到±2×10^-3。     

在DCF光纤中放大的背向自发拉曼散射的增益特性

光脉冲沿色散补偿光纤（DCF）传输会产生背向自发拉曼散射，当入纤激光功率大于阈值时，出现放大的背向自发拉曼散射现象。实验发现，反斯托克斯（ASR）和斯托克斯（SR）自身脉冲光纤拉曼放大的阈值泵浦峰值脉冲功率是18．2W和14．5W．当入纤激光功率为52W时，背向SR和ASR散射的增益分别为12dB和7dB。放大的反斯托克斯和斯托克斯背向自发拉曼散射时域曲线上的阈值时间位置随激发功率的增大而前移并具有规律性。     

高斯光束到光纤的单透镜耦合

分析了基模高斯激光束到单模和多模光纤的单透镜耦合过程中的各种损耗,把多模光纤的光场用高斯分布近似,采用模场耦合理论计算了基模高斯光束到单模和多模光纤的单透镜耦合效率.模拟计算了当激光-光纤耦合系统的工程参数(光束束宽、光纤数值孔径和光纤的纤芯芯径)一定时,单透镜耦合效率与所选用透镜的焦距之间的关系.并利用532mn激光(M2≤1.05)在几种不同焦距的透镜下对纤芯直径为3.μm的单模光纤和25μm的多模光纤进行了耦合效率的测定实验,得到了与理论计算基本吻合的实验结果.     

激光加热基座法单晶光纤生长技术

单晶光纤是指具有光学纤维形态的单晶体，其同时保持了玻璃光纤的形态优势以及体块单晶优异的物理和化学性能，为高功率激光应用中替代传统玻璃光纤提供了一种思路。随着单晶光纤在材料种类及应用方向的不断拓展，单晶光纤在辐射探测、高温传感等领域也具有潜在的应用前景。本文在介绍单晶光纤应用背景的基础上，对国内外激光加热基座法单晶光纤生长技术进行了总结，详细讨论了单晶光纤生长过程中存在的问题及其改进方案，最后对单晶光纤未来的发展方向进行了展望。     

The Research of Anti-Wear Properties of Organomolybdenum Compounds in the Engine Oils

A four-ball tester was used to evaluate the anti-wear performance of three kinds of organomolybdemun compounds in the engine oils, i. e., molybdenum dialkyldithiophosphate (MoDDP), molybdenum dialkyldithiocarbamate ( MoDTC), and sulphur and phosphorus freeorganomolybdeum (Molybdate). The results indicate that a low concentration of MoDDP doesn' t improve the anti-wear properties of the commercial engine oils, but a high concentration of MoDDP can obviously improve the anti-wear properties and the load-carrying capacity of the engine oils. MoDTC doesn' t improve the antiwear properties of the engine oils, but worsens the anti-wear properties of the oils. Signifi can timprove ment of frictional and wear characteristics is obtained with Molybdate added in the commercial engine oils and the formulated oils.     

Effect of Permeable Crystalline Material on Steel Reinforcement Corrosion of Concrete

Permeable crystalline materialcan permeate into pores and cracks of concrete and catalyze the reaction between Ca(OH) 2and unhydrated cement to generate a great quantity needle non-soluble crystals, which can stop up the pores and cracks of concrete, and increase the impermeability of concrete. This paper reported the results of a study conducted to evaluate steel reinforcement corrosion of concrete specimens uncoated and coated with permeable crystalline material as well as mixed with the permeable crystalline material. The properties evaluated for corrosion test were water impermeability, water absorption, compressive strength and potential. The results of water impermeability, water absorption, compressive strength clearly showed that the permeable crystalline material could prohibit water, any soluble salts and moisture from penetrating the concrete to cause corrosion, leaking, and other problems, and it did increase the compressive strength, which was favorable for protection of corrosion of reinforcing steel. Moreover, it was concluded from the potential-time curve that the steel reinforcement of uncoated specimen was in the state of activation whereas that of other specimens coated and mixed with the permeable crystalline material was in the state of inactivation. Above all, it was indicated that the permeable crystalline materialis very effective to protect the steel reinforcement of concrete from corrosion.     

The Research and Application About "Dry Peeling Off" Technology for Airplane Surface Paint Layer

In this paper, the principle of spurting take off lacquer were introduced; and with orthogonal method the unsaturate polyester was prepared ;it was easy to peel airplane paint layer off with this material and equipment.     

Quality Study of Honeycomb Core Shaping Without Wax Stabilization

Sandwich panels utilizing honeycomb cores result in lightweight, high-strength units that are very rigid. Indeed, they give honeycomb panels the best strength-to-weight ratio of any construction type available. Conventionally, the wax is poured into the cell of the core to strengthen the structure and prevent the core from being crushed during milling. Much time and labor is required to wax, mill, and clean the cores. In this study, the process of pouring wax into the core was skipped. In other words, the cutter directly milled the core. Experiments showed that the compressive strength of the core produced without wax stabilization was only 3% lower than that of cores produced using the traditional method. In addition, the drum peel strengths of cores produced without wax stabilization were 38.4% higher than cores produced using the traditional method, in which residual wax seriously polluted the adhesive. It was also found that eliminating the wax process can reduce costs.     

Certification Becomes Important for the I Quality; and Safety Supervision of the Chinese Liquor Sector

The end of 2007, over 200 unit products of more than 80 Chinese firms have passed the quality grade certification for liquor products. These products involve distilled spirits, beer, wine, yellow wine, fruit syrup wine and others, and cover over 80% of the national top-branded liquor products.……     

Deposition and Coating Properties on CVD Tungsten

Surface characterization and microstructure studies are performed on chemical vapor deposited (CVD) tungsten coating. There is about 2 μm thickness diffusion layer of tungsten in the molybdenum substrate. The thermal shock test shows tungsten coating has good adhesion with molybdenum substrate, but the elements of oxygen and carbon in the tungsten coating have the bad affection to the adhesion. The result of high-temperature diffusion experiment is the diffusion rate from molybdenum substrate to tungsten coating is faster.     

Analysis of marine hydrobiont lipid extracts as possible cryoprotective agents

We studied a combined effect of the cryoprotectants both of lipid and carbohydrate origin at the presence of DMSO or without it on cell viability and the RNA synthesis in the embryonic mollusc and echinoderm cell cultures obtained at different developmental stages. Cryoprotective properties of exogenous lipids correlated with their thermotropic behavior. Lipid extracts from marine hydrobiontes, which thermal transitions are characterized by relatively small part of calorimetric thermogram area lying at temperatures above 0 °C (6–18%), were found to possess a considerable cryoprotective activity. The results are discussed in relation to the prediction of the cryoprotective activity of lipid extracts for marine animal cells. In addition, it was found that marine invertebrate cells can be cryopreserved without DMSO at the presence of trehalose and lipid extracts of some marine hydrobiontes.     

Low-Temperature Properties of Silver

Pure silver is used extensively in the preparation of high-temperature superconductor wires, tapes, films, and other configurations in which the silver not only shields the superconducting material from the surrounding materials, but also provides a degree of flexibility and strain relief, as well as stabilization and low-resistance electrical contact. Silver is relatively expensive, but at this stage of superconductor development, its unique combination of properties seems to offer the only reasonable means of achieving usable lengths of conductor. In this role, the low-temperature physical (electrical, thermal, magnetic, optical) and mechanical properties of the silver all become important. Here we present a collection of properties data extracted from the cryogenic literature and, to the extent possible, selected for reliability.     

Early ironwork in Biscay: Survey,excavation, experimentation and materials characterization. An integral study of the mountainside ironworks (ferrerías de monte or “haizeolak”)

ABSTRACT

The production of iron in Biscay (Basque Country, Spain) has been a hallmark of this territory of the North of the Iberian Peninsula throughout its history. The Archaeology team of the Basque Country Mining Museum has spent 13 years, so far, studying the origins of this activity through the evidences left at the old pre-hydraulic iron production workshops known as mountainside ironworks (ferrerías de monte) or haizeolak. It has catalogued 170 archaeometallurgical sites of this type in Biscay, and the archeological excavation of some of them has led to the knowledge of the different stages of the production process that took place in these workshops. The team has also experimentally reproduced the work carried out in a mountainside ironworks from the High Middle Ages, and it has currently started the characterization process of this type of activity through the study of the collected materials.     

In-process thermal treatment of polylactic acid in fused deposition modelling

Polylactic acid (PLA) is one of the most widely used open source fused filament fabrication materials due to its ease of extrusion, biodegradability, and mechanical strength. The mechanical strength of PLA largely depends on the proper growth of its semi-crystalline structure, which can be severely impaired by a low rate of crystallization, particularly in open source printers. This can be further aggravated by the non-uniform thermal distribution of heat that causes improper curing among the extruded beads of the printing material. As a result, PLA printed on open source printers does not achieve the best mechanical properties. This research, for the first time, proposes an additive-free solution implemented through a detailed set of experimentation to improve the curing rate through in-process temperature variations to cure the joints among the beads. Scanning electron microscopy (SEM), differential scanning calorimetry (DSC) and Fourier transform infrared (FTIR) spectroscopy is used to confirm the improvements in the bead joints. This work is conducted in two phases of experiments. In the first phase, a full factorial ANOVA is used to investigate various process parameters and the important variables are used in the second phase to print test specimens in four different sets.