Al2O3sf.SiCp／LY12复合材料液态下浸渗与塑性成形的研究

采用液态浸渗和渗后直接挤压的方法,成功地制备出Al2O3sf·SiCp／LY12非连续混杂增强金属基复合材料。其增强物分布均匀,基体组织致密,与基体LY12相比具有较高的弹性模量、屈服强度、抗拉强度,并且延伸率也保持较高的水平。同液态浸渗制备的复合材料相比,各项力学指标均有提高。     

SiC_p/AZ91镁基复合材料的热挤压

采用搅拌铸造法制备SiC体积分数为5%、10%和15%的颗粒增强AZ91镁基复合材料（SiCp/AZ91）。复合材料经过T4处理后,于350°C以固定挤压比12：1进行热挤压。在铸态复合材料中,颗粒在晶间微观区域发生偏聚。热挤压基本上消除了这种偏聚并有效地改善颗粒分布。另外,热挤压有效地细化基体的晶粒。结果表明：热挤压明显提高复合材料的力学性能。在挤压态复合材料中,随着SiC颗粒含量的升高,基体的晶粒尺寸减小,强度和弹性模量升高,但是伸长率降低。     

SiCp/AZ31镁基纳米复合材料的高能超声制备及性能

文章采用自行设计的高能超声装置制备SiCp/AZ31镁基纳米复合材料,并对制备的复合材料进行显微组织观察和力学性能测试。实验结果表明,高能超声波能使纳米SiCp在镁合金熔体中均匀分散,复合材料抗拉强度和屈服强度都比基体有较大提高,并能保持较高的延伸率。另外,对高能超声波制备金属基复合材料的分散机理,以及SiCp增强镁基纳米复合材料的增强机制,进行了初步探讨。     

喷射沉积7090/SiCp复合材料SiC颗粒分布均匀性研究

制备了喷射共沉积及粉末冶金SiCp/7090Al复合材料,以不同的挤压比进行热挤压成形,研究了两种复合材料中SiC增强颗粒的分布特点。实验结果表明,沉积坯经过热挤压后,沿挤压方向SiC颗粒存在明显的带状分布特征,在横截面上具有同心圆环组织。而粉末冶金坯料经过热挤压后则避免了这一现象的产生,合理的热挤压工艺可以显著改善粉末冶金复合材料中的SiC增强颗粒的形貌,细化SiC增强颗粒的粒度。增强颗粒细化后得到的细小等轴颗粒更易随着基体的塑性流动而呈弥散均匀分布,改善或消除微区域内增强体颗粒的偏聚,减弱了偏聚的程度。室温力学性能测试结果表明,随着挤压比的增加,挤压态粉末冶金复合材料的抗拉强度由挤压比为11时的362.84MPa,增大到挤压比为25时的425.27MPa。     

Development and characterization of liquid carbon fibre reinforced aluminium matrix composite

The progress and developments in materials technology have resulted in several new materials like metal–matrix composites (MMCs). On account of excellent physical, mechanical and development properties, MMCs are applied widely in aircraft and automobile technology. The present paper deals with the development of aluminium matrix composite reinforced with carbon preform having a volume fraction of 20–25% using squeeze casting infiltration process. Hardness, impact and tension test on the squeeze cast matrix and the composite was conducted to study the improvement in properties compare to that of matrix. Even though ultimate tensile strength of composite is found to be decreased, an increased Brinell hardness number and a four-fold improvement in toughness are noticed. Characterization of the materials done using optical and scanning electron microscope (SEM) revealed that the carbon fibers are evenly distributed in the matrix and the alloy is appeared to have smaller dendrite size. The lack of observed fibre pull-out on fracture and improved mechanical properties resulted due to the good wetting of the fibers by the liquid alloy.     

热挤压变形对搅拌铸造SiCp/2024复合材料显微组织与力学性能的影响

利用搅拌铸造?热挤压工艺制备SiCp/2024复合材料板材。通过金相观察(OM)、扫描电镜(SEM)及力学性能测试等手段研究了该复合材料热挤压变形前后的显微组织与力学性能。结果表明,复合材料铸坯主要由大小为80μm~100μm的等轴晶组成,晶界第二相粗大呈非连续状分布,SiC颗粒较均匀地分布于基体合金,大部分SiC颗粒沿晶界分布,少数颗粒分布于晶内;热挤压变形后,显微孔洞等铸造缺陷和SiC颗粒团聚现象明显消除,SiC颗粒及破碎的第二相沿热挤压方向呈流线分布,复合材料的强度和塑性显著提高;拉伸断口表明,热挤压变形有利于改善SiC颗粒与基体合金的界面结合;SiCp/2024复合材料主要的断裂方式为SiC颗粒断裂和SiC/Al的界面脱粘。     

Enhanced mechanical properties in Al/diamond composites by Si addition

Diamond particles reinforced aluminum–silicon matrix composites,abbreviated as Al(Si)/diamond composites,were fabricated by squeeze casting.The effect of Si content on the microstructure and mechanical properties of the composites were investigated.The mechanical properties are found to increase monotonically with Si content increasing up to 7.0 wt%.The Al-7.0 wt% Si/diamond composite exhibits tensile strength of 78 MPa,bending strength of 230 MPa,and compressive strength of426 MPa.Al–Si eutectic phases are shown to connect with Al matrix and diamond particles tightly,which is responsible for the enhancement of mechanical properties in the Al(Si)/diamond composites.     

低过热度浇注SiC_p/Gr/ZL101复合材料组织与性能研究

采用半固态搅拌、低过热度重力浇注的方法制备了SiCp/Gr颗粒复合增强ZL101铝基复合材料。通过显微组织观察、拉伸试验以及阻尼性能测试,研究了不同体积分数SiCp/Gr对铝基复合材料性能的影响。结果表明,通过半固态搅拌、低过热度重力铸造法,使ZL101合金中的初生相α-Al由枝晶形态变为蔷薇状,晶粒明显细化。随着SiCp体积分数的增加,复合材料的抗拉强度先升高后降低,伸长率逐渐下降,复合材料的最高抗拉强度达到191MPa,比ZL101合金提高了32%。SiCp与Gr的加入改善了ZL101合金的阻尼性能,复合材料的内耗值Q-1明显高于基体合金,并且随着SiCp体积分数的增加,复合材料内耗值Q-1逐渐提高。     

The effect of thermal cycling on the mechanical properties of sic whisker reinforced magnesium alloy-based composites

The effect of thermal cyclings on mechanical properties at room and some elevated temperatures of SiC whisker-reinforced magnesium-matrix composites produced by squeeze casting and hot extrusion are clarified. Subsequent thermal cycling produces internal stress at the matrix/SiC whisker interfaces causing fatigue. The mechanical properties of composites are more influenced by the low thermal cycling of 298 K— 77 K than the high thermal cycling 673 K—298 K. The high thermal cycling of 673 K—298 K has only a slight affect on such mechanical properties as tensile strength and proof stress at temperatures lower than 473 K. However, at 473 K and 573 K, the thermal cyclings there almost no influence on the mechanical properties of SiC whisker reinforced AE42 alloy-matrix composites.     

热处理对SiC_p／ZL109复合材料机械性能和物理性能的影响

试验分析了不同热处理方法对ＳｉＣｐ／ＺＬ１０９复合材料机械性能和物理性能的影响；通过金相和透射电镜分析研究了其热处理强化机理．结果表明．Ｔ６热处理可大幅度提高复合材料的强度；Ｔ４热处理在提高强度的同时可增加复合材料的延伸率；复合材料强度的提高是由于ＳｉＣｐ的均匀分布和ＳｉＣｐ与Ａｌ基体热膨胀系数差导致的高密度位错产生的．     

Effect of hot extrusion on microstructures and mechanical properties of SiC nanoparticles reinforced magnesium matrix composite

Particulate reinforced magnesium matrix nanocomposite prepared with semisolid stirring assisted ultrasonic vibration was subjected to extrusion at 350 °C with an extrusion ratio of 12:1. Extrusion of the SiCp/AZ91 nanocomposite induced large scale dynamic recrystallization resulting in a fine matrix microstructure. There were two kinds of zones in the extruded nanocomposite: SiC nanoparticle bands parallel to the extrusion direction and refined-grain zones between the SiC nanoparticle bands. In the SiC nanoparticle bands, there were SiC nanoparticles along the boundaries of refined grains. The distribution of SiC nanoparticles was uniform although some agglomerates of SiC nanoparticles still existed in the SiC nanoparticle bands. The ultimate tensile strength, yield strength and elongation to fracture of the SiCp/AZ91 nanocomposite were simultaneously improved by extrusion. Results from the extruded SiCp/AZ91 nanocomposite tensile testing at different temperatures (75, 125, 175 and 225 °C) revealed an increase of the tensile strength and ductility values compared with the unreinforced and extruded AZ91 alloy.     

深冷处理对SiCp/A356复合材料力学性能的影响

采用熔铸搅拌法制备了SiCp质量分数为38%的A356铝基复合材料,研究了深冷处理和深冷处理循环次数对铝基复合材料力学性能的影响.试验表明.深冷处理使铝基复合材料的屈服强度和抗拉强度提高了约10%,深冷处理循环次数对力学性能影响不大.对复合材料的微观形貌观察和EDAX分析表明,在深冷过程中有Si相和其他超微第二相的析出,观察了扫描断口,发现增强相在断裂过程中产生了规则的解理面,复合材料的断裂主要是增强相的解理断裂和基体的撕裂.     

SiC颗粒增强AZ91基复合材料拉伸性能研究

针对风力发电机组摩擦材料对性能的要求,在不同的温度下,成功制备出了SiC颗粒增强的AZ91镁合金基复合材料,并且对其拉伸性能进行研究.结果表明,SiCp/AZ91复合材料的抗拉强度高于AZ91基体镁合金;在同样的烧结温度下,直径较小的SiC颗粒对复合材料的抗拉强度提高幅度较大.     

反挤压对SiCw/6061力学性能影响的实验研究

以挤压工艺对SiCw/6061复合材料力学性能的影响为研究目标,通过改变挤压温度、挤压比以及凸模中心锥角等工艺参数,系统分析了挤压铸造制备的SiCw/6061复合材料反挤压变形前后强度、塑性及硬度的变化规律.研究表明,挤压变形可以有效地提升复合材料试件的各项力学性能指标;随着挤压温度的升高,试件的屈服强度、抗拉强度均呈现升高的变化趋势,延伸率先显著增大而后略有减小,硬度则呈现下降的趋势;随着挤压比的增加,试件的强度、塑性及硬度均呈现上升趋势;随着凸模中心锥角的增大,试件的屈服强度、抗拉强度均呈现先升高后下降的趋势,延伸率及硬度则随着锥角的增加始终呈上升趋势.     

不同热处理下滑动速度对SiCp/Al复合材料摩擦学性能影响研究

SiCp/Al复合材料非匀质性微观结构使其摩损机制较传统匀质材料更为复杂,不同工况及热处理工艺下复合材料的摩擦学性能也存在差异。以SiCp/2024Al复合材料为研究对象,进行球-面接触干滑动摩擦磨损实验,探究它在不同热处理状态及滑动速率下的摩擦磨损性能及磨损机制。结果表明:热处理对复合材料力学性能和摩擦学性能有显著影响,固溶+人工时效态复合材料具有更高的强度、硬度及耐磨性;滑动速度影响复合材料的表面接触性质及磨损程度,摩擦因数和磨损量随滑动速度提高逐渐增大;随滑动速度增加,复合材料主要磨损机制由剥层磨损向磨粒磨损转变,而磨损机制的转变明显加快了复合材料的磨损,在实际应用中应尽量避免此现象发生。     

SiC_w/6061Al复合材料的组织与性能SCIEI

本文对SiC_w/6061Al复合材料的组织与性能进行了研究,结果表明,压铸法可以制备出高强度、高模量的各向同性复合材料,挤压使复合材料的强度由压铸态的582MPa提高到639MPa,并使材料变为各向异性,这可以由晶须的定向排列和基体的高密度位错得到解释。复合材料的抗高温性能要比基体高150℃,透射电镜观察还发现,层错是SiC晶须中常见的一种面缺陷。     

MICROSTRUCTURE AND PROPERTIES OF SiC_w/6061Al COMPOSITE The Author is now with Institute of Metal Research,Academia Sinica,China

The SiC_w/Al composite prepared by squeeze casting has a combination of superior roomtemperature specific strength and modulus together with excellent thermal properties.Theextrusion can make an improvement on the strength and ductility of the composite from 582MPa as squeeze casted up to 639 MPa,and on the transformation from isotropic to theanisotropic structure.This seems to be explained by the orientation of whiskers and thedensification of dislocations in matrix.TEM observation indicates that the stacking fault isthe usual planar defect on the SiC_w surface.     

Effect of Particle Size on the Microstructures and Mechanical Properties of SiC-Reinforced Pure Aluminum Composites

This article examined the effects of particle size and extrusion on the microstructures and mechanical properties of SiC particle-reinforced pure aluminum composites produced by powder metallurgy method. It has been shown that both particle size and extrusion have important effects on the microstructures and mechanical properties of the composites. The SiC particles distribute more uniformly when the ratio of the matrix powder size and SiC particle size approaches unity, and the smaller-sized SiC particles tend to cluster easily. The voids are found to coexist with the clustered and large-sized SiC particles, and they significantly decrease the density and mechanical properties of the composites. Extrusion can redistribute the SiC particles in the matrix and decrease the number of pores, thus make the SiC particles distribute more uniformly in the matrix, and enhance the interfacial bonding strength. The decrease in the SiC particle size improves the tensile strength and yield strength, but decreases the ductility of the composites.     

Tensile and Fracture Properties of 15 vol% SiC_p/2009Al Composites Fabricated by Hot Isostatic Pressing and Hot Extrusion Processes

15 vol% silicon carbide particle （SiCp）-reinforced 2009A1 matrix （15 vol% SiCp/2009A1） composites were fabricated by hot isostatic pressing （HIP） and hot extrusion processes. The tensile and fracture properties of 15 vol% SiCp/ 2009Al were studied. The results showed that hot extrusion increased the ultimate tensile strength （UTS）, yield strength （YS）, elongation （EL）, reduction in area （RA）, and fracture toughness of the composites. The heat treatment resulted in the increase in UTS, YS, and fracture toughness, but a decrease in EL and RA. Both hot extrusion and heat treatment had negligible effects on elastic modulus （E）. With the increase of SiCp size, the UTS, YS, and E decreased, but the EL and RA increased. The fracture toughness increased first and then decreased with increasing SiCp size, and when the SiCp size was about 7 μm, the composites obtained the maximum fracture toughness value of 31.74 MPa m^1/2.     

石墨对亚微米SiCp/Cu复合材料耐磨性能的影响

以亚微米SiCp、石墨和铜粉为原料,采用冷压烧结和热挤压方法制备了亚微米SiCp/Cu基复合材料和亚微米SiCp 石墨/Cu基复合材料,考察了添加石墨对亚微米SiCp/Cu基复合材料硬度、拉伸性能、致密性和耐磨性的影响.结果表明,石墨的加入轻微降低了SiCp/Cu基复合材料的硬度、伸长率、致密性和耐磨性,在一定程度上提高了抗拉强度,并且磨损表面上的粘着、塑性变形和物质转移倾向亦明显降低,能起到较好的减磨作用.