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利用X射线衍射仪(XRD)和热场发射透射电镜(TEM)分别对在弱磁场下通过低温中和法制备的纳米MnOOH进行相成分和颗粒形貌分析.试验结果表明:在弱磁场下,锰的氢氧化物的沉淀物由无磁场下的Mn(OH)2向MnOOH转变.随着弱磁场强度增大,MnOOH颗粒进一步细化,在0.5 T弱磁场下制备出了粒径达30 nm左右MnOOH颗粒,并且纳米MnOOH颗粒的粒度分布均匀.此外,弱磁场不影响MnOOH的结晶度. 相似文献
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利用X射线衍射仪(XRD)和热场发射透射电镜(TEM)分别对在弱磁场下通过低温中和法制备的纳米MnOOH进行相成分和颗粒形貌分析.试验结果表明在弱磁场下,锰的氢氧化物的沉淀物由无磁场下的Mn(OH)2向MnOOH转变.随着弱磁场强度增大,MnOOH颗粒进一步细化,在0.5 T弱磁场下制备出了粒径达30 nm左右MnOOH颗粒,并且纳米MnOOH颗粒的粒度分布均匀.此外,弱磁场不影响MnOOH的结晶度. 相似文献
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介绍了Gd.Si.Ge磁致冷材料的晶体结构、磁相变、磁热效应、制备方法、防腐等方面的研究进展.室温磁致冷材料Gds(Si,Ge1-x)4在O≤x≤0.5、磁场H>5T时,呈现巨磁热效应;磁热效应的物理本质是一级磁晶相变;原材料Gd对Gd-Si-Ge系合金巨磁热效应的影响较大;Gd-Si-Ge磁致冷材料的成型方法主要有包覆法、复合法和真空扩散焊等. 相似文献
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采用化学共沉淀法制备纳米Fe_3O_4磁颗粒,用油酸钠作表面活性剂对其进行表面改性,用硅油作为载液制备出硅油基磁流体。重点研究了氨水的不同添加顺序及氨水的不同添加速度对磁流体性能的影响,通过磁性能测试、观察磁流体静置后的沉降现象以及透射电镜对磁流体进行表征,结果表明先加氨水再加油酸钠制备的磁流体分散稳定性好,其饱和磁化强度为11.4(A·m~2)/kg,进一步研究了以10 mL/min速度滴加氨水再加油酸钠,得到的磁流体分散稳定性较好,其饱和磁化强度为14.3(A·m~2)/kg。 相似文献
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采用区熔定向凝固方法,以480 mm/h速度制备了<110>取向Tb0.36Dy0.64(Fe0.85Co0.15)2合金棒.通过测试在0-0.325 T磁场范围内合金棒的应力-应变回线,计算了应力幅σm分别为-10,一30和一50 MPa的阻尼系数ΔW/W.结果表明,零磁场下的ΔW/W最大;随磁场强度增大,同一σm条件下的ΔW/W逐渐降低.在低磁场中,ΔW/W随σm的增加而降低;在高磁场中,ΔW/W随σm的增加而升高.利用不同预压应力下的磁致伸缩-磁化强度关系曲线,分析了磁场-应力复合加载条件下非180°磁畴和畴壁的运动形式.依据局部内应力理论,解释了合金棒的磁机械阻尼系数随外磁场强度和应力幅值变化的规律. 相似文献
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在强磁场下采用共沉淀-相转化法制备出了纳米级的钴铁氧体颗粒;通过SEM,XRD和VSM等分析手段,考察了磁感应强度对纳米钴铁氧体形貌及性能的影响规律.结果表明:无磁场及磁感应强度小于2T时,纳米钴铁氧体颗粒为球形;当磁感应强度大于、等于4 T时,棒状纳米钴铁氧体开始形成.随着磁感应强度的增大,棒状纳米颗粒数量增加,纳米钴铁氧体的晶化程度提高,磁性能(Mr,Ms,Mr/Ms)也大幅度提高.与无磁场相比, 10 T时制备的纳米钴铁氧体颗粒的剩余磁化强度Mr增加近15倍,饱和磁化强度Ms提高约1.44倍.从磁聚合定向生长和临界磁畴角度分析了强磁场影响共沉淀-相转化法制备的纳米钴铁氧体的形貌、晶化程度及磁性变化的机理. 相似文献
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采用真空感应熔炼法,制备Fe1-xMnx(x=O.30,0.35,0.40,0.50,0.55(原子分数))合金,在1000℃保温24h,炉冷至室温.研究了不同结构Fe1-xMnx合金样品的室温磁致伸缩性能.结果表明,x≤0.40时,Fe1-xMnx合金样品为,γ ε双相结构,并且ε相体积分数随Mn含量增加而减小,磁致伸缩性能较差;x>0.40时,合金样品为单一的γ相,具有良好的磁致伸缩性能.Fe0.50Mn0.50合金样品在1.9T磁场中的磁致伸缩可达8.73x 10-4 相似文献
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A two-phase numerical model coupled with heat transfer was presented to describe the radial distribution of SiC particles on centrifugally-cast metal matrix composite,and a transverse static magnetic field was concurrently imposed to induce electromagnetic stirring of the melt as it revolved with the mold.Meanwhile,experimental observations were also carried out to examine the radial distribution of SiC particles in pure aluminum.The effects of the imposed magnetic field,particle size and the matrix metals were discussed.The computational results show that the particles tend to be congregated by the centrifugal force,and both increasing the imposed magnetic field and decreasing the particle size tend to result in even distribution of the particles.With the magnetic field varying from 0 to 1 T and the particle size from 550 to 180 μm,a uniform distribution of the particles in the aluminum matrix can be obtained among the computational results.The matrix metal can also influence the particle distributions due to the difference in physical properties of metals.Experimental observation shows similar tendency of particle distributions in aluminum matrix influenced by magnetic field and particle size.However,the chilling effect from the mold wall results in an outer particle-free zone,which is not involved in the numerical model. 相似文献
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利用化学反应的方法研制了一种带膜观察磁畴结构的改进型磁流体—Fe3O4磁流体,并对其生成条件及影响其磁性的因素进行了分析.实验表明:当FeCl2·4H2O:FeCl3·6H2O:NaOH=1:1:6(摩尔比)时最容易生成稳定的Fe3O4.在反应过程中,水质的好坏及有无搅拌是影响 Fe3O4磁流体颗粒大小及磁性的主要因素.对Z8牌号的硅钢片进行带膜磁畴观察表明,该磁流体能够实现带膜观察,成纹性及重现性较好,而且磁稳定性也较好,未经任何处理的Fe3O4磁流体可以放置一周左右而磁性不发生变化;用去离子水清洗至pH值为7并且隔绝空气后,可放置更长时间. 相似文献
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采用化学共沉淀法,通过改变Fe3O4纳米颗粒的生长温度、包覆环境pH、清洗、分散方式等工艺参数进行对比试验,得出Fe3O4纳米颗粒在生长阶段、包覆阶段、分散阶段的最佳参数条件,优化以往的制备工艺,使油酸包覆的磁性颗粒在煤油中的分散稳定性得到提高。通过XRD、TEM、VSM等对样品进行表征,并使用旋转流变仪对所制煤油基磁性液体的流变性能进行分析。结果表明,改性后的Fe3O4纳米颗粒平均粒径约为14nm,呈现较为规则的球形,饱和磁化强度为60 (A·m2)·kg-1,可制备出质量分数可达60%的高密度煤油基磁性液体,与普通磁液相比,以此制备工艺得的高密度煤油基磁性液体在饱和磁化强度、抗氧化性等方面皆有较大提升,拥有更高的应用价值。 相似文献
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In order to synthesize the targeting drug carrier system, magnetic chitosan-5-fluorouracil nano-particles were prepared by using 5-fluorouracil (5-Fu) as model drug, Fe3O4 nano-particles as kernel, chitosan as enveloping material and glutaraldehyde as cross linking agent through ultrasonic technique. The morphology of the magnetic chitosan-5-Fu nano-particles was observed with a transmission electron microscope(TEM). The results showed that magnetic chitosan-5-Fu nano-particles were prepared in spherical structure with a size range of 50–60 nm. The delivering capacity and drug releasing properties of magnetic chitosan-5-Fu nano-particles were investigated by UV-vis spectrum analysis. The results showed that the loading capacity was 13.4% and the cumulative release percentage in the phosphate buffer (pH=7.2) solutions was 68% in 30 h. These data indicate that the wrapped drug of magnetic chitosan-5-Fu nano-particles was slowly-released. The magnetic response of magnetic chitosan-5-Fu nano-particles was studied by UV-vis spectrometer to detect the changes of solution absorbance. Without external magnetic field, the nano-particle deposition rate was slow. When being subjected to 8 mT magnetic field, the particle sedimentation rate was increased rapidly. The results showed that magnetic chitosan-5-Fu nano-particles have a magnetic stability and strong targeting characteristics. 相似文献
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采用SEM,XRD,TEM,TG等手段研究了磁场对共沉淀法制备纳米MnZn铁氧体前驱体形貌及晶态结构的影响。结果表明,随着磁感应强度增大并达到某一临界值时,纳米颗粒形貌由球状向链状转变,继续增加磁感应强度将获得针状、棒状或纤维状的颗粒,10T强磁场下获得棒状颗粒呈现单晶结构。热重分析表明10T磁场下获得的纳米颗粒由于单维尺寸增加而导致活性降低。根据晶体生长理论,讨论了磁场影响纳米颗粒形核和长大过程的机理。 相似文献
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金属磁性液体的制备及特性研究 总被引:1,自引:0,他引:1
论述了利用羰基铁蒸气在载液中热分解制备金属磁性液体的方法。研究了羰基铁蒸气的浓度、热分解温度等条件对纳米级颗粒形成的影响,同时对界面活性剂、载液的选择也进行了探讨。 相似文献