Effect of Cold Rolling on the Fretting Wear Behavior and Mechanism in Inconel 690 Alloy

The influence of cold rolling on the fretting wear behavior and mechanism of Inconel 690 alloy at 320?°C in air was studied. The wear volume and worn surface were obtained and analyzed using laser scanning confocal microscopy, electron back-scattering diffraction, scanning electron microscopy, and energy-dispersive X-ray spectroscopy. The grinding surface and strain distribution were also studied by electron back-scattering diffraction to analyze the mechanism of fretting damage. The results indicated that with an increase in cold rolling reduction, the microhardness was increased. However, the friction coefficient and wear volume first increased and then decreased. The characteristics of fretting areas changed from a gross slip regime to a partial slip regime. Accordingly, the damage mechanism in the gross slip regime was a combination of oxidative wear, abrasive wear, and delamination, whereas the damage mechanism in the partial slip regime was mainly adhesive wear.     

Experimental Study of the Fretting Wear Behavior of Incoloy 800 Alloy at High Temperature

The fretting wear behavior of the nuclear power material Incoloy 800 was investigated in this study. A PLINT high-temperature fretting tester was used on an Incoloy 800 cylinder against a 304SS cylinder at vertical cross contact under different temperatures (25, 300, and 400°C). During testing, a normal load of 80 N was applied, and the displacement amplitudes ranged from 2 to 40 µm. The fretting wear mechanism at high temperatures and the kinetic character of the materials of the Incoloy 800 steam generator tube were analyzed. Results showed that the fretting running regimes varied little with ncreasing temperature, and some microcracks were observed in both the mixed fretting regime (MFR) and the partial slip regime (PSR) at high temperatures. Slight abrasive wear and microcracks were the main wear mechanisms of the Incoloy 800 alloy in PSR, whereas those in the MFR and the gross slip regime were oxidative wear, abrasive wear, and delamination.     

聚四氟乙烯基粘结固体润滑涂层微动磨损性能研究

在不同位移幅值与载荷条件下研究了酚醛环氧粘结聚四氟乙烯(PTFE)基固体润滑涂层的微动磨损特性，并利用扫描电子显微镜、表面轮廓仪和傅里叶表面红外仪等对涂层磨斑进行分析。结果表明，粘结PTFE基涂层具有良好的抗微动损伤性能，随循环次数的变化只存在部分滑移区和滑移区，部分滑移区的损伤轻微，滑移区的损伤强烈依赖于栽荷，其损伤与PTFE分子链在往复交变载荷作用下的疲劳断裂相关。     

TiAlZr合金微动磨损性能研究

采用高精度液压式微动磨损试验机研究了TiA lZr合金在不同微动运行区域的微动磨损行为,建立了其运行工况微动图。试验结果表明:滑移区、混合区和部分滑移区的摩擦因数随循环次数变化呈现不同的规律,其中部分滑移区摩擦因数较低,磨损体积随着位移幅值的增大而增大;滑移区、混合区磨损体积随着法向载荷的增加而增大,而部分滑移区磨损体积随着法向载荷的增加而减小;滑移区磨屑堆积于中心区域,磨损以磨粒磨损和剥层机制为主;混合区磨损机制主要表现为粘着磨损与磨粒磨损并存;部分滑移区磨损轻微。     

粘结石墨固体润滑涂层微动磨损性能研究

在不同位移幅值与载荷下研究了粘结石墨固体润滑涂层的微动磨损特性，并利用扫描电镜和X射线衍射仪分析了涂层微动磨斑。结果表明：粘结石墨涂层具有良好的抗微动损伤性能，随循环次数的变化只存在部分滑移区和滑移区，部分滑移区涂层损伤轻微；滑移区损伤严重，主要表现为裂纹萌生和扩展，最终按剥层机制呈层状剥落。     

AZ91D镁合金微动磨损特性研究

采用液压高精度材料试验机考察了平面一球面接触的AZ91D镁合金摩擦副的微动磨损行为，分析了位移幅值、法向载荷和频率等参数对摩擦因数和磨损体积的影响，考察了不同实验条件下的磨斑形貌，并探讨了其磨损机理。结果表明：AZ91D镁合金的微动区域可分为部分滑移区、混合区和滑移区3个区域，粘着磨损、疲劳磨损和磨粒磨损分别是3个区域的主要磨损机制；磨损体积随着位移幅值和法向载荷的增加而增大，但却随着频率的增大而减小。在微动部分滑移区和混合区，摩擦因数随着位移增大迅速增加；在微动滑移区，摩擦因数随法向载荷的增大而减小，而位移幅值和频率对摩擦因数的影响较小。     

Torsional Fretting Wear Behavior of Bonded MoS2 Solid Lubricant Coatings

The effects of applying a bonded MoS₂ solid lubricant to a 1050 steel substrate were investigated using a torsional fretting wear apparatus. Tests were conducted under a normal load of 50 N with angular displacement amplitudes ranging from 0.1 to 5°. Wear scars were examined using scanning electron microscopy, energy-dispersive X-ray spectrometry, optical microscopy, and surface profilometry. The MoS₂ coating exhibited different torsional fretting regimes than those of the substrate. Fretting regimes of the coating were primarily in the partial slip regime (PSR) and the slip regime (SR) with no mixed fretting regime. The width of the PSR narrowed. Due to the lubricating effects of the coating, the friction torque was consistently lower than that of the substrate. The damage to the coating in the PSR was very slight, and its granular structure remained even after 1,000 cycles. The damage mechanism to the SR coating was a combination of abrasive wear, oxidative wear, and delamination. The MoS₂ coating had potential to alleviate torsional fretting wear.     

不同水介质下GCr15/45#钢微动腐蚀行为研究

在洁净水、酸性水和海水3种不同水介质条件下，对GCr15／45^#钢进行了不同位移幅值的微动磨损试验。结果表明：洁净水和酸性水改变了微动区域，降低了摩擦系数和磨损量，具有润滑效果，磨损受水润滑和介质腐蚀双重作用影响,且润滑作用随位移幅值的增加而减弱；对海水，摩擦系数与干态相近,电化学腐蚀作用强烈，磨痕中可观察到大量点蚀坑。     

Fretting wear behavior of superelastic nickel titanium shape memory alloy

The fretting behavior of superelastic nickel titanium (NiTi) shape memory alloy was studied at various displacement amplitudes on a serve-hydraulic dynamic test machine. The results showed that the superelastic properties of the material played a key role in the observed excellent fretting behavior of NiTi alloy. Due to the low phase transition stress (only 1/4 the value of its plastic yield stress) and the large recoverable phase transition strain (5%) of NiTi, the friction force of NiTi/GCr15 stainless steel pair is smaller than the value of GCr15/GCr15 pair and at the same time the Rabinowicz wear coefficient of NiTi plate is about 1/9 the value of GCr15 plate under the same fretting conditions. For NiTi/GCr15 pair, even NiTi has a much lower hardness than GCr15, the superelastic NiTi alloy exhibits superior fretting wear property than GCr15 steel. It was found that the weak ploughing was the main wear mechanism of NiTi alloy in the partial slip regime. While in the mixed regime and gross slip regime, the wear of NiTi was mainly caused by the abrasive wear of the GCr15 debris in the three-body wear mode.     

Effect of Cold Rolling on the Fretting Wear Behavior and Mechanism in Inconel 600 Alloy

The fretting test was carried out using an SRV IV fretting test rig in order to investigate the fretting wear behavior and mechanism in Inconel 600 alloy at room temperature. The materials were rolled to different reductions before the test. The effect of cold rolling on the friction coefficient and wear volume was subsequently investigated. The surface and cross-sectional morphologies of the wear scar were studied by scanning electron microscopy (SEM), laser scanning confocal microscopy (LSCM), and electron back-scattering diffraction (EBSD). The results indicated that the cold rolling had a different effect on wear behavior in different slip regimes. In the stick regime, cold rolling strongly decreased the wear volume, although it did not affect the friction coefficient. The 25% rolled specimen had the minimum wear volume. The mechanisms of as-received and 50% rolled specimens were delamination and oxidation wear, whereas for the 25% rolled specimen, cracking was the main wear mechanism. In the gross slip regime, cold rolling had little effect on the friction coefficient or wear volume. The fretting wear process gave rise to a decrease in the Σ3 grain boundary, an increase in local misorientation, and a change in the crystal orientation.     

Fretting wear behaviors of steel wires under friction-increasing grease conditions

Fretting wear tests were performed on the self-made fretting wear rig to investigate fretting wear behaviors of steel wires under friction-increasing grease conditions. The results demonstrated that the fretting regimes were dependent on displacement amplitudes and normal loads. The friction coefficient exhibited different variation trends in different fretting regimes. Friction-increasing grease changed the fretting running behavior and had a very good wear resistance for steel wires. Wear was slight in partial slip regime. Mixed regime was characterized by plastic deformation, fatigue cracks and abrasive wear. Slip regime presented main damage mechanisms of abrasive wear, fatigue wear and oxidation.     

桨-毂轴承材料扭动微动磨损行为研究

采用面接触扭动微动形式,以动力定位系统可调距螺旋桨桨-毂轴承摩擦副材料(CuNiAl-42CrMo4)为对象,以不同的角位移幅值模拟海水波动影响下的微动磨损行为,并结合扫描电子显微镜和超景深三维显微镜对磨痕形貌进行分析,探究桨-毂轴承摩擦副材料扭动微动磨损规律。结果表明,随着角位移幅值的增加,扭动微动依次运行于部分滑移区、混合区、滑移区,摩擦因数减小,同时磨损量增加,微动损伤中剥层机制所占的比例逐渐增加,且由于疲劳裂纹扩展的不利影响,实际运行过程中要尽量避开混合区。     

粘结MoS2固体润滑涂层的转动微动磨损特性

采用粘结法在LZ50钢表面制备MoS2固体润滑涂层,研究MoS2涂层及LZ50钢基体在干态不同角位移幅值下的转动微动磨损行为。在分析转动微动动力学特性的同时,结合光学显微镜、扫描电子显微镜、电子能谱仪以及轮廓仪对磨痕形貌进行微观分析。结果表明:涂层和基体的转动微动运行区域仅呈现部分滑移区(Partial slip regime,PSR)和滑移区(Slip regime,SR),未观察到混合区。涂层改变基体的微动运行区域,使得PSR缩小,SR运行区域向小角位移幅值方向移动。由于MoS2涂层的固体润滑作用,涂层的摩擦因数在整个试验过程都明显低于基体。在PSR,涂层损伤轻微;在SR,涂层的转动微动磨损机制主要表现为剥层和摩擦氧化。研究表明粘结MoS2固体润滑涂层具有明显的防护作用,显著降低LZ50钢的转动微动磨损。     

Fretting Wear Behavior of UHMWPE—Influence of Load and Stroke

In this study, the tribological behavior of ultra-high-molecular-weight polyethylene (UHMWPE) against a GCr 15 steel ball during fretting wear conditions was investigated using an oscillating reciprocating tribometer. The aim of this study was to characterize the critical value of normal load and stroke corresponding to this transition in UHMWPE worn surface at room temperature. Results showed that there existed a critical value of load or stroke at fixed condition. The friction coefficient and wear volume loss of UHMWPE at or near the critical values of load and stroke exhibited extreme changes. Based on observation of the worn surface by scanning electron microscopy (SEM) and 3D surface profiler measurements, it can be found that damage to the worn surface can be linked to the contact load and stroke. In addition, results showed that during the process of fretting wear under different load or stroke conditions, the gross slip regime dominated throughout the whole test period.     

基于双重扩展自适应卡尔曼滤波的汽车状态和参数估计

准确实时地获取行驶过程中的状态信息是汽车动态控制系统研究的关键,为此提出了一种新的汽车状态估计器。建立了包含不准确模型参数和未知时变统计特性噪声的非线性汽车动力学模型,针对该非线性系统提出一种双重扩展自适应卡尔曼滤波算法（DEAKF）。该算法采用两个卡尔曼滤波器并行运算,状态估计和参数估计互相更新,同时将带遗忘因子的噪声统计估值器嵌入到状态校正过程和参数校正过程之间,以解决系统的噪声时变问题。基于ADAMS的虚拟试验和实车试验结果表明,该算法的状态估计精度高于EKF方法和DEKF方法的状态估计精度,同时具有良好的模型参数校正能力,对汽车动态控制系统中估计器的设计具有理论指导意义。
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中性腐蚀环境下钢丝的微动疲劳行为

在自制的微动疲劳试验机上开展中性腐蚀环境下单根钢丝的微动疲劳实验,考察在相同接触载荷下,不同振幅对钢丝的微动疲劳行为的影响,并用扫描电子显微镜观察疲劳钢丝的磨痕和断口形貌,研究钢丝微动疲劳断裂机制.结果表明:在较大的振幅下,钢丝的微动区均处于滑移状态,而在较小振幅下,钢丝的微动区从滑移状态逐渐转变为黏着状态;磨损机制主要为磨粒磨损、疲劳磨损、腐蚀磨损和塑性变形;钢丝疲劳寿命随着微动振幅的增大而减小;钢丝的疲劳断口可分为3个区域,即疲劳源区、裂纹扩展区及瞬间断裂区.     

Fretting properties of SUS304 stainless steel in a vacuum environment

In this paper the effect of the ambient pressure on the friction and wear of SUS304 stainless steel during fretting at room temperature is described.

The ambient pressure was varied from 10⁻³ to 10⁵ Pa. The experiment was carried out under the following conditions: normal load, 14 N; slip amplitudes, 35 and 110 μm; frequency, 8.3 Hz; number of fretting cycles, 6 × 10⁴.

The relationship between the frictional behaviour and the number of cycles is affected by the pressure. The coefficient of friction at steady state increases with a decrease in the pressure to below 10 Pa. From the point of view of the wear mechanism, the transition is determined as that from oxidative wear at the higher pressure to adhesive wear at the lower pressure. The transition pressure depends on the slip amplitude, i.e.it is 2.7 Pa at 35 μm and 10⁻¹ Pa at 110 μm. The wear volume is greater in the oxidative wear regime than in the adhesive wear regime. Oxide wear debris is removed easily from the interface in the former regime. In contrast, metallic wear debris is retained at the interface and adhesive transfer occurs from one surface to the opposing surface in the latter regime. The characteristic feature of the wear damage at 10⁻³ Pa and at 35 μm is the formation of a vertical crack at the boundary between the fretted and the unfretted areas.     

Fretting wear behaviors of a railway axle steel

Fretting damage was one of the most important reasons for the failure of the railway axle. Fretting wear (tangential fretting mode) tests of a railway axle steel (LZ50 steel) flats against 52 100 steel balls were carried out under different normal loads and displacement amplitudes on a hydraulic fretting wear rig. Dynamic analyses in combination with microscopic examinations have been performed. The experimental results showed that the fretting regimes of the LZ50 steel were strongly dependent upon the imposed normal loads and displacement amplitudes. The F_t/F_n curves exhibited different variation trends in different fretting running regimes. The fretting scars presented slight damage in partial slip regime. In mixed fretting regime, the trace of the plowing and plastic deformation flow can be observed on the fretting scars. The wear mechanism during this regime was the combination of the abrasive wear, oxidative wear and delamination accompanied with obvious plastic deformation. The detachment of particles and plowing traces were the main phenomena in slip regime. And, thicker debris layer covered the contact zone of the scar. The severe degradation in slip regime presented the main wear mechanisms of abrasive wear, oxidative wear and delamination.     

Effect of contact load on fretting fatigue behaviour of steel wires

Abstract

The tension–tension fretting fatigue tests of steel wires were performed on a self-made fretting fatigue test equipment under contact loads ranging from 40 to 70 N and a strain ratio of 0·8. The results showed that when the contact load increased, the fretting regime of steel wires transformed from gross slip regime to mixed fretting regime. The fretting fatigue life in the mixed fretting regime was significantly lower than that in the gross slip regime. The main fretting wear mechanisms in the gross slip regime, where there were serious fretting damage and a lot of wear debris, were abrasive wear and fatigue wear. Microcracks were observed in the fretting scar of the mixed fretting regime, and the main fretting wear mechanisms were adhesive and fatigue wears. The fretting wear scar was the fatigue source region, and the fatigue fracture surface could be divided into three regions.     

人股骨皮质骨轴面微动摩擦磨损特性研究

采用高精密微动试验台外加体液恒温循环装置,在一定法向载荷和不同位移幅值条件下,研究了天然活性人股骨皮质骨对纯钛的微动摩擦磨损行为。试验结果显示：随位移幅值的增加,股骨皮质骨的微动运行状态从部分滑移向完全滑移状态转变,详细讨论了不同位移幅值下摩擦因数随循环次数的演变规律。微观观察表明：接触表面处于部分滑移状态时损伤轻微,而在完全滑移状态下磨损较严重。人股骨皮质骨的磨损机理主要表现为磨粒磨损和微骨折导致的剥层剥落。微动磨痕的深度随位移幅值的增加而增加,而且磨痕深度与摩擦因数有很好的对应关系。研究认为控制植入体/骨界面的微动幅度有利于提高皮质骨抗微动损伤的能力。