强磁场对Bi-Mn合金半固态凝固过程中MnBi析出相组织的影响

在Bi-6%Mn合金从高于355℃(升温过程中MnBi化合物磁性转变温度)的固液两相区凝固过程中,研究了MnBi析出相组织在无磁场和强磁场条件下的演化过程.结果表明:在无磁场条件下MnBi析出相形态在340℃(MnBi相顺磁-铁磁转变温度)附近发生突变,由较规则的六方块状变为沿ab面长大的不规则片状;10 T磁场条件下析出相形态突变的温度提高到355℃左右.另外,10 T磁场能够控制析出相晶粒以c轴平行磁场取向、定向聚合和熔合长大,使析出相的最终形态又趋向较规则的六方块状.     

磷酸钙骨水泥的生物相容性

磷酸钙（α-TCP/TTCP）复合骨水泥具有良好的水硬性能，与固化液按固液比为1.50g/mL拌和后，凝固时间可调，抗压强度达45．36MPa，其水化产物为羟基磷灰石（HAP）。通过体外模拟溶解实验表明，α-TCP/TTCP骨水泥具有一定的溶解性能，通过体外实验，动物实验，结合SEM和EPMA观察表明α-TCP/TTCP骨水泥不会产生全身或局部毒性反应，对肌肉无刺激，不致溶血，凝血，不引起炎症和排斥反应等，有利于骨组织长入并与骨组织紧密接触。α-TCP/TTCP骨水泥在动物体内可继续水化硬化，且随着植入时间的延长，材料与缩主骨完全融合在一起，α-TCP/TTCP骨水泥具有优良的生物相容性和生物活性，具有一定的降解性能和较好的成骨作用，适合于作为骨缺损的填充材料。     

EFFECTS OF CARBON AND YTTRIUM ON 500℃ AGING EMBRITTLEMENT OF ALLOY Fe-15Cr-4Al

测定了Ｆｅ－１５Ｃｒ－４Ａｌ合金在５００℃的时效脆化动力学，利用内耗，ＴＥＭ，ＥＰＭＡ和ＳＥＭ等手段研究了合金在时效后的组织变化和断裂行为。结果表明，时效脆化第一阶段（０－１００ｈ）主要是碳化物在α相晶界析出的作用，它损害界面结合，降低断裂应力，使塑性在时效０．２５ｈ后消失；第二阶段（１００－１０００ｈ）主要是富Ｃｒ－α＇相均匀析出的作用，它通过强化基体引起二次脆化。含０．２和０．４％的Ｆｅ－１５     

A new high strength and high tolerance-resistance A1-Li alloy

In order to develop a new high strength and high tolerance-resistance Al-Li alloy which can be used in aerospace industry, the effects ofmicroalloying elements such as Mg, Ag, Mn and Zn on the mechanical properties of Al-Cu-Li alloys were studied. The results show that the strengthening effects of Mg＋Ag and Mg＋Zn additions are higher than those of the individual Mg, Ag or Zn addition. The element Mn can also bring some extent strengthening effects on the alloys, but it has nothing to do with the other microalloying elements present or not. Finally, a new Al-Li alloy with Mg＋Zn＋Mn additions was developed, which possesses high strength and high tolerance-resistance promising properties for aerospace applications.     

单晶铜制备HSYV-5e 4×2×0.5数字通讯电缆的性能研究

用自制区域熔炼单晶化设备制备了直径为2.7 mm铜单晶线材,经过冷拔加工至直径为0.51 mm,采用信息产业部生产标准YD/T 1019-2001制成HSYV-5e 4×2×0.5数字通讯实心水平对绞电缆,分别对导体材料为变形单晶铜和普通无氧铜电缆的电气性能进行检测,对比试验结果表明:变形单晶铜比普通无氧铜电缆的直流电阻低4.59%;变形铜单晶电缆对信号的衰减作用有明显的改善;单晶铜线材冷拔变形后显微组织存在变形孪晶和晶界.     

网状阳极在大型储罐底板阴极保护工程中的应用

文章介绍了网状阳极在茂名、湛江、岚山和上海地区的大型储罐阴极保护系统的应用情况。从实际运行的结果看,罐底板的保护电位都达到了设计要求和标准规定,保护电位分布相当均匀。保护电流密度也满足了设计要求。保护效果较好,表明网状阳极对于大型储罐的外底板的阴极保护是一种较好的解决方案。对于发现的几个问题也作了讨论。     

Structure and tensile／wear properties of microarc oxidation ceramic coatings on aluminium alloy

Thick and hard ceramic coatings were prepared on the Al-Cu-Mg alloy by microarc oxidation in alkali-silicate electrolytic solution. The thickness and microhardness of the oxide coatings were measured. The influence of current density on the growth rate of the coating was examined. The rnicrostructure and phase composition of the coatings were investigated by means of scanning electron microscopy, energy dispersive spectroscopy, and X-ray diffraction. Moreover, the tensile strength of the AI alloy before and after microarc oxidation treatment were tested, and the fractography and morphology of the oxide coatings were observed using scanning electron microscope. It is found that the current density considerably influences the growth rate of the microarc oxidation coatings. The oxide coating is mainly composed of α-Al2 O3 and γ-Al2O3, while high content of Si is observed in the superficial layer of the coating. The cross-section microhardness of 120μm thick coating reaches the maximum at distance of 35μm from the substrate/coating interface. The tensile strength and elongation of the coated AI alloy significantly decrease with increasing coating thickness. The rnicroarc oxidation coatings greatly improve the wear resistance of AI alloy, but have high friction coefficient which changes in the range of 0.7-0.8. Under grease lubricating, friction coefficient is only 0. 15 and wear loss is less than 1/10 of the loss under dry friction.     

双孔模型材挤压过程的有限元分析

本文采用大变形弹塑性有限元理论 ,对双孔模型材挤压成形过程进行了有限元分析。模拟了双孔模非对称角铝型材挤压变形过程 ,获得了挤压变形时网格畸变、流速、应力和应变分布 ,展示了型材挤压件变形不均匀细节。并与单孔模型材挤压过程进行了比较 ,发现双孔模[1] 挤压时 ,变形体内存在两个互为相反方向的涡流场 ,它们相互抵消 ,从而可以消除型材挤压过程中产生的扭拧、波浪、弯曲等缺陷。为提高挤压件质量 ,优化设计多孔型材挤压模以及制定合理的工艺 ,提供了理论依据     

SiCp/AZ61镁基复合材料制备工艺和性能的研究

研究了三种不同铸造工艺条件下镁基复合材料的组织结构,并对其硬度进行了测定。结果表明:与全液态铸造法和半固态铸造法相比,搅熔铸造制备的SiCp/AZ61镁基复合材料,其增强相SiC颗粒分布均匀,气孔率较少,是一种较理想的金属基复合材料制备工艺。未增强的AZ61基体镁合金的维氏硬度高于其半固态坯料的维氏硬度;而SiCp/AZ61镁基复合材料的维氏硬度明显高于基体的维氏硬度,并随着SiC颗粒体积分数的增加其复合材料的维氏硬度不断提高。     

瞬间液相连接的过冷连接新工艺

提出了瞬间液相(TLP)连接的新工艺--过冷连接工艺,即首先将待连接区域加热至某高温进行短时保温,然后再降至一定温度进行长时保温连接.由于液相经历了一次温度过冷,在液/固界面前沿就形成了成分过冷区,破坏了平衡状态下的界面稳定性,形成胞状界面.随着凝固过程的完成,界面消失,形成跨界面连续晶粒,实现冶金接合.以Fe-Ni基非晶合金为中间层,进行了低碳钢过冷TLP连接实验,并与传统的TLP连接工艺进行了比较.结果表明,过冷TLP连接工艺产生了非平面状界面,并且随着凝固的完成界面消失,形成无界面的组织均匀接头.与传统TLP连接工艺接头相比,过冷TLP连接工艺可大大提高接头冲击韧性,其数值达到母材水平.