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991.
The deactivation characteristics of Pd/SiO2 in the selective hydrogenation of acetylene were correlated with changes in the amount of the C4 species produced. The amounts of butenes produced changed in parallel with the catalyst activity, indicating that the rate limiting step for butene production was the same as that for acetylene hydrogenation. On the other hand, the amount of 1,3-butadiene produced changed, showing a maximum with catalyst deactivation because 1,3-butadiene is an intermediate in the sequential reaction process which involves both the production and consumption of 1,3-butadiene. This was verified by a simultaneous TG/reaction experiment showing that 1,3-butadiene was a precursor of green oil. The catalyst showed a self-regenerative behavior in its activity and the amounts of C4 species produced during the early stage of deactivation because two opposite factors, which contributed to either the lowering or the promotion of activity, were involved in the process. A specific type of polymer species, produced during the initial period of deactivation, is proposed to be responsible for the promotion of catalyst activity. 相似文献
992.
In order to develop a basic electrode with low fume and good usability, a uew slag system has been designed after analyzing several basic electrode slag systems. Then in view of uniform design method, arranging the experiment points by it, the influenced laws of the uew system coating compouents on the arc stability had been searched. In the formula, niue coating compouents were taken as independent variables and they were divided into six levels in all twenty-four experiments. The arc stability was taken as function and taken down the data when welding and then put them into the computer to be processed statistically. The analysis results give the mathematical model and trend diagrams between independent variables and the function. They indicate that the effects of many coating compouents on the arc stability are in the mutual form. The mutual effects between CaCO3 and BaF2, BaF2 and BaCO3 , increases the arc stability separately. While the mutual effects between CaF2 and iron powder, the square item of iron powder itself decreases the arc stability separately. 相似文献
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998.
Porous alumina films can be found in a wide variety of materials, including filters, thermal insulation components, dielectrics, biomedical and catalyst supports, coatings and adsorbents. Production methods for these films are as equally diverse as their applications. In this work, a hybrid process based upon chemical vapor deposition and gas-to-particle conversion is presented as an alternative technique for producing porous alumina films, with the main advantages of solvent-free, low substrate-temperature operation. In this process, nanoparticles were produced in the vapor phase by reaction of aluminum acetylacetonate in the presence of oxygen. Downstream of this reaction zone, these nanoparticles were collected via thermophoresis onto a cooled substrate, forming a porous film. Some deposited films were subjected to post-processing in the form of annealing in air. Fourier-transform infrared spectra and X-ray energy-dispersive spectroscopy analysis confirmed the production of alumina at processing temperatures above 973 K. X-Ray diffraction revealed that the films were amorphous. Film thickness, ranging from 30 to 250 μm, and the average deposition rate were determined from scanning electron microscopy results. From transmission electron microscopy, the average primary particle size was determined to be approximately 18 nm and the formation of nanoparticle aggregates was evident. Annealing of the films at temperatures ranging from 523 to 1173 K in the presence of air did not have an effect on particle size. The specific surface area of the powder composing the films ranged from 10 to 185 m2 g−1, as determined from nitrogen gas adsorption by the Brunauer–Emmett–Teller method. 相似文献
999.
接地故障保护的设置和整定(三) 总被引:1,自引:0,他引:1
7 TT系统接地故障保护 TT系统的电源中性点直接接地,而电气设备的外露可导电部分则经各自的PE线接地。这样在大多数情况下,由于故障回路包括两个接地电阻,使接地故障电流太小,不足以使过电流保护动作切断接地故障电流。而且由于故障电流小,故障点未被熔焊,故障点阻抗是难以估计的接触电阻。因此,TT系统接地故障回路阻抗和故障电流难以估算。所以,必须设置漏电电流动作保护。 相似文献
1000.
本文从TBM地区目的层的地质和地球物理特征分析出发,以三维地震资料为基础,综合利用人工和神经网络波形分类等定性储层预测方法和利用反演及敏感地震属性分析,对TBM地区低孔渗砂岩分布区开展了砂体展布特征分析和天然气高产区预测研究。根据研究结果部署了10口钻井,已完钻的4口井中有3口获得高产气流(其中DK27井日产天然气36.8×104m3)。值得指出的是,目前所用的预测方法还不能预测厚度小于6m的单砂层或砂层组构成的储层。 相似文献