LLM-105的Cu(Ⅱ)和Co(Ⅲ)含能配合物:热分解特性及与HMX相容性

为了研究LLM-105(2,6-二氨基-3,5-二硝基吡嗪-1-氧化物)与过渡金属Cu和Co配合物的热分解特性及其相容性,合成了LLM-105与Cu(Ⅱ)和Co(Ⅲ)的配合物,用傅里叶变换红外光谱和粉末X射线衍射表征其结构。采用差示扫描量热法(DSC)测试了不同升温速率下Cu(Ⅱ)和Co(Ⅲ)配合物的分解温度,并用Kissinger法和Ozawa-Doyle法计算了其表观活化能(E)和指前因子(A);利用转化率(α)和与其对应的温度(T),得到不同转化率下活化能随温度变化曲线。利用DSC测试了Cu(Ⅱ)和Co(Ⅲ)配合物与HMX在不同质量比下混合炸药的分解温度,并对其相容性进行了分析,结果表明,Cu(Ⅱ)配合物与HMX相容性较好,且优于Co(Ⅲ)配合物。     

NFC端到端兼容性测试研究

近场支付由于其产业链过长、相关硬件厂商众多的特点,给其兼容性带来了巨大挑战.在NFC一致性测试的基础上,提出了严格的一致性测试、仪表兼容性测试、R/W兼容性测试、POS兼容性测试等4种提高NFC终端与POS之间兼容性的测试方法,并分析了其优缺点.行业相关方可结合自身资源及需求,采用其中一种或几种方法相结合的测试手段,提高NFC端到端兼容性,优化NFC支付生态环境.     

添加剂对航空润滑油橡胶相容性的影响

采用满足MIL-PRF-23699F规范中航空发动机润滑油要求的季戊四醇酯为基础油，研究了3种抗氧剂和3种极压抗磨剂对航空润滑油橡胶相容性的影响。结果表明：磷酸酯极压抗磨剂使丁腈橡胶的体积变化率增大，其他添加剂对丁腈橡胶的体积变化率无显著影响；极压抗磨剂对氟橡胶的体积变化率几乎没有影响，而抗氧剂使氟橡胶的体积变化率有微弱的减小；胺类添加剂在酯类润滑油中对氟橡胶拉伸性能无显著影响；酸性磷酸胺极压抗磨剂使硅橡胶体积发生收缩，使氟硅橡胶的体积变化率减小；酸性磷酸胺极压抗磨剂与硅橡胶和氟硅橡胶可发生化学反应，使橡胶的拉伸性能大幅下降。     

Coupled field formulation of exactly integrated membrane finite elements insensitive to distortion

Abstract

An efficient 4-noded membrane element tolerant and insensitive to mesh distortion is developed using kinematically coupling the in-plane displacements which satisfy the equilibrium equations in Cartesian coordinates and results in material-dependent coupled field interpolation functions making the element free from volumetric and shear locking. The proposed formulation provides a preliminary concept for the satisfaction of natural boundary conditions which is used to satisfy the strong patch test. The proposed element, passed several benchmark problems from the literature, compared well with elasticity solutions, passed the weak patch test and the inf-sup test for both compressible and incompressible cases.     

Crystal structure and functional properties of Nd1.6Ca0.4Ni1-yCuyO4+δ as prospective cathode materials for intermediate temperature solid oxide fuel cells

Complex oxides Nd_1.6Ca_0.4Ni_1-yCu_yO_4+δ (y = 0.0–0.4) have been prepared by a pyrolysis of glycerol-nitrate compositions. According to the X-ray diffraction analysis, the materials are single-phase up to y = 0.3 and crystallize in an orthorhombic structure (Bmab) at room temperature. High-temperature studies assert that they all undergo a phase transition from orthorhombic to tetragonal (I4/mmm) structure in a range of 300–400 °C. With Cu doping, the over-stoichiometric oxygen content δ decreases from 0.07 (y = 0.0) down to 0.00 (y = 0.3). The studies on the compact samples reveal the maximum value of total conductivity (165 S cm^?1 at 420 °C) and the minimum value of the linear coefficient of thermal expansion (11.9·10^?6 K^?1 in a range of 400–1000 °C in air) at y = 0.2. Chemical compatibility of the Nd_1.6Cа_0.4Ni_1-yCu_yO_4+δ (y = 0.0, 0.2) oxides with oxygen- and proton conducting electrolytes (Ce_0.9Gd_0.1O_1.95, Ce_0.8Sm_0.2O_1.9 and BaCe_0.5Zr_0.3Y_0.1Yb_0.1O_3-δ) up to a temperature of 1100 °C is demonstrated.     

油基泥饼解除液体系研制及性能评价

针对东海油田钻井过程中油基钻井液在井壁和筛管上形成的泥饼难以清除等复杂问题,室内经过有机溶剂、有机酸、增溶剂等处理剂优化筛选,研制出一套油基泥饼解除液体系,其配方为:55%5#白油+45%增溶剂HZRJ+5.5%有机酸HTS+5%有机溶剂RJ;通过API滤失实验、配伍性实验、渗透率恢复值实验对体系进行了性能评价,结果表明该体系具有良好的泥饼解除效果和较强的储层保护能力,且与钻井液及储层岩石、原油具有较好的配伍性。     

电磁兼容性试验方法CE107对电源线尖峰信号(时域)传导发射的解读

简述了电源线尖峰信号的传导发射,讨论了在电源开关通断状态尖峰信号最大值记录,给出了CE107项目测试方法的不足,并且提出了新的测试方法,给出了对此测试方法的理解。     

Display-control compatibility: the relationship between performance and judgments of performance

This study examined whether people can judge the usability of display-control mappings. Participants identified one of two alternatives which were presented in a questionnaire. Several types of stimuli were tested, ranging from simple shapes to semantic stimuli. Choices were found to be predominately correct when usability was defined by an unambiguous spatial relationship between displays and controls. In contrast, estimates were less accurate for items which did not solely rely on spatial congruence. The findings were interpreted in terms of the factors that need to be considered for judgments to be free of error.     

Systematic layout planning in human–system interface: An evaluation of alarm displays with spatial proximity for accidents diagnosis of advanced boiling water reactor

To ensure safety in nuclear power plants, this study investigated the interface design of a digital alarm system by analyzing the diagnosing process of operating information. This study focused on the layout planning of alarm windows and followed proximity compatibility principle and nuclear human–system interface design review guidelines to improve the human–system interface. This study adopt systematic layout planning to modify the design of alarm windows. The time of alarm handling, and accuracy, as well as human reliability were evaluated to compare the original layout with the improved one. In the end, according to the results of the comparison, an alternative alarm window layout human–system interface, which fits diagnosing process, is suggested.Relevance to industryThe similar layout planning process could be applied to design control centers in high reliability organizations, in particular which need decision-making by person.