全文获取类型
收费全文 | 20996篇 |
免费 | 1801篇 |
国内免费 | 920篇 |
专业分类
电工技术 | 620篇 |
综合类 | 1539篇 |
化学工业 | 4530篇 |
金属工艺 | 1466篇 |
机械仪表 | 428篇 |
建筑科学 | 1692篇 |
矿业工程 | 963篇 |
能源动力 | 531篇 |
轻工业 | 3754篇 |
水利工程 | 547篇 |
石油天然气 | 1411篇 |
武器工业 | 51篇 |
无线电 | 880篇 |
一般工业技术 | 1437篇 |
冶金工业 | 1691篇 |
原子能技术 | 157篇 |
自动化技术 | 2020篇 |
出版年
2024年 | 39篇 |
2023年 | 261篇 |
2022年 | 538篇 |
2021年 | 681篇 |
2020年 | 667篇 |
2019年 | 621篇 |
2018年 | 607篇 |
2017年 | 698篇 |
2016年 | 764篇 |
2015年 | 786篇 |
2014年 | 1335篇 |
2013年 | 1404篇 |
2012年 | 1616篇 |
2011年 | 1654篇 |
2010年 | 1186篇 |
2009年 | 1145篇 |
2008年 | 1004篇 |
2007年 | 1276篇 |
2006年 | 1136篇 |
2005年 | 954篇 |
2004年 | 914篇 |
2003年 | 764篇 |
2002年 | 609篇 |
2001年 | 505篇 |
2000年 | 450篇 |
1999年 | 380篇 |
1998年 | 285篇 |
1997年 | 217篇 |
1996年 | 207篇 |
1995年 | 197篇 |
1994年 | 166篇 |
1993年 | 127篇 |
1992年 | 103篇 |
1991年 | 85篇 |
1990年 | 57篇 |
1989年 | 48篇 |
1988年 | 40篇 |
1987年 | 27篇 |
1986年 | 25篇 |
1985年 | 25篇 |
1984年 | 16篇 |
1983年 | 8篇 |
1982年 | 19篇 |
1981年 | 13篇 |
1980年 | 9篇 |
1979年 | 7篇 |
1964年 | 4篇 |
1960年 | 3篇 |
1959年 | 3篇 |
1958年 | 3篇 |
排序方式: 共有10000条查询结果,搜索用时 29 毫秒
1.
2.
Zhongchao Fu Xiaodong Li Mu Zhang Qi Zhu Ji-Guang Li Jiao He Xing'an Wang Xudong Sun 《Journal of the American Ceramic Society》2021,104(6):2689-2701
An easy albeit quite effective deionization suspension treatment was adopted to alleviate the detrimental effects related to the hydrolysis of Y2O3 in an aqueous medium. Fabrication of highly transparent Y2O3 ceramics with a fine grain size via air pre-sintering and post–hot isostatic pressing (HIP) treatment without using any sintering additive was achieved using the treated suspensions. The hydrolysis issue of Y2O3 powder in an aqueous medium was effectively alleviated by using deionization treatment, and a well-dispersed suspension with a low concentration of dissolved Y3+ species was obtained. The dispersed suspensions were consolidated by the centrifugal casting method, and the green bodies derived from the suspension of 35.0 vol% solid loading showed an improved homogeneity with a relative density of 52.1%. Fully dense Y2O3 transparent ceramic with high transparency was obtained by pre-sintering consolidated green compacts at a low temperature of 1400°C for 16 h in air followed by a post-HIP treatment at 1550°C for 2 h under 200 MPa pressure. The sample had a fine average grain size of 690 nm. The in-line transmittance of the sample reached 83.3% and 81.8% at 1100 nm and 800 nm, respectively, very close to the theoretical values of Y2O3. 相似文献
3.
《Ceramics International》2021,47(23):33353-33362
High thermal conductivity Si3N4 ceramics were fabricated using a one-step method consisting of reaction-bonded Si3N4 (RBSN) and post-sintering. The influence of Si content on nitridation rate, β/(α+β) phase rate, thermal conductivity and mechanical properties was investigated in this work. It is of special interest to note that the thermal conductivity showed a tendency to increase first and then decrease with increasing Si content. This experimental result shows that the optimal thermal conductivity and fracture toughness were obtained to be 66 W (m K)-1 and 12.0 MPa m1/2, respectively. As a comparison, the nitridation rate and β/(α+β) phase rate in a static pressure nitriding system, i.e., 97% (MS10), 97% (MS15), 97% (MS20) and 8.3% (MS10), 8.3% (MS15), 8.9% (MS20), respectively, have obvious advantages over those in a flowing nitriding system, i.e., 91% (MS10), 91% (MS15), 93% (MS20) and 3.1% (MS10), 3.3% (MS15), 3.3% (MS20), respectively. Moreover, high lattice integrity of the β-Si3N4 phase was observed, which can effectively confine O atoms into the β-Si3N4 lattice using MgO as a sintering additive. This result indicates that one-step sintering can provide a new route to prepare Si3N4 ceramics with a good combination of thermal conductivity and mechanical properties. 相似文献
4.
5.
目的 麦胚孵育过程中蛋白酶将蛋白质水解成肽和氨基酸,多肽具有明确的生理活性和营养调节作用。本研究以麦胚为试验原料,采用微波辅助预处理的方法,研究孵育的温度、时间、pH及料液比4种因素对孵育后的蛋白酶活力及多肽含量的影响。 方法 通过单因素和响应曲面试验进行工艺条件优化。 结果 与未进行微波辅助预处理的样品相比,微波辅助处理(600 W, 10 s)能显著提高孵育后样品中的蛋白酶酶活力(约9.4倍)和肽含量(约3.1倍)。经过微波辅助处理后,孵育温度为51.5℃、pH为4.0、时间为6.33 h、料液比为1:7时,蛋白酶活力达最高为3826.24 U/g;孵育温度为45.0 ℃、pH为4.8、时间为8 h、料液比为1:7时,肽含量达最高为262.63 mg/g。 结论 微波辅助处理能有效的激活麦胚孵育液中的内源性蛋白酶活性,促进蛋白水解反应,显著提高孵育后的肽含量。该研究结果为麦胚多肽的制备新工艺开发提供了研究基础。 相似文献
6.
介绍了宁波中金石化有限公司200 kt/a 间二甲苯(MX)吸附分离装置的工业应用情况。该装置于2020年建成投产,一次投料开车成功,为全球最大的MX生产装置。装置性能测试结果表明,MX产能达到203.3 kt/a,产品纯度(w)为99.53%,单程收率为95.1%。保持吸附剂在合适的水含量范围内可以有效提高吸附剂选择性,提高产品纯度和单程收率;苯为吸附剂的暂时性毒物,解吸剂中苯含量增加会降低吸附分离过程的单程收率。 相似文献
7.
Qing Li Jun Wang Jie Ma Meng Ni Fan Yang Peng Liu Kuo Yang Lee Hsing-I Hsiang Deyuan Shen Dingyuan Tang 《Journal of the American Ceramic Society》2022,105(5):3375-3381
High-efficiency Yb:Y2O3 laser ceramics were fabricated using the vacuum-sintering plus hot isostatic pressing (HIP) without sintering additives. High-purity well-dispersed nanocrystalline Yb:Y2O3 powder was synthesized using a modified co-precipitation method in-house. The green bodies were first vacuum sintered at a temperature as low as 1430°C and then HIPed at 1450°C. Finally, the samples were air annealed at 800°C for 10 h. Although no sintering aids were used, full density of the samples with excellent optical homogeneity and an inline transmission of 80% at 400 nm could be obtained. Moreover, photodarkening phenomenon was not detected in the ceramics. Preliminary laser experiment with the fabricated ceramics in a two-mirror cavity has demonstrated 32 W continuous-wave (CW) output at ∼1077 nm with an optical-to-optical conversion efficiency of 58.2%. To the best of our knowledge, this is so far the highest CW output power and optical-to-optical conversion efficiency achieved with the Yb3+-doped sesquioxide ceramics in a simple two-mirror cavity. 相似文献
8.
This paper presents a novel No-Reference Video Quality Assessment (NR-VQA) model that utilizes proposed 3D steerable wavelet transform-based Natural Video Statistics (NVS) features as well as human perceptual features. Additionally, we proposed a novel two-stage regression scheme that significantly improves the overall performance of quality estimation. In the first stage, transform-based NVS and human perceptual features are separately passed through the proposed hybrid regression scheme: Support Vector Regression (SVR) followed by Polynomial curve fitting. The two visual quality scores predicted from the first stage are then used as features for the similar second stage. This predicts the final quality scores of distorted videos by achieving score level fusion. Extensive experiments were conducted using five authentic and four synthetic distortion databases. Experimental results demonstrate that the proposed method outperforms other published state-of-the-art benchmark methods on synthetic distortion databases and is among the top performers on authentic distortion databases. The source code is available at https://github.com/anishVNIT/two-stage-vqa. 相似文献
9.
《International Journal of Hydrogen Energy》2022,47(25):12726-12738
The use of a Pt-based catalyst was evaluated for autocatalytic hydrogen recombination. The Pt was supported on a mixture of Ce-, Zr- and Y-oxides (CZY) to yield nanosized Pt particles. The Pt/CZY/AAO catalyst was then prepared by the spray-deposition of the Pt/CZY intermediate onto an anodized aluminium oxide (AAO) layer on a metallic aluminum core. The Pt/CZY/AAO catalyst (3 × 1 cm) was evaluated for hydrogen combustion (1–8 vol% hydrogen in the air) in a recombiner section testing station. The thermal distribution throughout the catalyst surface was investigated using an infrared camera. The maximum temperature gradient (ΔT) for the examined hydrogen concentrations did not exceed 36 °C. The Pt/CZY/AAO catalyst was also evaluated for prolonged hydrogen combustion duration to assess its durability. An average combustion temperature of 239.0 ± 10.0 °C was maintained for 53 days of catalytic hydrogen combustion, suggesting that there was limited, or no, catalyst deactivation. Finally, a Pt/CZY/AAO catalytic plate (14.0 × 4.5 cm) was prepared to investigate the thermal distribution. An average surface temperature of 212.5 °C and a maximum ΔT of 5.4 °C was obtained throughout the catalyst surface at a 3 vol% hydrogen concentration. 相似文献
10.
《International Journal of Hydrogen Energy》2022,47(79):33765-33780
This work investigates selective Ni locations over Ni/CeZrOx–Al2O3 catalysts at different Ni loading contents and their influences on reaction pathways in ethanol steam reforming (ESR). Depending on the Ni loading contents, the added Ni selectively interacts with CeZrOx–Al2O3, resulting in the stepwise locations of Ni over CeZrOx–Al2O3. This behavior induces a remarkable difference in hydrogen production and coke formation in ESR. The selective interaction between Ni and CeZrOx for 10-wt.% Ni generates more oxygen vacancies in the CeZrOx lattice. The Ni sites near the oxygen vacancies enhance reforming via steam activation, resulting in the highest hydrogen production rate of 1863.0 μmol/gcat·min. In contrast, for 15 and 20-wt.% Ni, excessive Ni is additionally deposited on Al2O3 after the saturation of Ni–CeZrOx interactions. These Ni sites on Al2O3 accelerate coking from the ethylene produced on the acidic sites, resulting in a high coke amount of 19.1 mgc/gcat·h (20Ni/CZ-Al). 相似文献