电压调节变色的有机薄膜电致发光器件

制备了结构为ＩＴＯ／ＳＡ／ＰＢＤ／Ａｌｑ３／Ａｌ的电压调制发光颜色的有机薄膜电致发光器件，研究了有机层厚度不同的器件的发光光谱随电压变化的性能，建立了器件的能级结构模型，并用这种模型解释了器件的电致发光性能。     

垂直沟道器件的研究与进展

介绍了垂直沟道器件的常见结构和工艺，分析了垂直沟道器件的最新进展以及垂直沟道器件制作工艺中的最新技术，详细讨论了垂直沟道器件的性能，并分析了垂直沟道器件的优点以及存在的问题。     

SOI和应变Si的将来

利用SOI衬底生长部分／完全耗尽结构的晶体管或用应变沟道提高器件性能可制备出高性能CMOS逻辑器件；这两种方法均可用于CMOS结构，也可单独用于提高器件性能。将应变用于器件沟道，可将沟道迁移率提高50％，从而提高了器件电流。SOI晶体管的好     

金刚石薄膜电致发光中的奇异现象

制备了不同结构的金刚石薄膜电致发光器件，研究了其光谱特性和发光特性。结果发现一般结构的样品器件的发光强度和激发电源频率之间存在一极大值， 特殊结构的样品器件的发光强度和激发电压之间存在一极大值的奇异现象，并对这些现象作了解释。     

新结构TEFL器件的等效电路图

本工作通过对新结构TFEL器件的Q－V曲线的分析，得到了新结构器件的等效电路图，该等效电路图也被器件的单向注入电荷与外加电压的关系曲线所证实。     

三维结构应用于储能器件的研究进展

锂离子电池和超级电容器作为新型储能器件因具有能量密度高、充放电效率高、绿色环保等诸多优点，能够应用于能源、汽车、电子器件等领域，备受研究者的关注。三维结构能够增大电极材料的单位立足面积，有效提高电极材料的利用效率，显著改善储能器件的电化学性能。为了进一步提升储能器件的电化学性能和拓宽其应用领域，设计制备具有3D结构的电极材料显得非常必要。主要对利用三维结构电极材料制备锂离子电池和超级电容器进行综述，分析了不同三维结构制备储能器件的优点以及存在的问题，并对三维储能器件的发展方向进行了展望。     

纳米 MOSFET/SOI器件新结构

重点介绍器件进入纳米尺度后出现的MOSFET／SOI器件的新结构，如超薄SOI器件、双栅MOSFET、FinFET和应变沟道等SOI器件，并对它们的性能进行了分析。     

新结构TFEL器件的等效电路图

本工作通过对新结构ＴＦＥＬ器件的Ｑ－Ｖ曲线的分析，得到了新结构器件的等效电路图。该等效电路图也被器件的单向注入电荷与外加电压的关系曲线所证实。     

集成化MEMS工艺设计技术的研究

针对目前MEMS研究领域中普遍存在的器件设计与加工工艺脱节的问题，提出了一种集成化的MEMS工艺设计技术。即在器件设计的过程中充分考虑加工工艺的特点和制约，提高器件的工艺设计能力和效率．这种工艺设计方法以结构材料、反应材料、工艺设备和环境限制的数据库为基础，从工艺过程为结构材料和反应物之间的物理或化学反应的角度出发，提炼出了工艺设计规则；在设计过程中，结合版图尺寸和具体的工艺参数，对工艺过程中器件结构二维断面上的所有结构材料的状态和图形进行计算和记录，并以此信息为依据结合设计规则判断工艺流程的合理性，并把相应的工艺信息、材料信息等代入器件的结构分析中去，实现MEMS器件的集成化工艺和结构设计．最后三维可视化设计工具IMEE1．0实现了集成化的设计技术，并通过对一个结构比较复杂的气体传感器进行设计和制作。验证了这种集成化工艺设计技术的可行性和实用性．     

一维ZnO纳米结构的场发射研究进展

一维纳米结构材料因其优异的电、光及场发射特性，在光电器件、场发射器件等方面具有重要的应用价值而备受关注。ZnO因具有优异的化学及热稳定性，并且其一维纳米结构具有极大的场增强因子，因而在场发射器件阴极中有良好的应用前景。首先简要介绍了ZnO的结构与性质，并重点介绍了ZnO一维纳米材料的常用制备技术及其在场发射领域的研究进展。     

Ag掺杂的K_2La_2Ti_3O_(10)可见光催化制氢的研究

采用高温固相法合成了具有可见光响应的Ag掺杂的K2La2Ti3O10催化剂,利用XRD、UV-VisDRS、TEM和XPS对催化剂进行了表征。考察了催化剂的可见光催化分解甲醇水溶液制氢的活性,并对可见光催化机理进行了分析。研究表明,Ag的掺杂没有改变K2La2Ti3O10的微晶结构,并使催化剂粒径有所减小。紫外-可见漫反射分析表明禁带宽度为2.8eV左右,对可见光具有较高吸收。担载2%(质量分数)Pt后,在可见光下光催化活性较K2La2Ti3O10大大提高,掺杂1%(摩尔分数)Ag的K2La2Ti3O10的产氢量为0.37mmol,而纯K2La2Ti3O10的产氢量只有0.037mmol;掺杂1%(摩尔分数)Ag的K2La2Ti3O10的产氢速率最大0.08mmol/h。     

Electron microscope study of dislocations introduced by deformation in a Si between 77 and 873 K

Dislocations were introduced into Si by scratching between 77 and 873 K. The nature and configurations of dislocations were determined by the weak-beam method. Dislocations introduced below 703 K were perfect dislocations of the shuffle set, while those introduced above 823 K were dissociated dislocations of the glide set. At 77 K, the shuffle set of dislocations was very straight; between RT and 363 K, the shuffle set of dislocations blunted, but mostly parallel to crystallographic orientations. Above 383 K, the shuffle set of dislocations was heavily zigzagged. The mechanism responsible for the zigzagging of the shuffle set of dislocations was discussed.     

Radiance Temperatures (in the Wavelength Range 521 to 1500 nm) of Rhenium and Iridium at Their Melting Points by a Pulse-Heating Technique

The melting-point radiance temperatures (at seven wavelengths in the range 521 to 1500 nm) of rhenium and iridium were measured by a pulse-heating technique. The method is based on rapid resistive self-heating of the specimen from room temperature to its melting point in less than 1 s and on simultaneously measuring the specimen radiance temperature every 0.5 ms with two high-speed pyrometers. Melting was manifested by a plateau in the radiance temperature-versus-time function for each wavelength. The melting-point radiance temperatures for a given specimen were determined by averaging the measured temperatures along the plateau at each wavelength. The melting-point radiance temperatures for each metal were determined by averaging results for several specimens at each wavelength. The results are as follows. Based on estimates of the random and systematic errors arising from pyrometry and specimen conditions, the expanded uncertainty (two standard-deviation level) in the reported values is ±8K.     

Correlation between cyclic deformation behaviour and microstructure in a duplex steel between 300 and 773 K

Cyclic tests performed in the temperature range 300–773 K on duplex stainless steel DIN 1.4460 show that the cyclic stress–strain behaviour of this steel is strongly temperature dependent. At 300 and 473 K an almost constant peak tensile stress stage, is followed by a slight softening that continues up to failure in the case of 300 K, but by a secondary hardening at 473 K. Pronounced initial cyclic hardening followed by secondary hardening was the main feature of the temperature range between 573 and 723 K. At 773 K, after a weak hardening stage, a strong softening continues up to failure. The mechanical behaviour and the evolution of the microstructure were analysed, and the internal and the effective stresses were studied. It was found that the internal stress is responsible for the strong hardening that occurs in the intermediate temperature range and for the softening at 773 K.     

Measurements of the surface tension for R290, R600a and R290/R600a mixture

The surface tensions of R290, R600a and R290/R600a mixture have been measured by the modified differential capillary-rise method. Twenty-two data points for R290 and 21 data points for R600a were obtained in the temperature range between 273 K and 354 K, and 43 data points for R290/R600a mixture on three isotherms of 278 K, 300 K and 320 K were obtained. The experimental uncertainties of temperature and surface tension are estimated to be within 20 mK and 0.2 mN m⁻¹, respectively. Surface tension correlations as a function of temperature for pure R290 and R600a were formulated in the temperature range between 253 K and critical temperature, and the correlation as a function of the composition for R290/R600a mixture was discussed at 278 K, 300 K and 320 K. It is found that the surface tension for R290/R600a mixture can be reproduced by the simple mixing rule by mole fraction with the correlations of both pure components.     

Radiance temperatures (in the wavelength range 522–906 nm) of niobium at its melting point by a pulse-heating technique

Radiance temperatures (at six wavelengths in the range 522–906 nm) of niobium at its melting point were measured by a pulse-heating technique. The method is based on rapid resistive self-heating of the specimen from room temperature to its melting point in less than 1 s and on simultaneously measuring the specimen radiance temperatures every 0.5 ms with a high-speed multiwavelength pyrometer. Melting was manifested by a plateau in the radiance temperatureversus-time function for each wavelength. The melting-point radiance temperatures for a given specimen were determined by averaging the measured temperatures along the plateau at each wavelength (standard deviation of an individual temperature from the mean: 0.1–0.4 K). The melting-point radiance temperatures for niobium were determined, by averaging the results at each wavelength for 10 specimens (standard deviation: 0.3 K), as follows: 2497 K at 522 nm, 2445 K at 617 nm, 2422 K at 653 nm, 2393 K at 708 nm, 2337 K at 809 nm, and 2282 K at 906 nm. Based on estimates of the random and systematic errors arising from pyrometry and specimen conditions, the total error in the reported values is about 5 K at 653 nm and 6 K at the other wavelengths.Paper presented at the Second Workshop on Subsecond Thermophysics, September 20–21, 1990, Torino, Italy.     

KDC法合成钛酸钾纤维的研究

本文研究了ＫＤＣ法合成钛酸钾纤维的过程、生长反应和合成条件;应用ＫＤＣ法合成了Ｋ２Ｔｉ２Ｏ５,Ｋ２Ｔｉ４Ｏ９、Ｋ２Ｔｉ６Ｏ１３等纤维状物质。     

Thermodynamics of Alkali Metal Uranoborates

The standard enthalpies of formation of crystalline A^IBUO₅ (A^I = Li, Na, K, Rb, Cs) at 298.15 K were determined by reaction calorimetry. For these compounds, the heat capacities in the range 10–300 K were determined by adiabatic vacuum calorimetry, and the thermodynamic functions were calculated. The standard entropies and Gibbs energies of formation at 298.15 K and the standard thermodynamic functions of solution of these compounds were calculated.     

Radiance temperatures (in the wavelength range 519–906 nm) of tungsten at its melting point by a pulse-heating technique

Radiance temperatures (at six wavelengths in the range 519–906 nm) of tungsten at its melting point were measured by a pulse-heating technique. The method is based on rapid resistive self-heating of the specimen from room temperature to its melting point in less than 1 s; and on simultaneously measuring the specimen radiance temperatures every 0.5 ms with a high-speed six-wavelength pyrometer. Melting was manifested by a plateau in the radiance temperature versus time function for each wavelength. The melting-point radiance temperatures for a given specimen were determined by averaging the measured temperatures along the plateau at each wavelength. The melting-point radiance temperatures for tungsten were determined by averaging the results at each wavelength for 10 specimens (standard deviation in the range 0.5–1.1 K, depending on the wavelength) as follows: 3319 K at 519 nm, 3236 K at 615 nm, 3207 K at 652 nm, 3157 K at 707 nm, 3078 K at 808 nm, and 2995 K at 906 nm. Based on estimates of the random and systematic errors arising from pyrometry and specimen conditions, the total uncertainty in the reported values is about ±7 K at 653 nm and ± 8 K at the other wavelengths.Paper presented at the Third Workshop on Subsecond Thermophysics, September 17–18, 1992, Graz, Austria.     

Radiance Temperatures (in the Wavelength Range 527 to 1500 nm) of Palladium and Platinum at Their Melting Points by a Pulse-Heating Technique

The radiance temperatures (at seven wavelengths in the range 527 to 1500 nm) of palladium and platinum at their respective melting points were measured by a pulse-heating technique. The method, based on rapid resistive self-heating of a specimen from room temperature to its melting point in less than 1 s, used two high-speed pyrometers to measure specimen radiance temperatures every 0.5 ms during the heating and melting period. Melting was manifested by a plateau in the radiance temperature-versus-time function for each wavelength. The melting-point radiance temperatures for a given specimen were determined by averaging the measured temperatures along the plateau at each wavelength. The melting-point radiance temperatures for each metal as determined by averaging the results for several specimens at each wavelength are as follows. Based on uncertainties arising from pyrometry and specimen conditions, the expanded uncertainty (two-standard deviation level) is about ±7 K for the reported values in the range 527 to 900 nm and about ±8 K for the reported values at 1500 nm.