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1.
Xuye Wang Guopu Shi Qinggang Li Junyan Wu Hao Wu Liu Zhang Zhi Wang 《Ceramics International》2021,47(2):2280-2287
Owing to the good physicochemical compatibility and complementary mechanical properties of Ti3SiC2 and Al2O3, Ti3SiC2/Al2O3 composites are considered as ideal structural materials. However, TiC and TiSi2 typically coexist during the synthesis of Ti3SiC2/Al2O3 composites through an in-situ reaction, which adversely affects the mechanical properties of the resulting composites. In this study, Ti3SiC2/Al2O3 composites were prepared via in-situ hot pressing sintering at 1450 °C. Ge, which was used as a sintering aid, improved the purity and mechanical properties of the Ti3SiC2/Al2O3 composites. This is because Ge replaced some of the Si atoms to compensate the evaporation loss of Si to form Ti3(Si1-xGex)C2, which showed a crystal structure similar to that of Ti3SiC2. Furthermore, the molten Ge accelerated the diffusion reaction of the raw materials, increasing the overall density of the Ti3SiC2/Al2O3 composites. The optimum Ge amount for improving the mechanical properties of the composites was found to be 0.3 mol. The flexural strength, fracture toughness, and microhardness of the composite with the optimum Ge amount were 640.2 MPa, 6.57 MPa m1/2, and 16.21 GPa, respectively. The formation of Ti3(Si1-xGex)C2 was confirmed by carrying out X-ray diffraction, energy dispersive spectroscopy, and transmission electron microscopy analyses. A model crystal structure of Ti3(Si1-xGex)C2 doped with 0.3 mol Ge was established by calculating the solid solubility of Ge. 相似文献
2.
Ningyu Chen Jintang Zhou Zhengjun Yao Yiming Lei Ruiyang Tan Yuxin Zuo Wenjian Zheng Zibao Jiao 《Ceramics International》2021,47(8):10545-10554
The electromagnetic materials are featured by good magnetic permeability and dielectric constant characteristics, which are of significant importance in solving the pollution problem of electromagnetic. In this study, after the complete of the use of sol-gel method, argon gas was then introduced for calcination, and eventually a new type of MWCNTs/Ni0.5Zn0.5Nd0.04Fe1.96O4 composites was synthesized after the above mentioned procedures. The synthesized MWCNTs were able to be adsorbed on the surface of Ni0.5Zn0.5Nd0.04Fe1.96O4 and could form a good conductive work of 3D. Also, the effect of additional MWCNTs on microwave absorption properties of MWCNTs/Ni0.5Zn0.5Nd0.04Fe1.96O4 composites were also observed in this study. The results indicate that the additional MWCNTs function to significantly improve the microwave absorption property of MWCNTs/Ni0.5Zn0.5Nd0.04Fe1.96O4. Through altering the amount of MWCNTs, the microwave attenuation performance and impedance matching coefficient of this electromagnetic materials can be effectively improved. The S2 sample presented a minimum reflection loss of ?35.05 dB when its thickness reached 1.6 mm, meanwhile, the effective absorption bandwidth achieved 4.55 GHz. The prepared composites perform well in microwave absorption, which can attribute to the reasonable ratio of composites as well as its interaction with both of the magnetic and dielectric components. This research paved the way for novel ideas to be put in the electromagnetic absorption materials with high-efficient. 相似文献
3.
随着对环保及自用水率的要求日益严格,水厂生产废水的减排已成为发展趋势.但既有水厂用地紧张和生产废水的处理工艺占地多存在矛盾,制约了水厂新增生产废水处理工艺的可行性.文中引入斜管沉淀提升沉淀效率、取消浓缩池、使用叠螺脱水机代替离心脱水机的优化设计方案,相较原设计的传统分离式生产废水处理工艺,生产废水停留时间减少75%,占地面积减少约48%.实践证明,该优化设计方案能够有效解决水厂生产废水处理工艺设计过程中遇到的用地不足问题,并有效地降低建设投资. 相似文献
4.
Wan-Li Tan Dr. Chun Zhang Yang Li Dr. Kai Guo Dr. Xiao-Wei Gao Dr. Jun Wei Dr. Dong Yi Prof. Lin Pu Prof. Dr. Qin Wang 《ChemMedChem》2021,16(23):3569-3575
Forty samples of optically active falcarindiol analogues are synthesized by using the easily available C2 symmetric (R)- and (S)-1,1’-binaphth-2-ol (BINOL) in combination with Ti(OiPr)4, Zn powder and EtI. Their anticancer activities on Hccc-9810, HepG2, MDA-MB-231, Hela, MG-63 and H460 cells are assayed to elucidate their structure-activity relationships. These results showed that the falcarindiol analogue (3R,8S)- 2 i with the terminal double bond has the most potent anti-proliferation effect on Hccc-9810 cells with IC50 value of 0.46 μM. The falcarindiol analogue (3R,8S)- 2 i can induce obvious Hccc-9810 cell apoptosis in a concentration-dependent manner by Hoechst staining and flow cytometry analysis. The proposed mechanism suggests that the falcarindiol analogue (3R,8S)- 2 i increases LDH release and MDA content, and reduces the levels of SOD activity, which lead to the accumulation of oxidative stress and induce apoptosis in Hccc-9810 cells. 相似文献
5.
Phuong-Anh Ngoc Doan Tzyi-Horng Tan Lee Fong Siow Beng Ti Tey Eng Seng Chan Teck-Kim Tang Nur Azwani Abdul Karim Eng-Tong Phuah Yee-Ying Lee 《Journal of the American Oil Chemists' Society》2021,98(6):609-620
Palm fatty acid distillate (PFAD) is a rich source of vitamin E. As compared to other vegetable oil, PFAD has higher tocotrienol (70–80%) over tocopherol content, which makes it a valuable source for vitamin E extraction. Current vitamin E extraction methods are not sustainable due to the intensive usage of chemical and high operational cost. Hence, the present study investigated for the first time using dry fractionation process as a green and economical pretreatment method for separating solid fraction (stearin) and liquid fraction (olein) in order to concentrate vitamin E from PFAD in olein fraction. We examined the dry fractionation conditions: crystallization ending temperature (36–44 °C), cooling rate (0.3 and 1.5°C min−1), stirring speed (20–125 rpm), and holding time (0–60 min) on the composition of unsaturated and saturated fatty acids as well as vitamin E content in liquid fraction (olein) and solid fraction (stearin) using gas chromatography and high performance liquid chromatography, respectively. In most of these conditions, vitamin E was ultimately higher in olein fraction as compared to stearin fraction, which is correlated with the high degree of unsaturation. Under a cooling rate of 0.3°C min−1, 90 rpm stirring speed, and ending crystallization of 38 °C, the highest vitamin E rich olein fraction was attained with 1479 ± 10.51 ppm in 50 g olein fraction as compared to 1366 ± 7.94 ppm in 500 g of unfractionated PFAD. 相似文献
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8.
Yang Zhi Yang Jian Wang Qiang Sun Fengjing 《Chemistry and Technology of Fuels and Oils》2022,58(3):554-560
Chemistry and Technology of Fuels and Oils - For shale gas wells, plunger lift is challenged by the difficulties like difficult tool tripping in and high operation risks due to the liquid phase... 相似文献
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10.
Buhari Adamu Muhammad Ooi Chee-Pun Baskaran Vishnu Monn Phan Raphael CW Wong KokSheik Tan Wooi-Haw 《Multimedia Tools and Applications》2022,81(7):9151-9176
Multimedia Tools and Applications - The interest in real-time micro-expression recognition has increased with the current trend in human-computer interaction applications. Presently, there are... 相似文献