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1.
Zhai Shengnan Yu Kejing Meng Chaoran Wang Hongbo Fu Jiajia 《Journal of Materials Science》2022,57(15):7491-7502
Journal of Materials Science - In this paper, an eco-friendly method of producing hybrid silica aerogels by freeze-drying method (FD) is proposed. In the freeze-drying system, deionized water was... 相似文献
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Le Fang Qian Sun Yong-Hong Duan Jing Zhai Dan Wang Jie-Xin Wang 《Frontiers of Chemical Science and Engineering》2021,15(4):902
BaSO4 nanoparticles as important functional materials have attracted considerable research interests, due to their X-rays barrier and absorption properties. However, most of BaSO4 nanoparticles prepared by traditional technology are nanopowders with broad size distribution and poor dispersibility, which may greatly limit their applications. To the best of our knowledge, the synthesis of transparent BaSO4 nanodispersions was rarely reported. Here, we firstly present a novel and efficient method to prepare transparent and stable BaSO4 nanodispersions with a relatively small particle size around 10 to 17 nm using a precipitation method in a rotating packed bed (RPB), followed by a modification treatment using stearic acid. Compared with the BaSO4 prepared in a traditional stirred tank, the product prepared using an RPB has much smaller particle size and narrower size distribution. More importantly, by using RPB, the reaction time can be significantly decreased from 20 min to 18 s. Furthermore, the transparent BaSO4-polyvinyl butyral nanocomposite films with good X-ray shielding performance can be easily fabricated. We believe that the stable BaSO4 nanodispersions may have a wide range of applications for transparent composite materials and coatings with X-ray shielding performance for future research. 相似文献
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Li-Xiang Wu Lin-Lin Zhu Wei-Ming Guo Shi-Kuan Sun Wen-Bin Niu Jia-Xiang Xue Jian-Han Zhai Hai-Bin Ma Rui-Lin Lin Hua-Tay Lin Kevin Plucknett Ye-Hong Liao Tong Liu Qi-Sen Ren 《Journal of the European Ceramic Society》2021,41(1):225-232
The joining of liquid-phase sintered SiC (LPS-SiC) ceramics was conducted using spark plasma sintering (SPS), through solid state diffusion bonding, with Ti-metal foil as a joining interlayer. Samples were joined at 1400 °C, under applied pressures of either 10 or 30 MPa, and with different atmospheres (argon, Ar, vs. vacuum). It was demonstrated that the shear strength of the joints increased with an increase in the applied joining pressure. The joining atmosphere also affected on both the microstructure and shear strength of the SiC joints. The composition and microstructure of the interlayer were examined to understand the mechanism. As a result, a SiC-SiC joining with a good mechanical performance could be achieved under an Ar environment, which in turn could provide a cost-effective approach and greatly widen the applications of SiC ceramic components with complex shape. 相似文献
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In order to comply with discharge standards, a gas–solid separator is used to remove solid particles from the thorium molten salt reactor-solid fuel(TMSR-SF)system. As a key component, it directly determines system energy efficiency. However, current gas–solid separators,based on activated carbon adsorption technology, result in high pressure drops and increased maintenance costs. In the present study, a new combined gas–solid separator was developed for the TMSR-SF. Based on a simplified computational fluid dynamics(CFD) model, the gas–solid twophase flow and the motion trajectory of solid particles were simulated for this new separator using commercial ANSYS 16.0 software. The flow and separation mechanism for this structure were also been discussed in terms of their velocity effects and pressure field distributions, and then the structure was optimized based on the influence of key structural parameters on pressure and separation efficiency. The results showed that the standard k–e model could be achieved and accurately simulated the new combined separator. In this new combined gas–solid separator, coarse particles are separated in the first stage using rotating centrifugal motion, and then fine particles are filtered in the second stage, giving a separation efficiency of up to 96.11%. The optimum blade inclination angle and numbers were calculated to be 45° and four, respectively. It implicated that the combined separator could be of great significance in a wide variety of applications. 相似文献
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Junqi Chen Weishuang Fang Yifan Zhai Feihu Li Ying Tang Jie Li Huanhuan Guo Liang Fang 《Journal of the European Ceramic Society》2021,41(8):4473-4477
Orthorhombic-structured CaIn2O4 ceramics with a space group Pca21 were synthesized via a solid-state reaction method. A high relative density (95.6 %) and excellent microwave dielectric properties (εr ~11.28, Qf = 74,200 GHz, τf ~ ?4.6 ppm/°C) were obtained when the ceramics were sintered at 1375 °C for 6 h. The dielectric properties were investigated on the basis of the Phillips–Van Vechten–Levine chemical bond theory. Results indicated that the dielectric properties were mainly determined by the InO bonds in the CaIn2O4 ceramics. These bonds contributed more (74.65 %) to the dielectric constant than the CaO bonds (25.35 %). Furthermore, the intrinsic dielectric properties of the CaIn2O4 ceramics were investigated via infrared reflectivity spectroscopy. The extrapolated microwave dielectric properties were εr ~10.12 and Qf = 112,200 GHz. Results indicated that ion polarization is the main contributor to the dielectric constant in microwave frequency ranges. 相似文献
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步入新时代,我国经济实现了跨越式发展,企业面临着更多的发展机遇与挑战,但只有牢牢守住"安全生产"这一警戒线,一切生产经营活动才能真正创造经济价值.现介绍一起电镀企业失火事故,通过分析认定事故原因,并结合类似事故案例,探寻事故频发的深层原因,提出有效的预防对策和措施,希望引发从事电镀生产及安全管理、消防工作人员的深度思考,提供可借鉴的有益经验,为企业安全生产保驾护航. 相似文献
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氨基羟基脲(HSC)是一种新型无盐试剂,可有效控制后处理料液中钚的价态,实现铀钚分离和钚的纯化,其含量是后处理工艺中的一项重要参数,需准确测定。本文根据HSC和对二甲氨基苯甲醛在酸性介质中发生显色反应,其产物在456 nm处有明显特征吸收的原理,建立了后处理料液中HSC的分析方法,并优化了分析条件。结果表明,HSC的最佳测量条件为测量波长456 nm、显色温度80~90 ℃(水浴)、显色时间45 min,NO-2、Fe3+、N2H4及其他共存组分对HSC的测定无明显影响。HSC含量在2.5~60.0 μmol/L范围内符合比耳定律,R2为0.999 9,测量精密度优于5.0%。在45 d内工作曲线重复性好,具有良好的长期稳定性。真实样品的测量结果显示,其重加回收率在99%~105%之间。 相似文献