SiC埋层结构与C^＋注入剂量关系

采用ＭｅｔａｌＶａｐｏｒＶａｃｕｕｍＡｒｃ（ＭＥＶＶＡ）离子源的离子束合成法，往Ｓｉ衬底注入剂量为３．０×１０＾１７～１．６×１０＾１８ｃｍ＾－２的Ｃ＾＋制成ＳｉＣ埋层，Ｃ＾＋离子束的引出能量为５０ｋｅＶ，光电子能谱和红外吸收谱表明ＳｉＣ埋层的结构特征明显地依赖于剂量，采用ＭＥＶＶＡ离子源可以平均衬底温度低于４００℃时得到含有立方结构的ＳｉＣ埋层。     

亚毫安室温连续工作InGaAs垂直腔面发射激光器

报道了ＩｎＧａＡｓ应变量子讲垂直腔面发射激光器（ＶＣＳＥＬ）的室温连续工作。在ＭＢＥ生长过程中利用红外高温仪测量了表观衬底热辐射振荡，实现了原位厚度监测；采用阶梯型分布布拉格反射器（ＤＢＲ）及腐蚀倒台面结构，降低了器件串联电阻。对于２×３μｍ２的台面结构ＶＣＳＥＬ，室温连续工作阈值电流一般为１．５ｍＡ，最低达到０．７ｍＡ，阈值电压为２．５伏，输出功率达到０．５ｍＷ，激射波长为０．９４ｕｍ，量子效率为１２％。     

改性酚醛环氧—PTFE耐磨防蚀涂层

介绍了一种改性酚醛环氧－ＰＴＦＥ耐磨防蚀涂层。这种涂层Ｔｉｍｋｅｎ试验机上于３１２Ｎ，２．５ｍ／ｓａ下耐磨寿命可达１３５００ｍ／μｍ，摩擦系数为０．１６－０．２０；在スウスト试验机上３ＭＰａ、０．２ｍ／ｓ，干燥空气和相对湿度为５０％中耐磨寿命均大于２．５×１０＾５周。经５％ＮａＣｌ盐雾试验１００ｈ后，底材与涂层的粘结强度，抗冲击强度及     

改性酚醛环氧－PTFE耐磨防蚀涂层

介绍了一种改性酚醛环氧－ＰＴＦＥ耐磨防蚀涂层。这种涂层在Ｔｉｍｋｅｎ（环－块）试验机上于３１２Ｎ、２．５ｍ／ｓ下耐磨寿命可达１３５００ｍ／μｍ，摩擦系数为０．１６～０．２０；在试验机上３ＭＰａ、０．２ｍ／ｓ、干燥空气和相对湿度为５０％中耐磨寿命均大于２．５×１０５周。经５％ＮａＣｌ盐雾试验１００ｈ后，底材与涂层的粘结强度、抗冲击强度及柔韧性等良好，低碳钢底材无锈蚀，可广泛应用于耐磨及防蚀等场合。     

二维光纤列阵接口器件及其在光互连网络模块中的应用

提出了一种适用于光电子集成ＣＭＯＳ－ＳＥＥＤ灵巧像素光互连网络的二维光纤束列阵结构和制作方法, 采用精密加工的光纤列阵定位槽和光学监控系统, 成功地研制出３２×２ 的单模和多模光纤列阵Ｉ／Ｏ接口器件, 光纤列阵层内及层间位移误差均小于２μｍ , 角向差小于０．０２°。实验中, 已将二维光纤列阵Ｉ／Ｏ接口器件用于１６×１６ ＣＭＯＳ－ＳＥＥＤ灵巧像素光电子集成Ｃｒｏｓｓｂａｒ光互连模块中, 实验结果表明, 该光纤束列阵Ｉ／Ｏ接口器件完全满足光互连系统的高精度要求。     

一氧化碳和苯乙烯交替共聚物的合成与表征

利用乙酸钯和２，２′－联吡啶组成的催化剂体系催化一氧化碳和苯乙烯交替共聚合成出聚（１－氧代－２－苯基丙撑）（ＳＴＣＯ）。采用ＩＲ、ＮＭＲ、元素分析以及广角Ｘ光散射对该聚合物以表征。该共聚物晶体为单斜晶胞，晶胞参数为ａ＝１５．７×１０－１０ｍ，ｂ＝６．１７×１０－１０ｍ，ｃ＝７．４５×１０－１０ｍ，α＝９０．０°，β＝１０４．３°，γ＝９０．０°；晶胞体积为６９７．２×１０－３０ｍ３；空间点群为Ｐ２１／ｃ。此外，对该共聚物热降解进行了初步研究。     

DBM-g-PE与PVC的相互作用研究EI

采用固相接枝法制备了ＤＢＭ－ｇ－ＰＥ，用红外光谱分析证明了接枝物确实存在。ＰＶＣ／ＣＰＥ＝１００／５合金性能测定结果表明，添加５份接枝物的合金（Ａ），缺口冲击强度、拉伸强度分别为１８．２ｋＪ／ｍ２和５３．０ＭＰａ；而添加５份ＰＥ的合金（Ｂ），其相应性能为５．１ｋＪ／ｍ２和３３．８ＭＰａ。不加接枝物的合金（Ｃ），虽有高韧性，但拉伸强度却由５３．０ＭＰａ降至５０．２ＭＰａ。ＤＳＣ、ＳＥＭ的结果均表明，ＰＥ接枝ＤＢＭ后与ＰＶＣ的相互作用增强，与ＣＰＥ协同作用能增韧、增强ＰＶＣ，并探讨了其机理。     

双甲基丙烯酰氧基聚乙二醇与甲基丙烯酸盐共聚及导电性

在合成α，ω－双甲基丙烯酰氧基封端的聚乙二醇（ＢＭＡＰＥＧ）的基础上，通过ＢＭＡＰＥＧ与甲基丙烯酸盐（ＭＡＡＭ）共聚，制备了离子导电率（σ）在３０℃时为４．０×１０－６Ｓ／ｃｍ的单离子传导的ＡＢ交联型聚醚类固体电解质（ＡＢＣＰＥ）。研究了影响ＡＢＣＰＥ离子导电率的因素。结果表明，用甲基丙烯酰氯与聚乙二醇进行酯化反应可以合成所期望结构的ＢＭＡＰＥＧ。ＡＢＣＰＥ的σ随ＰＥＧ链段长度和共聚单体浓度的增加出现最大值；降低ＢＭＡＰＥＧ的双键官能度，或升高温度，σ升高。     

双马来酰亚胺作EPDM硫化胶的结构稳定剂

用热空气老化系数、压缩永久变形和热失重（ＴＧ）表征ＥＰＤＭ 硫化胶的热稳定性。结果表明，未加Ｎ，Ｎ′－间苯撑双马来酰亚胺（ＭＰＢＭ）的ＥＰＤＭ 硫化胶经１２０ ℃×７２ ｈ 和１５０ ℃×７２ ｈ 热空气老化后，伸长率的老化系数分别为０．７０ 和０．４２，而加入２ ｐｈｒ的ＭＰＢＭ 后，则分别为０．７８ 和０．６０，１２０ ℃×２２ ｈ 和１５０ ℃×２２ ｈ 的压缩永久变形，未加ＭＰＢＭ 时分别是７３％ 和８４．９％ ，而加入２ ｐｈｒ的ＭＰＢＭ 后则为５９．６％ 和７５％ ，增加ＭＰＢＭ 用量，压缩永久变形率进一步降低。非等温热失重分析表明，起始失重温度、失重终止温度都因加入２ ｐｈｒＭＰＢＭ 而向高温方向移动了４ ℃左右，加入５ ｐｈｒＭＰＢＭ 则提高了近１０ ℃，表明ＭＰＢＭ 不仅可作ＥＰＤＭ 的交联助剂，同时是老化过程中的结构稳定剂。     

波分复用系统中功率代价的测试

介绍了波分复用（ＷＤＭ）系统中功率代价的起因、测试方法和测试顺序,指出了各种起因对系统性能的影响,并提出了减小相应功率代价的方法。给出了８×２．５Ｇｂ／ｓ×（３×１５０ｋｍ常规单模光纤）ＷＤＭ系统中第６信道和第８信道的功率代价测试结果,ＣＨ８的总功率代价为１．８ｄＢ,其中色散代价为０．８ｄＢ,ＡＳＥ代价为０．９ｄＢ,串话代价为０．１ｄＢ;而ＣＨ６的总功率代价则仅有０．６ｄＢ。     

电磁铸造与普通连续铸造2024铝合金的组织性能对比

采用电磁铸造技术和普通连续铸造技术铸造了2024变形铝合金，采用光学显微镜和扫描电镜分析了其显微组织，而且对其进行了固溶处理加人工时效。结果表明电磁铸造锭内部组织细小均匀，有高的硬度和良好的疲劳性能，电磁铸造试样的硬度大约是普通连续铸造铸坯的2倍，疲劳性能是普通连续铸造铸坯的3倍。电磁铸造铸坯还有良好的耐磨性，磨损失重量是普通连续铸造的一半。     

The properties of AlN-filled epoxy molding compounds by the effects of filler size distribution

AlN filler was compared with crystalline silica as a filler for advanced epoxy molding compounds. Properties such as the thermal conductivity, dielectric constant, CTE, flexural strength, elastic modullus and water absorption ratio of water-resistant grade AlN-filled molding compounds according to the contents or size of AlN and the filler size distribution were evaluated. A spiral flow test was also carried out to measure the change in viscosity according to the AlN size distribution for improved fluidity. The properties of EMC that is filled with a 70 vol.% of 12 micron AlN was compared with a crystalline silica-filled EMC. Thermal conductivity was improved by 2.2 times, the dielectric constant was reduced to less than one-half, the flexural strength was improved, and the CTE was also reduced. A binary mixture of an AlN-filled (65 vol.%) EMC showed improved fluidity, thermal conductivity, dielectric constant, flexural strength and water resistance compared to a single-size AlN-filled EMC. The maximum improvement was obtained when the fraction of small particles in the binary mixture of the AlN is 0.2–0.3. The CTE of EMC was decreased by increasing the volume fraction of small particles in the binary mixture of the AlN.     

电磁铸造5182铝合金锭的组织与性能研究

采用电磁铸造技术铸造了易拉罐用5182变形铝合金，采用光学显微镜和扫描电镜分析了其显微组织，而且对其进行了均匀化处理和对比实验。结果表明，电磁铸造锭有更加良好的内部组织和优良的力学性能，电磁铸造试样的硬度大约是普通连续铸造试样的两倍，疲劳性能是普通连续铸造铸锭的3倍，电磁铸造铸锭还有良好的耐磨性，电磁铸造锭的优良性能得宜于电磁搅拌的作用使整个铸锭获得均匀细小的晶粒组织，电磁铸造技术是一种无模铸造技术，它依靠电磁力约束液体金属成型，液体金属不与铸模接触，铸锭表面光滑如镜；相反，普通连续铸造锭表面因存在振动痕和亚表面偏析等铸造缺陷，力学性能大大降低。     

Microstructure and performance of energetically modified cement (EMC) with high filler content

Energetically modified cement (EMC) has been produced by high intensive grinding/activation of normal portland cement (NPC) together with 20% and 50% quartz sand. EMC concretes were compared to NPC based concrete using the k-factor concept. The k-factor for concrete with w/c = 0.60–0.45 was 0.7–0.9 for 1 d and 1.1–1.3 for 28 d compressive strength. k > 1 for both capillary suction, porosity, vapor diffusion and chloride permeability. For carbonation resistance k was ≈0.55.Microstructure of EMC paste with 50% quartz sand and w/c = 0.40 showed that the quartz was extensively ground and formed agglomerates with cement having a high inner surface. The degree of hydration of the cement in EMC was as high as 71% after 1 d compared to 45% for untreated blend. Refined pore size distribution of EMC versus the blend means that even for equal hydration at higher ages EMC will perform better.     

单向EMC层合板非线性弯曲行为

对单向形状记忆聚合物复合材料(EMC)层合板在其基体玻璃化转变温度(T_g)之上的弯曲行为进行了研究。首先介绍了EMC层合板多约束弯曲变形实验, 并依据纤维微屈曲变形特征建立其形函数; 然后分析得出弯曲层合板的各分应变能及由其组成的总应变能; 在此基础上, 依据虚功原理, 通过总应变能推导出外力偶矩与曲率、 等效弯曲应变之间的非线性关系式。结果表明: 在EMC板的弯曲过程中, 中性层很快接近板的拉伸表面, 且中性层位置及板的弯曲行为对板的面内剪切模量非常敏感; 在板的初始弯曲阶段, 弯矩与曲率遵循传统单向板的线弹性弯曲理论; 而后随着曲率的增加, 弯矩与曲率关系遵循本研究所提出的非线性关系, 所得理论结果与EMC层合板的四点纯弯曲实验现象较为吻合。      

Equilibrium moisture content of radiata pine at elevated temperature and pressure reveals measurement challenges

Relatively few studies have been performed on the equilibrium moisture content (EMC) of wood under conditions of elevated temperature and pressure. Eight studies indicated that EMC near saturation decreased between 100 and 150 °C, whilst five studies indicated that EMC increased. The aim of this study was to identify the likely source of the disagreement using radiata pine (Pinus radiata D. Don) sapwood which was conditioned to a moisture content of around 3 % and then exposed for 1 h at 150 °C and relative humidities of either 50, 70 or 90 %. Mean values of EMC, obtained through in situ gravimetric analyses, were 5.7, 7.6 and 12.6 % with 95 % confidence intervals of the order of 1 %. In two further experiments, the humidity was allowed to rise briefly above 90 % and the moisture content after 1 h was found to be >30 % as in the five studies that indicated EMC increased above 100 °C. The high moisture contents were attributed to condensation of liquid water on the specimen with subsequent evaporation at a rate that was too slow for the moisture content to reach equilibrium before it was measured. Reliable EMC data at elevated temperatures require (1) tight process control of experimental conditions with minimal standard error, (2) specimens with low initial moisture content to avoid unwanted wood mass loss over time, (3) a relative humidity upper limit that avoids drift above 95 %, and (4) extrapolation of data to humidity approaching 100 %.     

集成电路封装用环氧模塑料的绿色阻燃

合成了三聚氰胺改性含氮酚醛树脂,以邻甲酚醛环氧树脂为基体树脂,以自制的改性酚醛树脂为固化剂和阻燃剂,对集成电路封装用环氧模塑料绿色阻燃配方及工艺进行了研究。结果表明自制的改性酚醛树脂固化能力好,阻燃效果好。     

Granulare ultradünne Nanoschichtsysteme Fe/FeO auf Aluminiumsubstrat,Modellierung einer 1 D ultradünnen granularen Schicht für elektromagnetische Verträglichkeitsanwendungen (EMV) der Flachbandkabeltechnik

Granular magnetic ultrathinthin multilayer films Fe/ FeO on Al substrates, modelling of a 1 D granulare thin film for EMC applications Hematite ferrite thin films in granular structures have attracted much attention as materials with unique proper ties. One of these properties is enhanced microwave absorption for a good EMC application. This gives a possibility to absorption electro magnetic covers ( EMC ) of cable application with ultrathin thickness and granular structure. The Electromagnetic Compatibility absorption of granular Ferrite polycristalline sample is 6 ‐ 7 dB in the GH z ‐ range.     

On combination of the equivalent material concept and J‐integral criterion for ductile failure prediction of U‐notches subjected to tension

The aim of the present research is to check the capability of the equivalent material concept (EMC) combined with the J‐integral failure criterion, called EMC‐J criterion, in predicting the load‐carrying capacity (LCC) of U‐notched ductile aluminium plates subjected to tension by considering the 2 moderate and large‐scale yielding regimes. For this purpose, first, a set of experimental results on LCC of 2 groups of thin U‐notched rectangular plates made of Al 7075‐T6 and Al 6061‐T6 are gathered from the recent literature. Then, because the Al 7075‐T6 and Al 6061‐T6 plates have ductile behaviour, EMC is employed to avoid performing elastic‐plastic failure analysis for LCC predictions. Up to now, different failure models in the context of the linear‐elastic notch fracture mechanics have been successfully utilized in combination with EMC for ductile failure prediction of notched members. However, this is the first time in this research that J‐integral, as a well‐known brittle failure criterion, is linked to EMC for predicting LCC of the U‐notched rectangular aluminium plates. Finally, it is shown that EMC‐J criterion can predict well the experimental results of tensile LCC.     

合同能源管理在我国供热空调系统中的应用前景分析

针对我国的能源形势,分析了供热空调系统的节能潜力,介绍了具有很好发展前景的合同能源管理概念、方法和步骤,以及在我国实施过程中出现的问题及对策.以实际空调和供热工程的案例对合同能源管理的效益进行了分析,结果表明,合同能源管理是一种业主和合同能源管理公司双赢的模式,在我国供热和空调行业有广阔的应用前景.